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ChemicalBook >> CAS DataBase List >>1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene

1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene

1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene Structure
1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene structure
CAS No.
41481-63-4
Chemical Name:
1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene
Synonyms
Diallyl Ether Bisphenol-S;BIS(4-ALLYLOXYPHENYL)SULFONE;Bis(p-allyloxyphenyl) sulfone;4,4'-Sulfonylbis((allyloxy)benzene);Bis-[4-(2propenyloxy)-phenyl]-sulfone;1-(benzenesulfonyl)-4-prop-2-enoxybenzene;Sulfonylbis(4,1-phenylene)bis(allyl ether);1,1'-PHENYLSULFONYL-4,4'-DIENEPROPYL ETHER;1,1'-sulfonylbis[4-(2-propenyl)oxy-benzene];1,1'-Phenylsulfonyl-4,4'-Dienepropyl(2)Ether
CBNumber:
CB0696083
Molecular Formula:
C18H18O4S
Molecular Weight:
330.4
MDL Number:
MFCD00506306
MOL File:
41481-63-4.mol
Last updated:2023-04-23 13:52:06
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1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene Properties

Melting point 141-142 °C(Solv: ethanol (64-17-5))
Boiling point 500.7±45.0 °C(Predicted)
Density 1.171±0.06 g/cm3(Predicted)
storage temp. -20°C Freezer, Under inert atmosphere
solubility DMSO (Slightly), Methanol (Slightly)
form Solid
color White to Off-White
CAS DataBase Reference 41481-63-4(CAS DataBase Reference)

1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene price

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
TRC A614508 bis(4-Allyloxyphenyl)sulfone 41481-63-4 10g $245 2021-12-16 Buy
Biosynth Carbosynth FB147064 Bis(4-allyloxyphenyl)sulfone 41481-63-4 100g $376 2021-12-16 Buy
AK Scientific P143 1,1'-Sulfonylbis[4-(2-propenyl)oxy-benzene] 41481-63-4 100g $557 2021-12-16 Buy
Biosynth Carbosynth FB147064 Bis(4-allyloxyphenyl)sulfone 41481-63-4 250g $752.5 2021-12-16 Buy
AK Scientific P143 1,1'-Sulfonylbis[4-(2-propenyl)oxy-benzene] 41481-63-4 250g $1065 2021-12-16 Buy
Product number Packaging Price Buy
A614508 10g $245 Buy
FB147064 100g $376 Buy
P143 100g $557 Buy
FB147064 250g $752.5 Buy
P143 250g $1065 Buy

1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene Chemical Properties,Uses,Production

Uses

1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene is a useful research chemical.

Chemical Properties

White crystalline powder

Preparation

The preparation of 1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene is as follows:2400g water, 216g caustic soda lye of 48% strength, 600g 4,4'-dihydroxydiphenyl sulfone and 204g Allyl chloride were mixed and the reaction was carried out at 55-60°C and autogenously generated pressure of 0.8-1. Okg/cm2 for 8 hours. 204g caustic soda lye of 48% strength was added in the reaction mixture, and maintained for 1 hour at 80°C thereafter filtered at 80°C to remove 4,4'-diallyloxydiphenyl sulfone. Further, the filtrate solution was treated with 5g activated carbon and 5g sequestering agent at 85- 90°C. The pH of filtrated solution was adjusted to 8.9 with 20% sulfuric acid and cooled to 35°C. The precipitate was separated by filtration and slurred in water. The pH was adjusted to 4.94 with 20% sulfuric acid and the precipitate was separated by filtration, and washed with water and dried to obtain 615g the product 4-allyloxy 4'-hydroxydiphenyl sulfone of 96% purity. The yield was 93.5% with respect to 4,4'-dihydroxydiphenyl sulfone. The wet cake of 4,4'-diallyloxydiphenyl sulfone was slurred in 100g of 5%w/v aqueous solution of sodium hydroxide and refluxed for 1 hour, then cooled to 80°C. The precipitate was filtered, washed with water and dried to obtain 45g of 4,4'-diallyloxy diphenyl sulfone of 91.9% purity. The yield was 6% with respect to 4,4'-dihydroxydiphenyl sulfone. pH of the mother liquor obtained after separation of 4-allyloxy 4'-hydroxydiphenyl sulfone, was adjusted to 4.5 with 20% sulfuric acid. The precipitate was separated by filtration, washed with water and dried to obtain 33g of 4,4'-dihydroxydiphenyl sulfone of 87.9% purity. The conversion of 4,4'-dihydroxydiphenyl sulfone was 94.50%.; 595g of 4-allyloxy 4'-hydroxydiphenyl sulfone of 96% purity was dissolved in 230g of 48% strength caustic soda lye and 1000g water, treated with 5g activated carbon and 5g sequestering agent at 85-90°C. The slurry was filtered and pH of the filtrate was adjusted to 8.95 with 20% sulfuric acid and then cooled to 35°C. The precipitate was separated by filtration, slurried in water and the pH was adjusted to 5.0 with 20% sulfuric acid. The slurry was filtrated and the precipitate was washed with water and dried to obtain 563g of 4- allyloxy 4'-hydroxydiphenyl sulfone of 99.273% purity.

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1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene synthesis

80-09-1
106-95-6
41481-63-4
Synthesis of 1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene from Bis(4-hydroxyphenyl) Sulfone and Allyl bromide

1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene Preparation Products And Raw materials

Raw materials

Allyl chloride propene Bis(4-hydroxyphenyl) Sulfone Allyl bromide

Preparation Products

Bis(3-allyl-4-hydroxyphenyl)sulfone

1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene Suppliers

Global( 90)Suppliers
Supplier Tel Email Country ProdList Advantage
Shanghai Daken Advanced Materials Co.,Ltd 		+86-371-66670886 info@dakenam.com China 15928 58
ATK CHEMICAL COMPANY LIMITED 		+undefined-21-51877795 ivan@atkchemical.com China 32480 60
career henan chemical co 		+86-0371-86658258 sales@coreychem.com China 29914 58
Shenzhen Nexconn Pharmatechs Ltd 		+86-755-89396905 +86-15013857715 admin@nexconn.com China 10248 58
Chongqing Chemdad Co., Ltd 		+86-023-61398051 +8613650506873 sales@chemdad.com China 39916 58
SIMAGCHEM CORP 		+86-13806087780 sale@simagchem.com China 17367 58
Hefei TNJ Chemical Industry Co.,Ltd. 		0551-65418671 sales@tnjchem.com China 34572 58
Dayang Chem (Hangzhou) Co.,Ltd. 		571-88938639 +8617705817739 info@dycnchem.com CHINA 52867 58
Hebei Duling International Trade Co. LTD 		+8618032673083 sales05@hbduling.cn China 15745 58
Hangzhou MolCore BioPharmatech Co.,Ltd. 		+86-057181025280; +8617767106207 sales@molcore.com China 49739 58
Supplier Advantage
Shanghai Daken Advanced Materials Co.,Ltd 		58
ATK CHEMICAL COMPANY LIMITED 		60
career henan chemical co 		58
Shenzhen Nexconn Pharmatechs Ltd 		58
Chongqing Chemdad Co., Ltd 		58
SIMAGCHEM CORP 		58
Hefei TNJ Chemical Industry Co.,Ltd. 		58
Dayang Chem (Hangzhou) Co.,Ltd. 		58
Hebei Duling International Trade Co. LTD 		58
Hangzhou MolCore BioPharmatech Co.,Ltd. 		58

View Lastest Price from 1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
1-Prop-2-enoxy-4-(4-prop-2-enoxyphenyl)sulfonyl-benzene pictures 2022-09-20 1-Prop-2-enoxy-4-(4-prop-2-enoxyphenyl)sulfonyl-benzene
41481-63-4
 US $0.00-0.00 / kg 1kg 98% 1Ton Henan Aochuang Chemical Co.,Ltd.
1-Prop-2-enoxy-4-(4-prop-2-enoxyphenyl)sulfonyl-benzene pictures 2021-08-12 1-Prop-2-enoxy-4-(4-prop-2-enoxyphenyl)sulfonyl-benzene
41481-63-4
 US $15.00-10.00 / KG 1KG 99%+ HPLC Monthly supply of 1 ton Zhuozhou Wenxi import and Export Co., Ltd
1-Prop-2-enoxy-4-(4-prop-2-enoxyphenyl)sulfonyl-benzene pictures 2019-07-06 1-Prop-2-enoxy-4-(4-prop-2-enoxyphenyl)sulfonyl-benzene
41481-63-4
 US $2.00 / kg 1kg 99% ask Career Henan Chemical Co

41481-63-4(1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene)Related Search:

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4-Methoxybenzoic acid Allyl ether Bis(4-hydroxyphenyl) Sulfone 4,4'-Thiobis-phenol Bis(4-methoxyphenyl) sulfoxide
1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene 4-((3,5-DIMETHYL-4-[(2,3,3-TRICHLOROACRYLOYL)OXY]PHENYL)SULFONYL)-2,6-DIMETHYLPHENYL 2,3,3-TRICHLOROACRYLATE 4-((4-[(2,3,3-TRICHLOROACRYLOYL)OXY]PHENYL)SULFONYL)PHENYL 2,3,3-TRICHLOROACRYLATE

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1,1'-sulfonylbis[4-(2-propenyl)oxy-benzene] 1,1'-PHENYLSULFONYL-4,4'-DIENEPROPYL ETHER 1,1'-Phenylsulfonyl-4,4'-Dienepropyl(2)Ether Bis-[4-(2propenyloxy)-phenyl]-sulfone Bis(p-allyloxyphenyl) sulfone Sulfonylbis(4,1-phenylene)bis(allyl ether) 1-allyloxy-4-(4-allyloxyphenyl)sulfonyl-benzene 1-prop-2-enoxy-4-(4-prop-2-enoxyphenyl)sulfonyl-benzene BIS(4-ALLYLOXYPHENYL)SULFONE 1-(benzenesulfonyl)-4-prop-2-enoxybenzene Diallyl Ether Bisphenol-S Benzene, 1,1'-sulfonylbis[4-(2-propen-1-yloxy)- 4,4'-Sulfonylbis((allyloxy)benzene) 1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene 41481-63-4 C18H18O4S Industrial/Fine Chemicals Aromatics