N-Phenylbenzylamine

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Products Intro: Product Name:n-benzylaniline
CAS:103-32-2
Purity:99.9% Package:1Kg;|5Kg;|25Kg
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Products Intro: Product Name:N-benzylaniline
CAS:103-32-2
Purity:98% (Min.) Package:1G;1KG;100KG
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Products Intro: Product Name:N-Benzylaniline;N-Phenylbenzylamine
CAS:103-32-2
Purity:AS COA Package:As your request Remarks:103-32-2
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Products Intro: Product Name:N-Phenylbenzylamine
CAS: 103-32-2
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Products Intro: Product Name:N-Phenylbenzylamine
CAS:103-32-2
Package:200kg drum

N-Phenylbenzylamine manufacturers

  • n-benzylaniline
  • n-benzylaniline pictures
  • $0.00 / 1Kg
  • 2024-03-28
  • CAS:103-32-2
  • Min. Order: 1Kg
  • Purity: 99.9%
  • Supply Ability: 200tons
  • N-Phenylbenzylamine
  • N-Phenylbenzylamine pictures
  • $7.00 / 1KG
  • 2019-07-06
  • CAS: 103-32-2
  • Min. Order: 1KG
  • Purity: 99%
  • Supply Ability: 100KG
N-Phenylbenzylamine Basic information
Synthesis
Product Name:N-Phenylbenzylamine
Synonyms:PHENYLACETIC ACID CHLORIDE;N-PHENYLBENZYLAMINE;LABOTEST-BB LT00852555;LABOTEST-BB LT00643802;A-TOLUYL CHLORIDE;AURORA 4803;AKOS BBS-00003909;N-PHENYLBENZYLAMINE, 99+%
CAS:103-32-2
MF:C13H13N
MW:183.25
EINECS:203-100-4
Product Categories:Amines, Aromatics, Metabolites & Impurities
Mol File:103-32-2.mol
N-Phenylbenzylamine Structure
N-Phenylbenzylamine Chemical Properties
Melting point 35-38 °C (lit.)
Boiling point 306-307 °C (lit.)
density 1.061 g/mL at 25 °C (lit.)
refractive index n20/D 1.5325(lit.)
Fp 217 °F
storage temp. Store below +30°C.
solubility alcohol: soluble
form Crystalline Powder or Low Melting Mass
pka3.89±0.10(Predicted)
Specific Gravity1.061
color Colorless to yellow-beige
Water Solubility INSOLUBLE
Merck 14,1126
CAS DataBase Reference103-32-2(CAS DataBase Reference)
NIST Chemistry ReferenceBenzenemethanamine, N-phenyl-(103-32-2)
EPA Substance Registry SystemBenzenemethanamine, N-phenyl- (103-32-2)
Safety Information
Hazard Codes C,Xi
Risk Statements 36/37/38
Safety Statements 26-37/39
RIDADR UN 2577 8/PG 2
WGK Germany 3
21
HS Code 29214980
MSDS Information
ProviderLanguage
Benzylaniline English
SigmaAldrich English
ACROS English
ALFA English
N-Phenylbenzylamine Usage And Synthesis
SynthesisN-Phenylbenzylamine can be obtained by condensation of benzyl chloride and aniline. Mix and stir sodium bicarbonate, water and aniline, heat to 90-95°C, and slowly add benzyl chloride. React at 90-95°C for 3h. Cool and filter. The filtrate was separated, and the organic layer was washed with saturated brine and dried over anhydrous sodium sulfate. Then, under reduced pressure distillation, the 81°C (1.6kPa) fraction was collected to recover aniline, and the 170-190°C (1.6kPa) fraction was cooled and solidified to give N-Phenylbenzylamine.
Chemical Propertiescolorless to yellow-beige crystalline powder
UsesN-Benzylaniline is a major metabolite of the antihistaminic Antazoline and other N-substituted benzylanilines.
UsesN-Benzylaniline was used in the separation of tervalent gallium, indium and thallium by solvent extraction method.
Synthesis Reference(s)Chemistry Letters, 8, p. 45, 1979
Organic Syntheses, Coll. Vol. 1, p. 102, 1941
Tetrahedron Letters, 19, p. 4987, 1978 DOI: 10.1016/S0040-4039(01)85789-0
General DescriptionThe electropolymerisation of N-benzylaniline at transparent Indium Tin Oxide glass electrodes has been investigated by UV-visible spectroelectrochemistry. N-Benzylaniline on electrochemical oxidation in aqueous sulfuric acid solution produces an adherent conducting polymer film at the platinum electrode.
Purification MethodsCrystallise the amine from pet ether (b 60-80o) (ca 0.5mL/g). The picrate has m 113o (from Et2O). [Beilstein 12 H 1023, 12 I 449, 12 II 548, 12 III 2215, 12 IV 2172.]
N-Phenylbenzylamine Preparation Products And Raw materials
Raw materialsBenzyl chloride
Preparation ProductsErioglaucine disodium salt-->BEPRIDIL-->1R-cis crysanthemic acid-->Acid Blue 9-->ACID BLUE 15
Tag:N-Phenylbenzylamine(103-32-2) Related Product Information
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