4-IODOPHTHALONITRILE 97
- CAS No.
- 69518-17-8
- Chemical Name:
- 4-IODOPHTHALONITRILE 97
- Synonyms
- 4-Iodophthalonitri;4-Iodophthalonitrile 97%;4-IODOPHTHALONITRILE 97;1,2-Dicyano-4-iodobenzene;1,2-Benzenedicarbonitrile, 4-iodo-
- CBNumber:
- CB2499525
- Molecular Formula:
- C8H3IN2
- Molecular Weight:
- 254.03
- MDL Number:
- MFCD01863730
- MOL File:
- 69518-17-8.mol
- MSDS File:
- SDS
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|||||||||
|---|---|---|---|---|---|---|---|---|---|---|
| Signal word | Warning | |||||||||
| Hazard statements | H302+H312+H332-H315-H319-H335 | |||||||||
| Precautionary statements | P261-P280-P301+P312-P302+P352+P312-P304+P340+P312-P305+P351+P338 | |||||||||
| Hazard Codes | Xn | |||||||||
| Risk Statements | 20/21/22-36/37/38 | |||||||||
| Safety Statements | 26-36 | |||||||||
| WGK Germany | 3 | |||||||||
| HS Code | 2926.90.4801 | |||||||||
| NFPA 704 |
|
4-IODOPHTHALONITRILE 97 price More Price(12)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Sigma-Aldrich | 515426 | 4-Iodophthalonitrile 97% | 69518-17-8 | 1g | $152 | 2024-03-01 | Buy |
| TCI Chemical | I1050 | 4-Iodophthalonitrile >98.0%(GC) | 69518-17-8 | 1g | $146 | 2024-03-01 | Buy |
| TRC | I737185 | 4-Iodophthalonitrile | 69518-17-8 | 100mg | $45 | 2021-12-16 | Buy |
| TRC | I737185 | 4-Iodophthalonitrile | 69518-17-8 | 500mg | $200 | 2021-12-16 | Buy |
| AK Scientific | 1633BB | 4-Iodophthalonitrile | 69518-17-8 | 1g | $224 | 2021-12-16 | Buy |
4-IODOPHTHALONITRILE 97 Chemical Properties,Uses,Production
Synthesis
1.6 g (0.011 mol) 4-aminophthalonitrile was dissolved in 22.4 mL of 2.5 M
H2SO4. The mixture was cooled to 0 ??C. To the solution was slowly added 0.9 g
(0.013 mol) of NaNO2 dissolved in 3.5 mL of water. After the mixture was stirred for
30 minutes, 2.08 g (0.013 mol) of KI dissolved in 12.8 mL of water was added. The
mixture was further stirred for 45 minutes at room temperature. After this period, the
brown solid was filtered and washed with water. It was dissolved in a minimal
amount of chloroform. The solution was washed first with saturated Na2S2O3 and
then with water. It was dried over Na2SO4. After the solution was filtered, it was
dried in vacuum and purified with column chromatography over silica gel by eluting
with dichloromethane. Molecular formula: IC6H3-1,2-(CN)2 (254.03 g/mol). Yield:
2.37 g (85%).
4-IODOPHTHALONITRILE 97 Preparation Products And Raw materials
Raw materials
Preparation Products
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| ATK CHEMICAL COMPANY LIMITED | +undefined-21-51877795 | ivan@atkchemical.com | China | 32480 | 60 |
| Alchem Pharmtech,Inc. | 8485655694 | sales@alchempharmtech.com | United States | 63711 | 58 |
| CR Corporation Lomited | fred.wen@crcorporation.cn | CHINA | 12069 | 58 | |
| Aceschem Inc. | +1-817863-6948 +1-（817）863-6948 | sales@aceschem.com | United States | 19639 | 58 |
| Aladdin Scientific | +1-833-552-7181 | sales@aladdinsci.com | United States | 57511 | 58 |
| TCI (Shanghai) Development Co., Ltd. | 021-67121386 | Sales-CN@TCIchemicals.com | China | 24539 | 81 |
| Energy Chemical | 021-021-58432009 400-005-6266 | sales8178@energy-chemical.com | China | 44751 | 61 |
| Adamas Reagent, Ltd. | 400-6009262 16621234537 | zhangsn@titansci.com | China | 14113 | 59 |
| TOKYO CHEMICAL INDUSTRY CO., LTD. | 03-36680489 | Sales-JP@TCIchemicals.com | Japan | 28398 | 80 |
| TCI Europe | 320-37350700 | sales@tcieurope.eu | Europe | 23680 | 75 |
| Supplier | Advantage |
|---|---|
| ATK CHEMICAL COMPANY LIMITED | 60 |
| Alchem Pharmtech,Inc. | 58 |
| CR Corporation Lomited | 58 |
| Aceschem Inc. | 58 |
| Aladdin Scientific | 58 |
| TCI (Shanghai) Development Co., Ltd. | 81 |
| Energy Chemical | 61 |
| Adamas Reagent, Ltd. | 59 |
| TOKYO CHEMICAL INDUSTRY CO., LTD. | 80 |
| TCI Europe | 75 |