N-叔丁氧羰基-去甲托品酮

N-叔丁氧羰基-去甲托品酮性质、用途与生产工艺

简介

制备

在室温条件下，向去甲托品酮盐酸盐(16.2g，100.0mmol)和DCM(300mL)的混合溶液中滴加TEA(30.4g，300.0mmol)，控制体系温度低于30℃。加毕后，再向反应体系中分批加入(Boc)2O(24.0g，110.0mmol)，加毕后，反应体系在室温下搅拌6h。TLC显示原料反应完成以后，反应液一次用1M的稀盐酸，饱和Na2CO3水溶液及饱和食盐水洗涤。有机相用无水Na2SO4干燥，减压浓缩得到22.1g(产率：98％)目标化合物，为无色油状物。

N-叔丁氧羰基-去甲托品酮 上下游产品信息

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N-叔丁氧羰基-去甲托品酮 生产厂家

185099-67-6, N-叔丁氧羰基-去甲托品酮 相关搜索:

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• 1185099-67-6
• N-BOC-NORTROPIN酮
• 8-BOC-3-OXO-8-氮杂双环[3.2.1]辛烷
• 3-氧代-8-氮杂双环[3.2.1]辛烷-8-羧酸叔丁酯
• 3-氧代-8-氮杂双环[3,2,1]辛-8-羧酸叔丁酯
• N-BOC-降托品酮
• N-BOC-去甲托品酮
• N-丁氧羰基去甲托品酮
• N-BOC-去甲基托品酮
• 8-叔丁氧羰基-8-氮杂双环[3,2,1]辛-3-酮,3-氧代-8-氮杂双环[3,2,1]辛-8-羧酸叔丁酯
• N-BOC-托品酮
• N-(叔丁氧羰基)去甲托品酮
• N-叔丁氧羰基去甲托品酮
• N-BOC-喏哌酮
• 185099-67-6
• ert-butyl3-oxo-8-azabicyclo[3.2.1]octane-8-carboxylate
• N-Boc-4-Nortropinone
• TERT-BUTYL 3-OXO-8-AZABICYCLO[3.2.1]OCTANE-8-CARBOXYLATE
• N-(tert-Butoxycarbonyl)-8-azabicyclo[3.2.1]octan-3-one
• 8-Azabicyclo[3.2.1]octane-8-carboxylic acid, 3-oxo-, 1,1-dimethylethyl ester
• N-(tert-Butoxycarbonyl)nortropinone >
• 8-Boc-3-oxo-8-azabicyclo[3.2.1]octane
• Boc-nortropinone98+%
• N-(tert-Butoxycarbonyl)nortropinone
• tert-Butyl 3-oxo-8-azabicyclo[3.2.1]octane-8-carboxylate, N-(tert-Butoxycarbonyl)nortropinone
• N-Boc-nortropinone N-(tert-Butoxycarbonyl)-8-azabicyclo[3.2.1]octan-3-one
• 8-Boc-8-azabicyclo[3.2.1]octan-3-one（N-Boc-nortropinone）
• tert-Butyl 8-aza-3-oxobicyclo[3.2.1]octane-8-carboxylate, N-(tert-Butoxycarbonyl)nortropinone
• tert-Butyl 3-oxo-8-azaicyclo[3.2.1]octane-8-carboxylate
• 8-Boc-8-azabicyclo[3.2.1]...
• pentan-3-ylhydrazine dihydrochloride
• N-Boc-nortropinone ,97%
• (1R,5S)-tert-butyl 3-oxo-8-azabicyclo[3.2.1]octane-8-carboxylate