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3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDE

CAS No.
24422-15-9
Chemical Name:
3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDE
Synonyms
Rivaroxaban Impurity 166;trichlorothiophene-2-carbonyl chloride;3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDE;3,4,5-trichloro-2-thiophenecarbonyl chloride;2-Thiophenecarbonyl chloride, 3,4,5-trichloro-;3,4,5-Trichlorothien-2-carboxylic acid chloride
CBNumber:
CB3482535
Molecular Formula:
C5Cl4OS
Molecular Weight:
249.93
MDL Number:
MFCD02093952
MOL File:
24422-15-9.mol
Last updated:2023-05-26 13:35:54

3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDE Properties

Melting point 38-40°C
Boiling point 124-125°C 10mm
Flash point 124-125°C/10mm
Sensitive Moisture Sensitive
BRN 1427060

SAFETY

Risk and Safety Statements

Symbol(GHS)  GHS hazard pictograms
GHS05
Signal word  Warning
Hazard statements  H314-H318
Precautionary statements  P260h-P301+P330+P331-P303+P361+P353-P305+P351+P338-P405-P501a
Risk Statements  34
Safety Statements  26-36/37/39-45
RIDADR  3261
HazardClass  8
PackingGroup  II
NFPA 704
1
3 0

3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDE price More Price(3)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Alfa Aesar L17704 3,4,5-Trichlorothiophene-2-carbonyl chloride, 97% 24422-15-9 1g $38.9 2021-12-16 Buy
Alfa Aesar L17704 3,4,5-Trichlorothiophene-2-carbonyl chloride, 97% 24422-15-9 5g $118 2021-12-16 Buy
AHH MT-36791 3,4,5-Trichlorothiophene-2-carbonylchloride 97% 24422-15-9 25g $300 2021-12-16 Buy
Product number Packaging Price Buy
L17704 1g $38.9 Buy
L17704 5g $118 Buy
MT-36791 25g $300 Buy

3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDE Chemical Properties,Uses,Production

Preparation

3,4,5-Trichlorothiophene-2-carbonyl chloride synthesis: A mixture of 3,4,5-trichloro-2-thiophenecarboxylic acid (20.4 g, 0.088 mol), SOCl2 (7.3 mL, 0.1 mol), and DMF (0.2 mL) in 80 mL of 1,2-dichloroethane was heated at reflux temperature for 3 h. The reaction mixture became homogeneous after 1 h of heating. The solution was cooled to 25℃, concentrated and placed under high vacuum to remove residual solvent, giving 22.0 g (98% wt.) of 3,4,5-trichloro-2-thiophenecarbonyl chloride as an oil which solidified on standing to an off-white powder; m.p. 37-41℃, having a GC area % purity > 99%.

26020-48-4
107-06-2
24422-15-9
Synthesis of 3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDE from 3,4,5-TRICHLOROTHIOPHENE-2-CARBOXYLIC ACID and 1,2-Dichloroethane

3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDE Preparation Products And Raw materials

Raw materials

Preparation Products

3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDE Suppliers

Global( 24)Suppliers
Supplier Tel Email Country ProdList Advantage
CONIER CHEM AND PHARMA LIMITED
+8618523575427 sales@conier.com China 47465 58
LEAPCHEM CO., LTD.
+86-852-30606658 market18@leapchem.com China 43348 58
Amadis Chemical Company Limited
571-89925085 sales@amadischem.com China 131981 58
Meryer (Shanghai) Chemical Technology Co., Ltd. 4006608290; 18621169109 market03@meryer.com China 40241 62
Alfa Aesar 400-6106006 saleschina@alfa-asia.com China 30132 84
Energy Chemical 021-021-58432009 400-005-6266 sales8178@energy-chemical.com China 44751 61
Shanghai Nuohey Chemical Co., Ltd. 021-52212593 13761626812 sales@nuohey.com China 10692 60
Aikon International Limited 025-58851090 13611564524 lwan@aikonchem.com China 15952 58
Hubei Qingbei Yunyan Pharmaceutical Technology Co., Ltd 18162595016 3287908757@qq.com China 9512 58
3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDE 3,4,5-Trichlorothien-2-carboxylic acid chloride 3,4,5-trichloro-2-thiophenecarbonyl chloride 2-Thiophenecarbonyl chloride, 3,4,5-trichloro- Rivaroxaban Impurity 166 trichlorothiophene-2-carbonyl chloride 24422-15-9 C5Cl4OS