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N-(Hydroxymethyl)phthalimide

N-(Hydroxymethyl)phthalimide
N-(Hydroxymethyl)phthalimide structure
CAS No.
118-29-6
Chemical Name:
N-(Hydroxymethyl)phthalimide
Synonyms
AURORA KA-454;N-(HydroxymethyL;AKOS BBS-00004724;PHTHALIMIDOMETHANOL;IFLAB-BB F0777-0575;N-(Hydroxymethyl)ph;oxymethylphthalimide;Phthalimidylmethanol;N-Methylolphthalimide;Oxymethyl phthalimide
CBNumber:
CB1392676
Molecular Formula:
C9H7NO3
Formula Weight:
177.16
MOL File:
118-29-6.mol

N-(Hydroxymethyl)phthalimide Properties

Melting point:
147-149 °C (lit.)
Boiling point:
309.06°C (rough estimate)
Density 
1.3312 (rough estimate)
refractive index 
1.5200 (estimate)
storage temp. 
Store below +30°C.
form 
Fine Crystalline Powder
pka
13.17±0.10(Predicted)
color 
White
BRN 
140946
InChIKey
MNSGOOCAMMSKGI-UHFFFAOYSA-N
CAS DataBase Reference
118-29-6(CAS DataBase Reference)
EWG's Food Scores
1
FDA UNII
G8L8BA278J
NIST Chemistry Reference
1H-isoindole-1,3(2h)-dione, 2-(hydroxymethyl)-(118-29-6)
EPA Substance Registry System
N-(Hydroxymethyl)phthalimide (118-29-6)
SAFETY
  • Risk and Safety Statements
Symbol(GHS) 
GHS07
Hazard statements  H315-H319-H335
Precautionary statements  P261-P280a-P304+P340-P305+P351+P338-P405-P501a
Safety Statements  22-24/25
WGK Germany  3
RTECS  TI5270000
TSCA  Yes
HS Code  29251995

N-(Hydroxymethyl)phthalimide price More Price(8)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Sigma-Aldrich 8.14422 N-(Hydroxymethyl)-phthalimide for synthesis 118-29-6 100 g $46.8 2021-03-22 Buy
Sigma-Aldrich 8.14422 N-(Hydroxymethyl)-phthalimide for synthesis. CAS 118-29-6, molar mass 177.16 g/mol., for synthesis 118-29-6 8144220100 $48.9 2020-08-18 Buy
Sigma-Aldrich H41803 N-(Hydroxymethyl)phthalimide 97% 118-29-6 100g $114 2021-03-22 Buy
TCI Chemical H0648 N-Hydroxymethylphthalimide >98.0%(HPLC)(N) 118-29-6 25g $30 2021-03-22 Buy
TCI Chemical H0648 N-Hydroxymethylphthalimide >98.0%(HPLC)(N) 118-29-6 250g $113 2021-03-22 Buy

N-(Hydroxymethyl)phthalimide Chemical Properties,Uses,Production

Chemical Properties

white crystalline powder

Definition

ChEBI: A primary alcohol comprising phthalimide carrying an N-hydroxymethyl substituent.

Preparation

To a flask equipped with a mechanical stirrer and condenser is added 511 gm (3.47 moles) of phthalimide, 260 ml of 40% formalin (3.47 moles), and 1750 ml of water. The mixture is refluxed for about 5-10 min or until a clear solution results (if any insoluble material remains, it is first filtered). Then the mixture is cooled for several hours. The resulting product is filtered with suction, washed with cold water, and air-dried to afford 594 gm (96%), m.p. 137-141°C.
NOTE: The product should not be oven-dried since it decomposes with the loss of formaldehyde. Recrystallization of the product from ethanol affords 94% recovery of the original material with the same melting point range.
Preparation of N-Hydroxymethylphthalimide

Synthesis Reference(s)

Journal of the American Chemical Society, 77, p. 1913, 1955 DOI: 10.1021/ja01612a068

N-(Hydroxymethyl)phthalimide Preparation Products And Raw materials

Raw materials

Preparation Products


N-(Hydroxymethyl)phthalimide Suppliers

Global( 268)Suppliers
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View Lastest Price from N-(Hydroxymethyl)phthalimide manufacturers

Image Release date Product Price Min. Order Purity Supply Ability Manufacturer
2021-09-29 N-(Hydroxymethyl)phthalimide
118-29-6
US $0.00 / Kg/Bag 1KG 99%min 10000kg WUHAN FORTUNA CHEMICAL CO., LTD
2021-08-26 N-(Hydroxymethyl)phthalimide
118-29-6
US $5.60 / KG 1KG 99% 5000kg Hebei Crovell Biotech Co Ltd
2021-07-02 N-(Hydroxymethyl)phthalimide
118-29-6
US $15.00-10.00 / KG 1KG 99%+ HPLC Monthly supply of 1 ton Zhuozhou Wenxi import and Export Co., Ltd

N-(Hydroxymethyl)phthalimide Spectrum


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