Aminomethylphenylketonhydrochlorid
|
|
|
- CAS-Nr.
- 5468-37-1
- Bezeichnung:
- Aminomethylphenylketonhydrochlorid
- Englisch Name:
- 2-Aminoacetophenone hydrochloride
- Synonyma:
- 2-aMino-1-phenylethan-1-one hydrochloride;PHENACYLAMINE HYDROCHLORIDE;α-Aminoacetophenone;2-amino-acetophenonhydrochlo;2-aminophenone hydrochloride;2-amino-acetophenonhydrochloride;w-Aminoacetophenone hydrochloride;ω-aminoacetophenone hydrochloride;O-AMINOACETOPHENONE HYDROCHLORIDE;2-AMINOACETOPHENONE HYDROCHLORIDE
- CBNumber:
- CB6412186
- Summenformel:
- C8H10ClNO
- Molgewicht:
- 171.62
- MOL-Datei:
- 5468-37-1.mol
|
Aminomethylphenylketonhydrochlorid Eigenschaften
- Schmelzpunkt:
- 194 °C (dec.)(lit.)
- storage temp.
- Refrigerator (+4°C)
- Löslichkeit
- DMSO (Slightly), Methanol (Slightly), Water (Slightly)
- Aggregatzustand
- Crystals
- Farbe
- Slightly yellow to beige
- BRN
- 3563173
- Stabilität:
- Hygroscopic
- InChI
- InChI=1S/C8H9NO.ClH/c9-6-8(10)7-4-2-1-3-5-7;/h1-5H,6,9H2;1H
- InChIKey
- CVXGFPPAIUELDV-UHFFFAOYSA-N
- SMILES
- C(C1=CC=CC=C1)(=O)CN.[H]Cl
- CAS Datenbank
- 5468-37-1(CAS DataBase Reference)
- EPA chemische Informationen
- Ethanone, 2-amino-1-phenyl-, hydrochloride (5468-37-1)
Aminomethylphenylketonhydrochlorid Chemische Eigenschaften,Einsatz,Produktion Methoden
R-Sätze Betriebsanweisung:
R36/37/38:Reizt die Augen, die Atmungsorgane und die Haut.
S-Sätze Betriebsanweisung:
S37/39:Bei der Arbeit geeignete Schutzhandschuhe und Schutzbrille/Gesichtsschutz tragen.
S26:Bei Berührung mit den Augen sofort gründlich mit Wasser abspülen und Arzt konsultieren.
Chemische Eigenschaften
Off-white crystalline
Synthese
To a stirred solution of phenacyl bromide (1 mmol, 1 equiv) in diethyl ether (13 mL) was added hexamethylenetetramine (1 mmol, 1 equiv) all at once and the mixture was stirred for 12 h at room temperature. The resulting solid was filtered, washed with diethyl ether (15 mL), and dried under reduced pressure to afford the quaternary salt, which was next placed in a two-necked round-bottomed flask fitted with a reflux condenser, and EtOH (22 mL) was added to it. Concentrated HCl (0.6 mL) was added, and the mixture was refluxed for 3 h (solid formed). After cooling to room temperature, the solid was filtered, washed with EtOH (20 mL), and dried under vacuum to afford pure 2-Aminoacetophenone hydrochloride.
läuterung methode
Crystallise the salt from Me2CO /EtOH, EtOH/ Et2O, 2-propanol or 2-propanol and a little HCl (slowly after a fe
Aminomethylphenylketonhydrochlorid Upstream-Materialien And Downstream Produkte
Upstream-Materialien
Downstream Produkte
Aminomethylphenylketonhydrochlorid Anbieter Lieferant Produzent Hersteller Vertrieb Händler.
Global( 261)Lieferanten
5468-37-1(Aminomethylphenylketonhydrochlorid)Verwandte Suche:
- ω-aminoacetophenone hydrochloride
- w-Aminoacetophenone hydrochloride
- aminomethylphenylketone hydrochloride
- 2-AMinoacetophenone hydrochloride, 96% 1GR
- OMEGA-AMINOACETOPHENONE HYDROCHLORIDE (CA. 4% NACL)
- 2-AMINOACETOPHENONE HYDROCHLORIDE 99%
- O-aminoacetophenone HCl ,1-(o-aminophenyl)ethanone
- ω-Aminoacetophenone hydrochloride, Phenacylamine hydrochloride
- 1-Phenyl-2-aminoethanone·hydrochloride
- Phenacylamine hydrochloride with 4% NaCl
- 2-amino-1-phenyl-ethanonhydrochloride
- 2-Aminoacetophenone hydrochloride,96%
- Acetophenone, 2-aMino-, hydrochloride
- Ethanone,2-aMino-1-phenyl-, hydrochloride (1:1)
- 2-Aminoacetophenone*HCl (with ca. 4% NaCl)
- 2-amino-acetophenonhydrochloride
- OMEGA-AMINOACETOPHENONE HYDROCHLORIDE
- O-AMINOACETOPHENONE HYDROCHLORIDE
- 2-AMINOACETOPHENONE HYDROCHLORIDE
- 2-AMINO-1-PHENYL-ETHANONE HYDROCHLORIDE
- ALPHA-AMINOACETOPHENONE HYDROCHLORIDE
- 2-OXO-2-PHENYL-ETHYL-AMMONIUM, CHLORIDE
- ETHANONE, 2-AMINO-1-PHENYL-, HYDROCHLORIDE
- 2-Aminoacetophenone hydrochloride with 4% NaCl
- w-Amino-acetophinone hydrochloride
- α-Aminoacetophenone (Mixed Salt, >85%)
- α-Aminoacetophenone
- α-Aminoacetophenone Hydrochloride
- 2-amino-acetophenonhydrochlo
- PHENACYLAMINE HYDROCHLORIDE
- 2-aMino-1-phenylethan-1-one hydrochloride
- 2-aminophenone hydrochloride
- 5468-37-1
- 15468-37-1
- C6H5COCH2NH2HCl
- C8H9NOClH
- Organic Building Blocks
- Ketones
- Building Blocks
- C7 to C8
- Carbonyl Compounds
- AMINE
- Ketones
- Organic Building Blocks
- Building Blocks
- C7 to C8
- Carbonyl Compounds
- Chemical Synthesis
