2-AMINOPHENOL-N,O-DIACETATE

2-AMINOPHENOL-N,O-DIACETATE Struktur
5467-64-1
CAS-Nr.
5467-64-1
Englisch Name:
2-AMINOPHENOL-N,O-DIACETATE
Synonyma:
(2-acetamidophenyl) acetate;2-AMINOPHENOL-N,O-DIACETATE;(2-acetamidophenyl) ethanoate;AcetaMide,N-[2-(acetyloxy)phenyl]-;acetic acid (2-acetamidophenyl) ester
CBNumber:
CB8837167
Summenformel:
C10H11NO3
Molgewicht:
193.2
MOL-Datei:
5467-64-1.mol

2-AMINOPHENOL-N,O-DIACETATE Eigenschaften

Schmelzpunkt:
122-124 °C
Siedepunkt:
369.2±25.0 °C(Predicted)
Dichte
1.206±0.06 g/cm3(Predicted)
pka
14.37±0.70(Predicted)

Sicherheit

2-AMINOPHENOL-N,O-DIACETATE Chemische Eigenschaften,Einsatz,Produktion Methoden

Synthese

The synthesis of 2-AMINOPHENOL-N,O-DIACETATE is as follows:The substrate (alcohol, phenol or amine; 1.0 mmol) was treated with Ac2O (2.0 mmol) in the presence of P(4-VPH)ClO4 (50 mg) at room temperature under solvent-free conditions and magnetic stirring. After completion of the reaction as indicated by TLC, the mixture was diluted with Et2O (25 ml) and the catalyst allowed to settle down. The supernatant ethereal solution was decanted off, the catalyst washed with Et2O (2 ml) and the combined ethereal solution concentrated under vacuum to afford the product, identical(mp, IR, 1H and 13C NMR, and GC-MS) to an authentic sample of acetylated product. The recovered catalyst was dried at 50 °C under vacuum for 2 h. The recovered catalyst, after drying, was reused for four more consecutive acetylation reactions of benzyl alcohol (1.0 mmol) affording 96, 96, 94, and 94% yields.
synthesis of 2-AMINOPHENOL-N,O-DIACETATE.png

2-AMINOPHENOL-N,O-DIACETATE Upstream-Materialien And Downstream Produkte

Upstream-Materialien

Downstream Produkte


2-AMINOPHENOL-N,O-DIACETATE Anbieter Lieferant Produzent Hersteller Vertrieb Händler.

Global( 11)Lieferanten
Firmenname Telefon E-Mail Land Produktkatalog Edge Rate
Nanjing Triumpharm Co.,Ltd
+86-02586182925 +86-15105172550
info@triumpharm.com China 129 58
Nanjing Shengkai Pharmaceutical Technology Co., Ltd. 025-86182925 17749516701
195645838@qq.com China 153 58
Hangzhou Milestone Pharmtech Co., Ltd. 0571-82896630 18969958410
sales_hz@milestonepharmtech.com China 4849 55

  • 2-AMINOPHENOL-N,O-DIACETATE
  • (2-acetamidophenyl) acetate
  • (2-acetamidophenyl) ethanoate
  • acetic acid (2-acetamidophenyl) ester
  • AcetaMide,N-[2-(acetyloxy)phenyl]-
  • 5467-64-1
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