3-ブロモ安息香酸
| メーカー |
製品番号 |
製品説明 |
CAS番号 |
包装 |
価格 |
更新時間 |
購入 |
|
富士フイルム和光純薬株式会社(wako)
|
W01AFAA12606 |
3-ブロモ安息香酸
3-Bromobenzoic Acid |
585-76-2 |
25g |
￥13430 |
2024-03-01 |
購入 |
|
富士フイルム和光純薬株式会社(wako)
|
W01AFAA12606 |
3-ブロモ安息香酸
3-Bromobenzoic Acid |
585-76-2 |
100g |
￥36590 |
2024-03-01 |
購入 |
|
東京化成工業
|
B0551 |
3-ブロモ安息香酸 >98.0%(GC)(T)
3-Bromobenzoic Acid
>98.0%(GC)(T) |
585-76-2 |
25g |
￥8400 |
2024-03-01 |
購入 |
|
東京化成工業
|
B0551 |
3-ブロモ安息香酸 >98.0%(GC)(T)
3-Bromobenzoic Acid
>98.0%(GC)(T) |
585-76-2 |
250g |
￥45800 |
2024-03-01 |
購入 |
|
関東化学株式会社(KANTO)
|
18135-2A |
３‐ブロモ安息香酸 99%
3‐Bromobenzoic acid 99% |
585-76-2 |
5g |
￥2800 |
2024-03-01 |
購入 |
3-ブロモ安息香酸 化学特性,用途語,生産方法
外観
白色～うすい黄色、結晶性粉末～粉末
使用上の注意
アルゴン封入
化学的特性
white to light yellow crystal powder. soluble in alcohols and ethers, insoluble in water.Used as organic synthesis reagent.
使用
3-Bromobenzoic acid was used as test solute in the determination of acidity constants by capillary zone electrophoresis. It was used as internal standard to study the retention mechanisms of an unmodified and a hydroxylated polystyrene-divinylbenzene polymer by solid-phase extraction. It was also used in synthesis of N-(1,1-dimethyl-2-hydroxyethyl)-3-bromobenzamide.
製造方法
3-Bromobenzoic acid is synthesized from 3-bromotoluene by oxidation of potassium permanganate. Mix m-bromotoluene, potassium hydroxide and water, heat to boiling, slowly add potassium permanganate, and reflux for 4 hours after adding. After acidification by filtration, the crude product was obtained by filtration. Then it is dissolved in ethanol with ammonia water, acidified with hydrochloric acid, filtered and washed with water to obtain 3-bromobenzoic acid.
純化方法
Crystallise the acid from acetone/water, MeOH or acetic acid. The anilide has m 137o (from EtOH/H2O). [Beilstein 9 IV 1013.]
3-ブロモ安息香酸 上流と下流の製品情報
原材料
準備製品
3-ブロモ安息香酸 生産企業
Global( 415)Suppliers
3-ブロモ安息香酸 スペクトルデータ(1HNMR、IR1、IR2、IR3、MS、Raman)
585-76-2(3-ブロモ安息香酸)キーワード:
- 585-76-2
- 3-BromobenzoicAcid99%
- 3-BROMO BENZOIC ACID FOR SYNTHESIS
- 3-Bromobenzoicacid,98+%
- Brombenzoesaure
- 3-BroMobenzoic aicd
- 3-BroMobenzoic acid, 99% 25GR
- 3-BroMobenzoic acid, 99% 5GR
- Benzoic acid, M-broMo- (8CI)
- NSC 83519
- BroMine between benzoic acid
- M-BROMOBENZOIC ACID
- M-CARBOXYBENZYL BROMIDE
- 3-Bromo-Benzoic Acid and tert-Butyl Ester
- 3-BROMOBENZOIC ACID
- 3-BROMBENZOIC ACID
- RARECHEM AL BO 0037
- 3-bromo-benzoicaci
- Benzoic acid, m-bromo-
- m-Bromobenzoic Acid 3-Bromobenzoic Acid
- Benzoicacid,3-bromo-
- Brombenzoicacid
- 3-Bromobenzene carboxylic acid
- 3-Bromobenzoic Acid >
- QVR CE
- TIANFUCHEM--High purity 3-Bromobenzoic acid factory price
- 3-Bromobenzoic Acid extrapure, 99%
- 3-Bromobenzoic acid CAS NO.585-76-2
- 3-ブロモ安息香酸
- m-ブロモ安息香酸
- 3ブロモ安息香酸
- 3-ブロモ安息香酸 臭化物
- 3‐ブロモ安息香酸