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N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE

N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE structure

CAS No.: 2842-44-6

Chemical Name:: N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE

Synonyms: FirstCure MHPT;2-(N-Methyl-p-toluidino);HYDROXYETHYL METHYLTOLUIDINE;Hydroxyethyl methyltolylamine;2-(N-methyl-p-toluidino)ethanol;2-(Methyl(p-tolyl)aMino)ethanol;N-methyl-hydroxyethyl-p-toluidine;2-(N-Methyl-N-4-tolylamino)ethanol;2-(N-methyl-N-p-tolylamino)ethanol;2-(Methyl(p-tolyl)amino)ethan-1-ol

CBNumber:: CB2158428

Molecular Formula:: C10H15NO

Molecular Weight:: 165.23

MDL Number:: MFCD05663421

MOL File:: 2842-44-6.mol

MSDS File:: SDS

Last updated:2023-08-29 17:14:30

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N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE Properties

Boiling point	152-154 °C(Press: 10 Torr)
Density	1.047±0.06 g/cm3(Predicted)
vapor pressure	0.062-0.115Pa at 20-25℃
storage temp.	Sealed in dry,Room Temperature
form	Liquid:viscous
pka	14.69±0.10(Predicted)
LogP	2.2 at 25℃ and pH6
FDA UNII	982J448EHD
EPA Substance Registry System	Ethanol, 2-[methyl(4-methylphenyl)amino]- (2842-44-6)

SAFETY

Risk and Safety Statements

Symbol(GHS)	GHS07
Signal word	Warning
Hazard statements	H302-H315-H319-H335
Precautionary statements	P261-P305+P351+P338
HS Code	2933599590

N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE price

Manufacturer	Product number	Product description	CAS number	Packaging	Price	Updated	Buy
American Custom Chemicals Corporation	CHM0290557	N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE 98.00%	2842-44-6	5MG	$502.35	2021-12-16	Buy
Labseeker	SC-91423	2-(Methyl(p-tolyl)amino)ethanol 95	2842-44-6	1kg	$700	2021-12-16	Buy
Crysdot	CD12088559	2-(Methyl(p-tolyl)amino)ethanol 95+%	2842-44-6	100g	$50	2021-12-16	Buy
Crysdot	CD12088559	2-(Methyl(p-tolyl)amino)ethanol 95+%	2842-44-6	500g	$150	2021-12-16	Buy
Chemenu	CM274824	2-(Methyl(p-tolyl)amino)ethanol 95%	2842-44-6	1000g	$234	2021-12-16	Buy

Product number	Packaging	Price	Buy
CHM0290557	5MG	$502.35	Buy
SC-91423	1kg	$700	Buy
CD12088559	100g	$50	Buy
CD12088559	500g	$150	Buy
CM274824	1000g	$234	Buy

N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE Chemical Properties,Uses,Production

Uses

N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE is an amine organic compound, which can be used as intermediate in organic synthesis.

Synthesis

Add reactant (0.2 mmol, 1.0 equiv), THF (2.0 mL) and CH2Br2 (0.6 mmol, 3.0 equiv) to a flame-dried 10 mL Schlenk tube in a glove box. Seal and take out of the glove box. Cool the reaction mixture to -78°C. Add nBuLi (0.56 mmol, 2.8 equiv) dropwise under N2 atmosphere within 3minutes. Stir the reaction at -78°C for 30 minutes and add ZnCl2 (0.1 mL, 0.5equiv, 1.0 M in Et2O). Allow the mixture to warm to room temperature and stir for 1 hour. Cool the mixture to 0°C. Add a premixture of H2O2 (30% in H2O, 0.5 mL) and NaOH (2.0 M, 1.0 mL). Stir the mixture at room temperature for another 1 hour and dilute with water (20 mL). Extract with DCM (30 mL x 2) and dry over Na2SO4. Filter and concentrate under vacuum. Purify the crude product by silica gel flash column chromatography to obtain product. 1H NMR (CDCl3, 500 MHz) δ 7.08 (d, J = 8.4 Hz, 2H), 6.78 (d, J = 8.4 Hz,2H), 3.80 (t, J = 5.6 Hz, 2H), 3.43 (t, J = 5.4 Hz, 2H), 2.93 (s, 3H), 2.28 (s, 3H), 2.01 (brs, 1H). 13C NMR (CDCl3, 125 MHz) δ 148.3, 129.8, 127.1, 114.0, 60.1, 56.2, 39.1, 20.4.
Fig The synthetic method of N-(2-hydroxyethyl)-N-methyl-4-toluidine

N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE synthesis

Synthesis of N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE from N-METHYL-P-TOLUIDINE

N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE Preparation Products And Raw materials

Raw materials

N-METHYL-P-TOLUIDINE Glycerol 2-Methylaminoethanol 4-Iodotoluene

Preparation Products

N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE Suppliers

Global( 140)Suppliers

Supplier	Tel	Email	Country	ProdList	Advantage
Yancheng Green Chemicals Co.,Ltd	+undefined-86-25-86655873	info@royal-chem.com	China	114	58
Changde Changlian Chemical Co., Ltd.	+86-25-86736270 +86-15905172087	brian.he@royal-chem.com	China	103	58
Hebei Mojin Biotechnology Co., Ltd	+8613288715578	sales@hbmojin.com	China	12453	58
Henan Tianfu Chemical Co.,Ltd.	+86-0371-55170693 +86-19937530512	info@tianfuchem.com	China	21695	55
Hangzhou FandaChem Co.,Ltd.	008657128800458; +8615858145714	fandachem@gmail.com	China	9352	55
Anhui Royal Chemical Co., Ltd.	+86-25-86655873 +8613962173137	marketing@royal-chem.com	China	205	55
Hefei TNJ Chemical Industry Co.,Ltd.	+86-0551-65418679 +86-18949832763	info@tnjchem.com	China	2989	55
Hebei Guanlang Biotechnology Co., Ltd.	+86-19930503282	alice@crovellbio.com	China	8822	58
Xiamen AmoyChem Co., Ltd	+86-592-6051114 +8618959220845	sales@amoychem.com	China	6387	58
Hubei xin bonus chemical co. LTD	86-13657291602	linda@hubeijusheng.com	CHINA	22968	58

Supplier	Advantage
Yancheng Green Chemicals Co.,Ltd	58
Changde Changlian Chemical Co., Ltd.	58
Hebei Mojin Biotechnology Co., Ltd	58
Henan Tianfu Chemical Co.,Ltd.	55
Hangzhou FandaChem Co.,Ltd.	55
Anhui Royal Chemical Co., Ltd.	55
Hefei TNJ Chemical Industry Co.,Ltd.	55
Hebei Guanlang Biotechnology Co., Ltd.	58
Xiamen AmoyChem Co., Ltd	58
Hubei xin bonus chemical co. LTD	58

N-(2-hydroxyethyl)-N-methyl-4-toluidine: Synthesis and Application
N-(2-hydroxyethyl)-N-methyl-4-toluidine is an important intermediate in organic synthesis.
Dec 7，2022

View Lastest Price from N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE manufacturers

Image	Update time	Product	Price	Min. Order	Purity	Supply Ability	Manufacturer
	2023-08-29	N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE 2842-44-6	US $0.00 / KG	1KG	99%	50000KG/month	Hebei Mojin Biotechnology Co., Ltd
	2021-07-31	N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE 2842-44-6	US $10.00 / KG	1KG	99%	10 mt	Hebei Guanlang Biotechnology Co., Ltd.

N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE
2842-44-6
US $0.00 / KG
99%
Hebei Mojin Biotechnology Co., Ltd

N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE
2842-44-6
US $10.00 / KG
99%
Hebei Guanlang Biotechnology Co., Ltd.

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N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE 2-(N-methyl-p-toluidino)ethanol N-Methyl-N-hydroxyethyl-P-toluidine N-(2-Hydroxyethyl)-N-methyl-p-toluidine 2-[Methyl(4-methylphenyl)amino]ethanol 2-(N-Methyl-N-4-tolylamino)ethanol FirstCure MHPT N-Methyl-N-(2-hydroxyethyl)-p-toluidine 2-(Methyl(p-tolyl)aMino)ethanol 2-(N-methyl-N-p-tolylamino)ethanol N-(2-HYDROXYETHYL)-N-METHYL-PARA-TOLUIDINE(MPHT) N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE(MHPT) Hydroxyethyl methyltolylamine (5S,8R,9S,10S,13S,14S,17R)-17-ethynyl-3,3-difluoro-10,13-dimethyl-2,4,5,6,7,8,9,11,12,14,15,16-dodecahydro-1H-cyclopenta[a]phenanthren-17-ol 2-(N-Methyl-p-toluidino) Ethanol, 2-[methyl(4-methylphenyl)amino]- N-methyl-hydroxyethyl-p-toluidine HYDROXYETHYL METHYLTOLUIDINE 2842-44-6 N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE 2-(Methyl(p-tolyl)amino)ethan-1-ol 2842-44-6 42-44-6