ChemicalBook >> CAS DataBase List >>1,3,5-TRIIODOBENZENE

1,3,5-TRIIODOBENZENE

CAS No.
626-44-8
Chemical Name:
1,3,5-TRIIODOBENZENE
Synonyms
5-Triiodobenzene;2,4,6-Triiodobenzene;1,3,5-TRIIODOBENZENE;Benzene, 1,3,5-triiodo-;1,3,5-TRIIODOBENZENE, 95 %
CBNumber:
CB1294914
Molecular Formula:
C6H3I3
Molecular Weight:
455.8
MDL Number:
MFCD02690052
MOL File:
626-44-8.mol
MSDS File:
SDS
Last updated:2023-12-28 18:13:10

1,3,5-TRIIODOBENZENE Properties

Melting point 184.2°C
Boiling point 381.91°C (rough estimate)
Density 2.8493 (rough estimate)
refractive index 1.8070 (estimate)
storage temp. Keep in dark place,Sealed in dry,Room Temperature
solubility Chloroform (Slightly), Methanol (Slightly, Heated)
form Solid
color White to Off-White

SAFETY

Risk and Safety Statements

Symbol(GHS)  GHS hazard pictograms
GHS07
Signal word  Warning
Hazard statements  H315-H319-H335
Precautionary statements  P261-P305+P351+P338

1,3,5-TRIIODOBENZENE price More Price(20)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Matrix Scientific 097888 1,3,5-Triiodobenzene 95+% 626-44-8 250mg $59 2021-12-16 Buy
AK Scientific J54628 1,3,5-Triiodobenzene 626-44-8 250mg $60 2021-12-16 Buy
Matrix Scientific 097888 1,3,5-Triiodobenzene 95+% 626-44-8 500mg $91 2021-12-16 Buy
Ark Pharm AK101088 1,3,5-Triiodobenzene 98% 626-44-8 10g $572 2021-12-16 Buy
American Custom Chemicals Corporation HCH0295342 1,3,5-TRIIODOBENZENE 98.00% 626-44-8 1G $1270.5 2021-12-16 Buy
Product number Packaging Price Buy
097888 250mg $59 Buy
J54628 250mg $60 Buy
097888 500mg $91 Buy
AK101088 10g $572 Buy
HCH0295342 1G $1270.5 Buy

1,3,5-TRIIODOBENZENE Chemical Properties,Uses,Production

Uses

1,3,5-Triiodobenzene is used in the synthesis of conjugated microporous polymers through cationic cyclization polymerization. It also can be used in optical materials.

Synthesis

1,3,5-Triiodobenzene was synthesized by reacting 2,4,6-triiodoaniline with NaNO2 in the presence of copper(I) oxide.
Experimental procedure: Finely ground NaNO2 (1.95 g, 0.028 mol) was slowly added with stirring to sulfuric acid (3.5 mL). Then a solution of 2,4,6-triiodoaniline(2.90 g, 6.16 mmol) in glacial AcOH (130 mL) was added dropwise with stirring and cooling at such a rate that the temperature of the reaction mixture was kept below 20 °C. Following addition of the amine, the reaction mixture was stirred at ≈20 °C for about 30 min. The resulting solution of the diazonium salt was added dropwise to a suspension of copper(I) oxide (2.52 g) in dry ethanol (70 mL) with vigorous stirring over 15 min. The reaction mixture was brought to boiling and stirred for 30 min until elimination of nitrogen ceased. Then the mixture was cooled, kept for one day, poured into ice water (300 mL), and extracted with benzene (3×50 mL). The benzene extracts were dried with anhydrous Na2SO4 and the solvent was distilled off in vacuo. The residue was repeatedly recrystallized from benzene. The yield was 2.01 g (84%), m.p. 182 °C (cf. lit. data11: m.p. 183 °C). 1H NMR (CDCl3), δ: 8.02 (s, 3 H, CH). 13C NMR (CDCl3), δ: 79; 128.

1,3,5-TRIIODOBENZENE Preparation Products And Raw materials

Raw materials

Preparation Products

1,3,5-TRIIODOBENZENE Suppliers

Global( 66)Suppliers
Supplier Tel Email Country ProdList Advantage
Henan Fengda Chemical Co., Ltd
+86-371-86557731 +86-13613820652 info@fdachem.com China 7845 58
ATK CHEMICAL COMPANY LIMITED
+undefined-21-51877795 ivan@atkchemical.com China 32480 60
Zhengzhou Alfa Chemical Co.,Ltd
+8618530059196 sale04@alfachem.cn China 12468 58
Career Henan Chemica Co
+86-0371-86658258 15093356674; laboratory@coreychem.com China 30255 58
CD Chemical Group Limited
+8615986615575 info@codchem.com China 20356 58
LEAP CHEM CO., LTD.
+86-852-30606658 market18@leapchem.com China 24738 58
Aromsyn Co., Ltd.
+86-0571-85585865 +8613336024896 CB@aromsyn.com China 19185 58
Hebei Guanlang Biotechnology Co., Ltd.
+86-19930503259 +86-19930503259 cherry@crovellbio.com China 18456 58
Shanghai Acmec Biochemical Technology Co., Ltd.
+undefined18621343501 product@acmec-e.com China 33349 58
Aladdin Scientific
+1-833-552-7181 sales@aladdinsci.com United States 57511 58

View Lastest Price from 1,3,5-TRIIODOBENZENE manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
1,3,5-TRIIODOBENZENE pictures 2023-12-29 1,3,5-TRIIODOBENZENE
626-44-8
US $101.00-1.00 / KG 1KG 99% g-kg-tons, free sample is available Henan Fengda Chemical Co., Ltd
Benzene, 1,3,5-triiodo- 1,3,5-TRIIODOBENZENE 2,4,6-Triiodobenzene 1,3,5-TRIIODOBENZENE, 95 % 5-Triiodobenzene 626-44-8 C6H3I3