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(10-Phenyl-9-anthracenyl)boronic acid pinacol ester

CAS No.
460347-59-5
Chemical Name:
(10-Phenyl-9-anthracenyl)boronic acid pinacol ester
Synonyms
10-Phenylanthracene-9-boronic Acid Pinacol Ester;(10-Phenyl-9-anthracenyl)boronic acid pinacol ester;9-Phenyl-10-anthracen(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl);9-Phenyl-10-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)anthracene;4,4,5,5-Tetramethyl-2-(10-phenyl-9-anthracenyl)-1,3,2-dioxaborolane;4,4,5,5-Tetramethyl-2-(10-Phenylanthracen-9-Yl)-1,3,2-Dioxaborolane;4,4,5,5-tetramethyl-2-(9-phenylanthracen-10-yl)-1,3,2-dioxaborolane;9-(4,4,5,5-Tetramethyl-[1,3,2]dioxaborolan-2-yl)-10-phenylanthracene;1,3,2-Dioxaborolane, 4,4,5,5-tetramethyl-2-(10-phenyl-9-anthracenyl)-
CBNumber:
CB52462210
Molecular Formula:
C26H25BO2
Molecular Weight:
380.29
MDL Number:
MFCD13194955
MOL File:
460347-59-5.mol
MSDS File:
SDS
Last updated:2023-06-08 17:06:35

(10-Phenyl-9-anthracenyl)boronic acid pinacol ester Properties

Melting point 165.0 to 169.0 °C
Boiling point 524.1±19.0 °C(Predicted)
Density 1.15
form powder to crystal
color White to Light yellow

SAFETY

Risk and Safety Statements

Symbol(GHS)  GHS hazard pictograms
GHS07
Signal word  Warning
Hazard statements  H302-H315-H319-H335
Precautionary statements  P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501
HS Code  2931.90.6000

(10-Phenyl-9-anthracenyl)boronic acid pinacol ester price More Price(11)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
TCI Chemical T3665 4,4,5,5-Tetramethyl-2-(10-phenylanthracen-9-yl)-1,3,2-dioxaborolane >98.0%(GC) 460347-59-5 1g $43 2024-03-01 Buy
TCI Chemical T3665 4,4,5,5-Tetramethyl-2-(10-phenylanthracen-9-yl)-1,3,2-dioxaborolane >98.0%(GC) 460347-59-5 5g $173 2024-03-01 Buy
TRC T889730 4,4,5,5-Tetramethyl-2-(10-phenylanthracen-9-yl)-1,3,2-dioxaborolane 460347-59-5 100mg $75 2021-12-16 Buy
Chem-Impex 40044 4,4,5,5-Tetramethyl-2-(10-phenylanthracen-9-yl)-1,3,2-dioxaborolane,98%(GC) 98%(GC) 460347-59-5 1G $236.32 2021-12-16 Buy
Chem-Impex 40044 4,4,5,5-Tetramethyl-2-(10-phenylanthracen-9-yl)-1,3,2-dioxaborolane,≥98%(GC) ≥98%(GC) 460347-59-5 5G $830.5 2021-12-16 Buy
Product number Packaging Price Buy
T3665 1g $43 Buy
T3665 5g $173 Buy
T889730 100mg $75 Buy
40044 1G $236.32 Buy
40044 5G $830.5 Buy

(10-Phenyl-9-anthracenyl)boronic acid pinacol ester Chemical Properties,Uses,Production

Preparation

9-Bromo-10-phenylanthracene (5.8g, 17.4mmol), bis(pinacolato)diboron(6.63 g, 26.1 mmol), Pd(dppf)Cl2 (710 mg, 0.87 mmol), and KOAc (10.23 g, 104.4 mmol) were mixed in a 250mL flask containing 1,4-dioxane (60 mL). The reaction mixture was refluxed for 24h under nitrogen. After it was cooled to room temperature, a dilute hydrochloric acid solution quenched. The mixture was extracted with CH2Cl2 and dried over anhydrous MgSO4. The crude product was concentrated by rotary evaporation and further purified by silica gel column chromatography (CH2Cl2 / petroleum ether (1:1,v/v)) to afford a light yellow powder (4.0 g, 60.4 %). 1H NMR (500 MHz, CDCl3) δ 8.46 (d, J = 8.7 Hz, 2H), 7.65 (d, J = 8.8 Hz, 2H), 7.57 (dq, J = 14.2, 7.0 Hz, 3H), 7.51 – 7.46 (m, 2H), 7.41 (d, J = 7.0 Hz, 2H), 7.34 (dd, J = 8.1, 7.1 Hz, 2H), 1.63 (s, 12H). EI-MS (m/z): Calculated for C26H25BO2: 380.29. Found [M+]: 379.92.
preparation of 4,4,5,5-Tetramethyl-2-(10-phenylanthracen-9-yl)-1,3,2-dioxaborolane
Synthesis of 4,4,5,5-Tetramethyl-2-(10-phenylanthracen-9-yl)-1,3,2-dioxaborolane

(10-Phenyl-9-anthracenyl)boronic acid pinacol ester Preparation Products And Raw materials

Raw materials

Preparation Products

Global( 53)Suppliers
Supplier Tel Email Country ProdList Advantage
Shanghai Daken Advanced Materials Co.,Ltd
+86-371-66670886 info@dakenam.com China 15928 58
ATK CHEMICAL COMPANY LIMITED
+undefined-21-51877795 ivan@atkchemical.com China 32480 60
SHAANXI WEISHINUO THE NEW MATERIALCO,.LTD
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BAYNOE CHEM CO.,LTD
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career henan chemical co
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Richest Group Ltd
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CD Chemical Group Limited
+8615986615575 info@codchem.com China 20356 58
Hefei TNJ Chemical Industry Co.,Ltd.
0551-65418684 +8618949823763 sales@tnjchem.com China 25363 58
Hangzhou MolCore BioPharmatech Co.,Ltd.
+86-057181025280; +8617767106207 sales@molcore.com China 49739 58
Shaoxin Catsyn Co., Ltd.
+undefined-0575-82040869 +86-0575-82040869; sales@catsyn.com China 6116 58

View Lastest Price from (10-Phenyl-9-anthracenyl)boronic acid pinacol ester manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
4,4,5,5-tetramethyl-2-(9-phenylanthracen-10-yl)-1,3,2-dioxaborolane pictures 2024-01-23 4,4,5,5-tetramethyl-2-(9-phenylanthracen-10-yl)-1,3,2-dioxaborolane
460347-59-5
US $0.00 / KG 1KG 98.00% 150KG /month Shanghai Daken Advanced Materials Co.,Ltd
(10-Phenyl-9-anthracenyl)boronic acid pinacol ester pictures 2020-01-10 (10-Phenyl-9-anthracenyl)boronic acid pinacol ester
460347-59-5
US $1.00 / KG 1KG 98% HPLC 10 tons/month Career Henan Chemical Co
(10-Phenyl-9-anthracenyl)boronic acid pinacol ester 4,4,5,5-Tetramethyl-2-(10-phenyl-9-anthracenyl)-1,3,2-dioxaborolane 9-(4,4,5,5-Tetramethyl-[1,3,2]dioxaborolan-2-yl)-10-phenylanthracene 4,4,5,5-tetramethyl-2-(9-phenylanthracen-10-yl)-1,3,2-dioxaborolane 4,4,5,5-Tetramethyl-2-(10-Phenylanthracen-9-Yl)-1,3,2-Dioxaborolane 1,3,2-Dioxaborolane, 4,4,5,5-tetramethyl-2-(10-phenyl-9-anthracenyl)- 10-Phenylanthracene-9-boronic Acid Pinacol Ester 9-Phenyl-10-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)anthracene 9-Phenyl-10-anthracen(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl) 460347-59-5 C26H25BO2