- Diisopropyl phosphite
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- $0.00 / 1KG
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2022-10-20
- CAS:1809-20-7
- Min. Order: 1KG
- Purity: 98%
- Supply Ability: 1ton
- Diisopropyl phosphite
-
- $15.00 / 1KG
-
2021-07-02
- CAS:1809-20-7
- Min. Order: 1KG
- Purity: 99%+ HPLC
- Supply Ability: Monthly supply of 1 ton
- Diisopropyl phosphite
-
- $1.00 / 1KG
-
2020-03-16
- CAS:1809-20-7
- Min. Order: 1KG
- Purity: 99%
- Supply Ability: 200000KG
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| | Diisopropyl phosphite Basic information |
| | Diisopropyl phosphite Chemical Properties |
| Hazard Codes | Xn | | Risk Statements | 36/37/38-22 | | Safety Statements | 37/39-26 | | RIDADR | 3265 | | RTECS | SZ7660000 | | TSCA | Yes | | HS Code | 29209085 | | Toxicity | guinea pig,LC50,inhalation,9010mg/m3 (9010mg/m3),LUNGS, THORAX, OR RESPIRATION: OTHER CHANGESGASTROINTESTINAL: CHANGES IN STRUCTURE OR FUNCTION OF SALIVARY GLANDSBEHAVIORAL: CONVULSIONS OR EFFECT ON SEIZURE THRESHOLD,Gigiena Truda i Professional'nye Zabolevaniya. Labor Hygiene and Occupational Diseases. Vol. 29(11), Pg. 51, 1985. |
| | Diisopropyl phosphite Usage And Synthesis |
| Chemical Properties | clear colourless liquid, corrosive, soluble in organic solvents such as ethanol. | | Uses | Diisopropyl phosphite is used as antiwear lubricant additive together with triphenyl thiophosphate on T8 steel/Al2O3 ceramics. | | Preparation | Diisopropyl phosphite is prepared by directly reacting isopropanol with phosphorus trichloride.
3(CH3)2CHOH+PCl3→[(CH3)2CHO]2POH+2HCl↑+(CH3)2CHCl
At a ratio of 3:1 (mol), continuously feed 215kg/h of isopropanol and 150kg/h of phosphorus trichloride. When mixed, this results in a violent reaction that generates hydrogen chloride gas. This gas is quickly removed from the mixing pot using vacuum mercury. The crude ester produced is then heated in a falling film type spinner deacidification device and further deacidified. The resulting product is then cooled to below 40°C and obtained with a content of 92%-95% and a yield of 95%～98%. | | Synthesis Reference(s) | Tetrahedron Letters, 29, p. 3327, 1988 DOI: 10.1016/0040-4039(88)85153-0 |
| | Diisopropyl phosphite Preparation Products And Raw materials |
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