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1-Acetylpiperazine

1-Acetylpiperazine structure

CAS No.: 13889-98-0

Chemical Name:: 1-Acetylpiperazine

Synonyms: N-ACETYLPIPERAZINE;1-AcetyL;AKOS BB-5737;acetylpiperazine;N-aetylpiperazine;1-ACETYLPIPERAZINE;N-ACETY PIPERAZINE;n-acetyl ptperazine;1-Piperazinoethanone;Olaparib Impurity 61

CBNumber:: CB1717961

Molecular Formula:: C6H12N2O

Molecular Weight:: 128.17

MDL Number:: MFCD00058676

MOL File:: 13889-98-0.mol

MSDS File:: SDS

Last updated:2023-08-16 18:05:29

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1-Acetylpiperazine Properties

Melting point	31-34 °C (lit.)
Boiling point	127 °C
Density	1.0754 (rough estimate)
refractive index	1.4880 (estimate)
Flash point	>230 °F
storage temp.	Keep in dark place,Inert atmosphere,Room temperature
solubility	methanol: soluble1g/10 mL, clear, colorless to faintly greenish-yellow
form	Liquid After Melting
pka	8.50±0.10(Predicted)
color	Clear light yellow
Water Solubility	Soluble in water 210 g/L (20°C).
Sensitive	Hygroscopic
BRN	112220
CAS DataBase Reference	13889-98-0(CAS DataBase Reference)
FDA UNII	A64RRE6QT5

SAFETY

Risk and Safety Statements

Symbol(GHS)

GHS05,GHS07,GHS08

Signal word

Danger

Hazard statements

H302-H314-H334-H335

Precautionary statements

P261-P301+P312+P330-P303+P361+P353-P304+P340+P312-P305+P351+P338-P342+P311

Hazard Codes

Risk Statements

36/38-36/37/38

Safety Statements

26-36-37/39

WGK Germany

3-10-34

Hazard Note

Irritant

HS Code

29339900

NFPA 704

	1
2		0

1-Acetylpiperazine price More Price(34)

Manufacturer	Product number	Product description	CAS number	Packaging	Price	Updated	Buy
Sigma-Aldrich	359513	1-Acetylpiperazine 99%	13889-98-0	5g	$57.9	2024-03-01	Buy
Sigma-Aldrich	359513	1-Acetylpiperazine 99%	13889-98-0	25g	$162	2024-03-01	Buy
TCI Chemical	A1399	1-Acetylpiperazine >98.0%(GC)(T)	13889-98-0	5g	$16	2024-03-01	Buy
TCI Chemical	A1399	1-Acetylpiperazine >98.0%(GC)(T)	13889-98-0	25g	$38	2024-03-01	Buy
Alfa Aesar	B20200	1-Acetylpiperazine, 99%	13889-98-0	5g	$41.65	2024-03-01	Buy

Product number	Packaging	Price	Buy
359513	5g	$57.9	Buy
359513	25g	$162	Buy
A1399	5g	$16	Buy
A1399	25g	$38	Buy
B20200	5g	$41.65	Buy

1-Acetylpiperazine Chemical Properties,Uses,Production

Chemical Properties

clear light yellow liquid after melting

Uses

1-Acetylpiperazine may be used in the synthesis of series of 7-alkoxyl substituted indolizinoquinoline-5,12-dione derivatives and 2-substituted-N-(naphth-1-ylmethyl)-pyrimidin-4-amines and 2-substituted-N-benzhydrylpyrimidin-4-amines.

Definition

ChEBI: 1-Acetylpiperazine is a member of phytanoyl-CoAs.

General Description

Infrared and Raman spectra of 1-acetylpiperazine have been recorded in the region of 4000-40cm^-1.

Purification Methods

Purify 1-acetylpiperazine by recrystallisation from 40% aqueous EtOH or from EtOH/Et2O. It is an irritant, and is hygroscopic. The hydrochloride has m 191o (from EtOH), and the tosylate salt has m 148-149o (from EtOH/EtOAc, 1:16). The free base, however, cannot be isolated by basifying the tosylate salt and extraction with CH2Cl2. [Jacobi Chem Ber 66 113 1933, Mosher et al. J Am Chem Soc 75 4949 1953, Hall J Am Chem Soc 78 2570 1956, Beilstein 23 IV 1786.]

1-Acetylpiperazine synthesis

Synthesis of 1-Acetylpiperazine from Piperazine and Acetic anhydride

1-Acetylpiperazine Preparation Products And Raw materials

Raw materials

Silica gel PIPERAZINE HEXAHYDRATE Acetic anhydride Sodium sulfate Acetyl chloride

Potassium carbonate Triethylamine Chloroform Piperazine Tetrahydrofuran

Dichloromethane Acetic acid Methanol Sodium hydroxide Magnesium sulfate

PETROLEUM ETHER

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Preparation Products

(4-ACETYL-PIPERAZIN-1-YL)-ACETIC ACID methyl 4-(4-acetylpiperazin-1-yl)benzoate

1-Acetylpiperazine Suppliers

Global( 351)Suppliers

Supplier	Tel	Email	Country	ProdList	Advantage
Hebei Mojin Biotechnology Co., Ltd	+8613288715578	sales@hbmojin.com	China	12456	58
Henan Tianfu Chemical Co.,Ltd.	+86-0371-55170693 +86-19937530512	info@tianfuchem.com	China	21691	55
career henan chemical co	+86-0371-86658258	sales@coreychem.com	China	29914	58
Changzhou Ansciep Chemical Co., Ltd.	+86 519 86305871	sales@ansciepchem.com	CHINA	4242	58
Hubei Jusheng Technology Co.,Ltd.	18871490254	linda@hubeijusheng.com	CHINA	28180	58
Jinan Finer Chemical Co., Ltd	+86-531-88989536 +86-15508631887	sales@finerchem.com	China	2967	58
Accela ChemBio Inc.	(+1)-858-699-3322	info@accelachem.com	United States	19965	58
Hebei Guanlang Biotechnology Co., Ltd.	+86-19930503282	alice@crovellbio.com	China	8823	58
Xi'an Kono chem co., Ltd.,	029-86107037 13289246953	info@konochemical.com	China	2995	58
Chongqing Chemdad Co., Ltd	+86-023-61398051 +8613650506873	sales@chemdad.com	China	39916	58

Supplier	Advantage
Hebei Mojin Biotechnology Co., Ltd	58
Henan Tianfu Chemical Co.,Ltd.	55
career henan chemical co	58
Changzhou Ansciep Chemical Co., Ltd.	58
Hubei Jusheng Technology Co.,Ltd.	58
Jinan Finer Chemical Co., Ltd	58
Accela ChemBio Inc.	58
Hebei Guanlang Biotechnology Co., Ltd.	58
Xi'an Kono chem co., Ltd.,	58
Chongqing Chemdad Co., Ltd	58

View Lastest Price from 1-Acetylpiperazine manufacturers

Update time	Product	Price	Min. Order	Purity	Supply Ability	Manufacturer
2023-08-16	1-Acetylpiperazine 13889-98-0	US $0.00 / KG	1KG	99%	50000KG/month	Hebei Mojin Biotechnology Co., Ltd
2023-07-27	1-Acetylpiperazine 13889-98-0	US $1.50 / g	1g	99.0% Min	100 Tons	Shaanxi Didu New Materials Co. Ltd
2022-02-19	1-Acetylpiperazine 13889-98-0	US $1.10 / g	1g	99.00%	100 Tons	Dideu Industries Group Limited

1-Acetylpiperazine
13889-98-0
US $0.00 / KG
99%
Hebei Mojin Biotechnology Co., Ltd

1-Acetylpiperazine
13889-98-0
US $1.50 / g
99.0% Min
Shaanxi Didu New Materials Co. Ltd

1-Acetylpiperazine
13889-98-0
US $1.10 / g
99.00%
Dideu Industries Group Limited

1-Acetylpiperazine Spectrum

1-Acetylpiperazine(13889-98-0)MS 1-Acetylpiperazine(13889-98-0)¹HNMR 1-Acetylpiperazine(13889-98-0)¹³CNMR 1-Acetylpiperazine(13889-98-0)IR1

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AKOS BB-5737 1-ACETYLPIPERAZINE 1-PIPERAZIN-1-YL-ETHANONE acetylpiperazine N-Acetylpiperazine97% N-Acetylpiperazine,99% n-acetyl ptperazine N-aetylpiperazine N-ACETY PIPERAZINE 1-Piperazinoethanone 1-Acetylpiperazine,98% 1-Acetylpiperazine ,99% 1-Acetylpiperazine, 98% 5GR 1-(Piperazin-1-yl)ethan-1-one, 1-Oxo-1-(piperazin-1-yl)ethane 1-Acetylpiperazine 99% N-Acetyl piperazine 1-Acetylpiperazine 1-AcetyL Olaparib Impurity 61 1-Acetylpiperazine > 1-Acetylpiperazine czj Ethanone, 1-(1-piperazinyl)- 1-Acetylpiperazine ISO 9001：2015 REACH 1-acetylpiperazine 13889-98-0 1-ACETYLPIPERAZINE For Synthesis N-ACETYLPIPERAZINE 13889-98-0 13889-88-0 Building Blocks Heterocyclic Building Blocks Piperazines Building Blocks Heterocyclic Building Blocks API intermediates Piperazines Piperaizine Piperidines, Piperidones, Piperazines