1-叔丁氧羰基-1-甲基肼

1-叔丁氧羰基-1-甲基肼性质、用途与生产工艺

用途

制备

将7.2g甲基硫酸肼(49.9mmol)加入到144ml水中，冷却至5℃，加入4.6gNaHCO3固体，用NaOH水溶液调节pH至10，向其中滴加144ml (Boc)2O(49.95mmol)的四氢呋喃溶液，搅拌12h，TLC监测反应完全(展开剂：石油醚/乙酸乙酯＝2/1)。乙酸乙酯萃取(100ml×3)，合并有机相，饱和食盐水洗涤，无水硫酸钠干燥，减压浓缩，得到无色透明液体1-叔丁氧羰基-1-甲基肼6.0g(收率82％)。

1-叔丁氧羰基-1-甲基肼 上下游产品信息

上游原料

下游产品

1-叔丁氧羰基-1-甲基肼 生产厂家

21075-83-2, 1-叔丁氧羰基-1-甲基肼 相关搜索:

• 高端化学
• 肼系列
• 化学连接
• 氮化合物
• 1-甲基-1-叔丁氧羰基肼
• 2-甲基肼基甲酸叔丁酯
• 1-叔丁氧羰基-1-甲基肼
• 2-肼基甲酸叔丁酯
• 1-BOC-1-甲基肼
• BOC-甲基肼
• N-BOC-N-甲基肼
• N-(叔丁氧羰基)-N-甲基肼
• 21075-83-2
• 1-Methylhydrazinecarboxylic acid tert-butyl ester
• 1-methyl-Hydrazinecarboxylic acid 1,1-dimethylethyl ester (9CI ACI)
• Hydrazinecarboxylic acid, 1-methyl-, 1,1-dimethylethyl ester (9CI, ACI)
• 1-tert-Butoxycarbonyl-1-methylhydrazine
• Tert-butyl N-amino-N-methyl-carbamate
• 1-Boc-1-methyL
• tert-Butyl 2-Methylcarbazate >
• Hydrazinecarboxylic acid, 1-methyl-, 1,1-dimethylethylester
• 2-Methylcarbazic Acid tert-Butyl Ester
• Boc-1-Methylhydrazine
• 1-Methyl-1-tert-butoxycarbonylhydrazine
• 1-Boc-1-Methylhydrazine 97%
• 2-Methyl-2-propanyl 1-Methylhydrazinecarboxylate
• tert-Butyl 2-methylcarbazate
• tert-Butyl 1-methylhydrazinecarboxylate
• N-Methylhydrazinecarboxylic acid tert-butyl ester
• N-Boc-N-methylhydrazine
• N-(tert-Butoxycarbonyl)-N-methylhydrazine
• 1-Carbo-tert-butoxy-1-methylhydrazine
• 1,1-Dimethylethyl 1-methylhydrazinecarboxylate
• 2-Methylcarbazic acid tert-butyl ester, N-(tert-Butoxycarbonyl)-N-methylhydrazine, N-Boc-N-methylhydrazine
• 1-Boc-1-methylhydrazine
• METHYL TERT BUTYL CARBAZATE OR CEP 11841