2-Methyl-2-nitropropan-1-ol
- CAS No.
- 76-39-1
- Chemical Name:
- 2-Methyl-2-nitropropan-1-ol
- Synonyms
- 1-Propanol, 2-methyl-2-nitro-;2-Methyl-2-nitropropanol;2-methyl-2-nitro-1-propano;2-METHYL-2-NITRO-1-PROPANOL;2-NITRO-2-METHYL-1-PROPANOL;2-NITROISOBUTANOL;Methylnitropropanol;methyl-2nitro-2propanol;2-Nitro-2-methylpropanol;2-methyl-2-nitropropan-1-ol
- CBNumber:
- CB3474945
- Molecular Formula:
- C4H9NO3
- Molecular Weight:
- 119.12
- MDL Number:
- MFCD00007394
- MOL File:
- 76-39-1.mol
- MSDS File:
- SDS
| Melting point | 86-89 °C(lit.) |
|---|---|
| Boiling point | 94-95 °C10 mm Hg(lit.) |
| Density | 1.0765 (estimate) |
| refractive index | 1.4413 (estimate) |
| pka | 13.79±0.10(Predicted) |
| InChI | InChI=1S/C4H9NO3/c1-4(2,3-6)5(7)8/h6H,3H2,1-2H3 |
| InChIKey | MVGJRISPEUZYAQ-UHFFFAOYSA-N |
| SMILES | C(O)C(C)([N+]([O-])=O)C |
| EWG's Food Scores | 1 |
| FDA UNII | RGG97AOX42 |
| NIST Chemistry Reference | 1-Propanol, 2-methyl-2-nitro-(76-39-1) |
| EPA Substance Registry System | 1-Propanol, 2-methyl-2-nitro- (76-39-1) |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302-H319 |
| Precautionary statements | P264-P270-P301+P312-P330-P501-P264-P280-P305+P351+P338-P337+P313P |
| WGK Germany | 3 |
| RTECS | UB8575000 |
2-Methyl-2-nitropropan-1-ol price More Price(7)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| AK Scientific | 0231BA | 2-Methyl-2-nitro-1-propanol | 76-39-1 | 250mg | $181 | 2021-12-16 | Buy |
| Matrix Scientific | 159675 | 2-Methyl-2-nitropropan-1-ol | 76-39-1 | 0.500g | $240 | 2021-12-16 | Buy |
| Matrix Scientific | 159675 | 2-Methyl-2-nitropropan-1-ol | 76-39-1 | 1g | $300 | 2021-12-16 | Buy |
| American Custom Chemicals Corporation | CHM0009071 | 2-METHYL-2-NITRO-1-PROPANOL 95.00% | 76-39-1 | 5MG | $499.28 | 2021-12-16 | Buy |
| Matrix Scientific | 159675 | 2-Methyl-2-nitropropan-1-ol | 76-39-1 | 5g | $1000 | 2021-12-16 | Buy |
2-Methyl-2-nitropropan-1-ol Chemical Properties,Uses,Production
Uses
The direct hydrogenation of 2-Methyl-2-nitropropan-1-ol obtains product 2-amino-2-methyl-1-propanol (AMP-95). AMP-95 is a kind of multifunction additive being widely known by the people, be widely used in coating and printing ink, metal working fluid, in the industries such as personal nursing and medicine intermediate.
Synthesis
By catalyst 10g (Ti-V-ZSM-5), acetone 58.08g, ammonium hydroxide 20g are
added in 400ml methanol, are warming up to 70
DEG C, hydrogen peroxide (35%) 226.7g is slowly added dropwise,
temperature is maintained to react 1h at 65-75 DEG C, obtain 2- nitros
third after being added dropwise
Alkane reaction solution；Filtering adds in 5g sodium hydroxides to
reaction solution, is warming up to 35 DEG C, formaldehyde (40% aqueous
solution) is added dropwise, drip with
the reaction was continued afterwards 3h, obtains 2-Methyl-2-nitropropan-1-ol.
Purification Methods
Distil it under vacuum and/or crystallise it from pet ether or MeOH. [Astle & Abbott J Org Chem 21 1229 1956, Kambe & Yasuda Bull Soc Chem Jpn 41 1444 1968, Beilstein 1 H 378, 1 III 1546, 1 IV 1604.]
2-Methyl-2-nitropropan-1-ol Preparation Products And Raw materials
Raw materials
Preparation Products
2-Methyl-2-nitropropan-1-ol Suppliers
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Beijing Risun Science and Technology Limited | +8619801193650 | xykj@risun.com | China | 13 | 58 |
| CONIER CHEM AND PHARMA LIMITED | +8618523575427 | sales@conier.com | China | 47465 | 58 |
| Alfa Chemistry | info@alfa-chemistry.com | United States | 2344 | 58 | |
| Aston Chemical | 13000000000 | sales@astonchem.com | United States | 1634 | 58 |
| Dayang Chem (Hangzhou) Co.,Ltd. | 571-88938639 +8617705817739 | info@dycnchem.com | CHINA | 52867 | 58 |
| Henan Alfa Chemical Co., Ltd | +8618339805032 | alfa4@alfachem.cn | China | 12756 | 58 |
| PT CHEM GROUP LIMITED | +86-85511178 +86-85511178 | peter68@ptchemgroup.com | China | 35453 | 58 |
| LEAPCHEM CO., LTD. | +86-852-30606658 | market18@leapchem.com | China | 43348 | 58 |
| Aladdin Scientific | +1-833-552-7181 | sales@aladdinsci.com | United States | 57511 | 58 |
| RISUN Technology Co., Ltd | 010-63781398 15175743701 | xykj@risun.com | China | 12 | 58 |
View Lastest Price from 2-Methyl-2-nitropropan-1-ol manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
 |
2022-05-23 | 2-Methyl-2-nitropropan-1-ol
76-39-1
|
US $0.00 / kg | 180kg | 98% GC | 20 tons | Beijing Risun Science and Technology Limited |
-
- 2-Methyl-2-nitropropan-1-ol
76-39-1
- US $0.00 / kg
- 98% GC
- Beijing Risun Science and Technology Limited
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