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1-Methyl-3-pyrrolidinol

1-Methyl-3-pyrrolidinol structure

CAS No.: 13220-33-2

Chemical Name:: 1-Methyl-3-pyrrolidinol

Synonyms: 1-METHYL-PYRROLIDIN-3-OL;3-HYDROXY-1-METHYLPYRROLIDINE;NSC 89279;3-Hydroxy-1-methyL;N-Methyl-3-hydroxy-;1-Methyl-3-pyrrolidi;N-methyl-3-pyrrolitol;N-Methyl-3-pyrrolidinol;1-METHYL-3-PYRROLIDINOL;N-Methyl-pyrrolidin-3-ol

CBNumber:: CB9296691

Molecular Formula:: C5H11NO

Molecular Weight:: 101.15

MDL Number:: MFCD00003176

MOL File:: 13220-33-2.mol

MSDS File:: SDS

Last updated:2023-12-20 20:39:53

Request For Quotation

1-Methyl-3-pyrrolidinol Properties

Boiling point	50-52 °C1 mm Hg(lit.)
Density	0.921 g/mL at 25 °C(lit.)
refractive index	n20/D 1.464(lit.)
Flash point	159 °F
storage temp.	2-8°C
solubility	Chloroform (Slightly), Methanol (Slightly)
form	Oil
pka	14.95±0.20(Predicted)
color	Colourless
InChI	InChI=1S/C5H11NO/c1-6-3-2-5(7)4-6/h5,7H,2-4H2,1H3
InChIKey	FLVFPAIGVBQGET-UHFFFAOYSA-N
SMILES	N1(C)CCC(O)C1
CAS DataBase Reference	13220-33-2(CAS DataBase Reference)
FDA UNII	CGW2AL7PQ7
NIST Chemistry Reference	1-Methyl-3-pyrrolidinol(13220-33-2)

SAFETY

Risk and Safety Statements

Symbol(GHS)

GHS07

Signal word

Warning

Hazard statements

H227-H315-H319-H335

Precautionary statements

P210e-P261-P280a-P305+P351+P338-P405-P501a

Hazard Codes

Risk Statements

36/37/38

Safety Statements

26-36/37/39

WGK Germany

HS Code

29339900

NFPA 704

	2
2		0

1-Methyl-3-pyrrolidinol price More Price(35)

Manufacturer	Product number	Product description	CAS number	Packaging	Price	Updated	Buy
Sigma-Aldrich	M79506	1-Methyl-3-pyrrolidinol 95%	13220-33-2	1g	$41.7	2024-03-01	Buy
TCI Chemical	M2115	1-Methyl-3-pyrrolidinol	13220-33-2	5G	$100	2024-03-01	Buy
TCI Chemical	M2115	1-Methyl-3-pyrrolidinol	13220-33-2	25G	$347	2024-03-01	Buy
Alfa Aesar	H28122	3-Hydroxy-1-methylpyrrolidine, 97%	13220-33-2	1g	$93.9	2023-06-20	Buy
Alfa Aesar	H28122	3-Hydroxy-1-methylpyrrolidine, 97%	13220-33-2	5g	$307	2023-06-20	Buy

Product number	Packaging	Price	Buy
M79506	1g	$41.7	Buy
M2115	5G	$100	Buy
M2115	25G	$347	Buy
H28122	1g	$93.9	Buy
H28122	5g	$307	Buy

1-Methyl-3-pyrrolidinol Chemical Properties,Uses,Production

Chemical Properties

Clear colorless to pale yellow liquid

Uses

1-Methyl-3-pyrrolidinol (cas# 13220-33-2) is a compound useful in organic synthesis.

Synthesis

A 500 mL four-necked flask was charged with a 40 wt% aqueous solution of monomethylamine and cooled to 10 ° C in an ice-water bath. Then, while stirring, 1,4-dichloro-2-butanol was added dropwise, and the temperature was controlled at 15 ° C. Then pour the system into an Autoclave, sealed, evacuated to a pressure of 1.0 ± 0.1MPa, while heated to 120 ℃, the reaction was stirred for about 10h. After the reaction was over and cooled to room temperature, the material was discharged, batch-wise added sodium hydroxide was released, and a large amount of methylamine gas, controlling the temperature below 50 ℃, precipitated a lot of white solid, stirred for 1h; filtration, the filtrate layered, the upper organic phase Ethanol And anhydrous magnesium sulfate, stirring 2 ~ 3h; and then filtered, the filtrate was concentrated in vacuo to give a yellow transparent oily liquid, and then vacuum distillation to give colorless and t1-Methyl-3-pyrrolidinol, Yield 64.8%, purity 99.3%.

1-Methyl-3-pyrrolidinol synthesis

Synthesis of 1-Methyl-3-pyrrolidinol from 1,4-DICHLORO-2-BUTANOL and Methylamine

1-Methyl-3-pyrrolidinol Preparation Products And Raw materials

Raw materials

Solid sodium hydroxide Methylamine 1,4-DICHLORO-2-BUTANOL 2-Butanol, 1,4-bis(methylamino)- 1,4-DIBROMO-2-BUTANOL

1H-Pyrrole, 2,5-dihydro-1-methyl- 1-N-Ethoxycarbonyl-3-pyrrolidone 3-Pyrrolidinol

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Preparation Products

1-Methyl-3-pyrrolidinol Suppliers

Global( 337)Suppliers

Supplier	Tel	Email	Country	ProdList	Advantage
Anhui Dexinjia Biopharm Co., Ltd	+86-531-82375818 +86-15064153060	alice@jndxj.com	China	309	58
Hebei Mojin Biotechnology Co., Ltd	+8613288715578	sales@hbmojin.com	China	12457	58
Zibo Hangyu Biotechnology Development Co., Ltd	+86-0533-2185556 +8617865335152	Mandy@hangyubiotech.com	China	11013	58
Capot Chemical Co.,Ltd.	571-85586718 +8613336195806	sales@capotchem.com	China	29797	60
Shanghai Daken Advanced Materials Co.,Ltd	+86-371-66670886	info@dakenam.com	China	15928	58
Beijing Cooperate Pharmaceutical Co.,Ltd	010-60279497	sales01@cooperate-pharm.com	CHINA	1811	55
Henan Tianfu Chemical Co.,Ltd.	+86-0371-55170693 +86-19937530512	info@tianfuchem.com	China	21695	55
career henan chemical co	+86-0371-86658258	sales@coreychem.com	China	29914	58
Zhejiang ZETian Fine Chemicals Co. LTD	18957127338	stella@zetchem.com	China	2141	58
Accela ChemBio Inc.	(+1)-858-699-3322	info@accelachem.com	United States	19965	58

Supplier	Advantage
Anhui Dexinjia Biopharm Co., Ltd	58
Hebei Mojin Biotechnology Co., Ltd	58
Zibo Hangyu Biotechnology Development Co., Ltd	58
Capot Chemical Co.,Ltd.	60
Shanghai Daken Advanced Materials Co.,Ltd	58
Beijing Cooperate Pharmaceutical Co.,Ltd	55
Henan Tianfu Chemical Co.,Ltd.	55
career henan chemical co	58
Zhejiang ZETian Fine Chemicals Co. LTD	58
Accela ChemBio Inc.	58

View Lastest Price from 1-Methyl-3-pyrrolidinol manufacturers

Update time	Product	Price	Min. Order	Purity	Supply Ability	Manufacturer
2024-04-24	1-Methyl-3-pyrrolidinol 13220-33-2	US $3360.00-3310.00 / kg	200kg	99.99%	100Tons	Hebei Dangtong Import and export Co LTD
2024-04-24	1-Methyl-3-pyrrolidinol 13220-33-2	US $200.00-4000.00 / KG	100g	no less than 98%	1MT per month	Anhui Dexinjia Biopharm Co., Ltd
2024-03-28	1-Methyl-3-pyrrolidinol 13220-33-2	US $0.00 / kg	25kg	≥98%	Inquiry	PNP Biotech Co. Ltd

1-Methyl-3-pyrrolidinol
13220-33-2
US $3360.00-3310.00 / kg
99.99%
Hebei Dangtong Import and export Co LTD

1-Methyl-3-pyrrolidinol
13220-33-2
US $200.00-4000.00 / KG
no less than 98%
Anhui Dexinjia Biopharm Co., Ltd

1-Methyl-3-pyrrolidinol
13220-33-2
US $0.00 / kg
≥98%
PNP Biotech Co. Ltd

1-Methyl-3-pyrrolidinol Spectrum

1-Methyl-3-pyrrolidinol(13220-33-2)MS 1-Methyl-3-pyrrolidinol(13220-33-2)¹HNMR 1-Methyl-3-pyrrolidinol(13220-33-2)¹³CNMR 1-Methyl-3-pyrrolidinol(13220-33-2)IR1 1-Methyl-3-pyrrolidinol(13220-33-2)Raman

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