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Ethyl (2Z)-chloro[(4-methoxyphenyl)hydrazono]ethanoate

Ethyl (2Z)-chloro[(4-methoxyphenyl)hydrazono]ethanoate Structure
Ethyl (2Z)-chloro[(4-methoxyphenyl)hydrazono]ethanoate structure
CAS No.
473927-63-8
Chemical Name:
Ethyl (2Z)-chloro[(4-methoxyphenyl)hydrazono]ethanoate
Synonyms
Apixaban I;Apixaban int;Apixaban Impurity O;Ethyl (2Z)-chloro[(4-methoxyphenyl)hydrazono]acetate;Ethyl (2Z)-chloro[(4-methoxyphenyl)hydrazono]ethanoate;Acetic acid, chloro[(4-methoxyphenyl)hydrazono]-, ethyl este...;Ethyl (2Z)-2-chloro-2-[2-(4-methoxyphenyl)hydrazinylidene]acetate;ethyl (2Z)-2-chloro-2-[2-(4-methoxyphenyl)hydrazin-1-ylidene]acetate;Acetic acid, chloro[(4-Methoxyphenyl)hydrazono]-, ethyl ester, (2Z)-;(2Z)-2-Chloro-2-[2-(4-methoxyphenyl)hydrazinylidene]acetic acid ethyl ester
CBNumber:
CB32514108
Molecular Formula:
C11H13ClN2O3
Molecular Weight:
256.69
MDL Number:
MOL File:
473927-63-8.mol
MSDS File:
SDS
Last updated:2023-08-15 13:21:15
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Ethyl (2Z)-chloro[(4-methoxyphenyl)hydrazono]ethanoate Properties

Boiling point 349.0±44.0 °C(Predicted)
Density 1.23
vapor pressure 0.008Pa at 25℃
pka 11.63±0.10(Predicted)
InChI InChI=1S/C11H13ClN2O3/c1-3-17-11(15)10(12)14-13-8-4-6-9(16-2)7-5-8/h4-7,13H,3H2,1-2H3/b14-10-
InChIKey ATNPZEGMKLGIFA-UVTDQMKNSA-N
SMILES C(OCC)(=O)/C(/Cl)=N/NC1=CC=C(OC)C=C1
LogP 2.53

SAFETY

Risk and Safety Statements

Symbol(GHS)  GHS hazard pictogramsGHS hazard pictograms
GHS06,GHS08
Signal word  Danger
Hazard statements  H301-H311-H331-H341
Precautionary statements  P201-P202-P261-P264-P270-P271-P280-P302+P352-P304+P340-P308+P313-P310-P330-P361-P403+P233-P405-P501

Ethyl (2Z)-chloro[(4-methoxyphenyl)hydrazono]ethanoate price

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Crysdot CD12069983 (Z)-Ethyl2-chloro-2-(2-(4-methoxyphenyl)hydrazono)acetate 95+% 473927-63-8 5g $360 2021-12-16 Buy
Alichem 473927638 (Z)-Ethyl2-chloro-2-(2-(4-methoxyphenyl)hydrazono)acetate 473927-63-8 10g $523.8 2021-12-16 Buy
Crysdot CD12069983 (Z)-Ethyl2-chloro-2-(2-(4-methoxyphenyl)hydrazono)acetate 95+% 473927-63-8 10g $540 2021-12-16 Buy
Product number Packaging Price Buy
CD12069983 5g $360 Buy
473927638 10g $523.8 Buy
CD12069983 10g $540 Buy

Ethyl (2Z)-chloro[(4-methoxyphenyl)hydrazono]ethanoate Chemical Properties,Uses,Production

Uses

Ethyl (2Z)-chloro[(4-methoxyphenyl)hydrazono]ethanoate can be used as organic synthesis intermediates and pharmaceutical intermediates, mainly used in laboratory research and development and chemical and pharmaceutical production processes.

Synthesis

Synthesis_473927-63-8
Preparation of ethyl (2Z)-chloro[(4-methoxyphenyl)hydrazono]ethanoate To p-anisidine (16 g, 0.129 mol) in conc. HCL (40 mL), 100 mL) H2O, cooled to -5?? C. and sodium nitrite (9.4 g, 0.136 mol) in H2O (60 mL) was added. The reaction mixture was stirred at -5?? C. for 20 min and a mixture of ethylchloroacetoacetate (22 g, 0.133 mol), ethanol (100 mL), sodiumacetate (32 g, 0.389 mmol), and H2O (400 mL) was added. The reaction was allowed to warm up to room temperature and stirred for 2h. The product precipitated as a black solid. It was filtered and dried (30 g). 1H-NMR (CDCl3) |? 8.28 (s, 1H), 7.18 (d, 2H), 6.90 (d, 2H), 4.41 (q, 2H), 3.80 (s, 3H), 1.42 (t, 3H) ppm.

Ethyl (2Z)-chloro[(4-methoxyphenyl)hydrazono]ethanoate synthesis

104-94-9
105-39-5
473927-63-8
Synthesis of Ethyl (2Z)-chloro[(4-methoxyphenyl)hydrazono]ethanoate from p-Anisidine and Ethyl chloroacetate

Ethyl (2Z)-chloro[(4-methoxyphenyl)hydrazono]ethanoate Preparation Products And Raw materials

Raw materials

Ethyl 2-chloroacetoacetate Sodium acetate p-Anisidine Ethyl chloroacetate

Preparation Products

Apixaban Impurity 17

Ethyl (2Z)-chloro[(4-methoxyphenyl)hydrazono]ethanoate Suppliers

Global( 115)Suppliers
Supplier Tel Email Country ProdList Advantage
Jinan Million Pharmaceutical Co., Ltd
+86-531-68659554 +8613031714605 info@millionpharm.com China 153 58
Capot Chemical Co.,Ltd. 		571-85586718 +8613336195806 sales@capotchem.com China 29797 60
Shanghai Daken Advanced Materials Co.,Ltd 		+86-371-66670886 info@dakenam.com China 15928 58
Beijing Cooperate Pharmaceutical Co.,Ltd 		010-60279497 sales01@cooperate-pharm.com CHINA 1811 55
Speranza Chemical Co., Ltd. 		+86-86-075521030354 +8618688942810 sophieliu@speranzachem.com China 723 55
Jinan Jianfeng Chemical Co., Ltd 		0531-88110457; +8615562555968 info@pharmachemm.com China 241 58
Jinan Finer Chemical Co., Ltd 		+86-531-88989536 +86-15508631887 sales@finerchem.com China 2967 58
Alchem Pharmtech,Inc. 		8485655694 sales@alchempharmtech.com United States 63711 58
Shenzhen Excellent Biotech Co., Ltd. 		13480692018 ramyan@ex-biotech.com CHINA 954 58
CONIER CHEM AND PHARMA LIMITED 		+8618523575427 sales@conier.com China 47465 58
Supplier Advantage
Jinan Million Pharmaceutical Co., Ltd
58
Capot Chemical Co.,Ltd. 		60
Shanghai Daken Advanced Materials Co.,Ltd 		58
Beijing Cooperate Pharmaceutical Co.,Ltd 		55
Speranza Chemical Co., Ltd. 		55
Jinan Jianfeng Chemical Co., Ltd 		58
Jinan Finer Chemical Co., Ltd 		58
Alchem Pharmtech,Inc. 		58
Shenzhen Excellent Biotech Co., Ltd. 		58
CONIER CHEM AND PHARMA LIMITED 		58

View Lastest Price from Ethyl (2Z)-chloro[(4-methoxyphenyl)hydrazono]ethanoate manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
Ethyl (2Z)-chloro[(4-methoxyphenyl)hydrazono]ethanoate pictures 2024-04-25 Ethyl (2Z)-chloro[(4-methoxyphenyl)hydrazono]ethanoate
473927-63-8
 US $30.00 / KG 1KG 99% 300MT/year Speranza Chemical Co., Ltd.
Ethyl (2Z)-chloro[(4-methoxyphenyl)hydrazono]ethanoate pictures 2024-04-25 Ethyl (2Z)-chloro[(4-methoxyphenyl)hydrazono]ethanoate
473927-63-8
 US $2.00 / kg 1kg 99% 1200KG/M Jinan Million Pharmaceutical Co., Ltd
Ethyl(2Z)-chloro[(4-methoxyphenyl)hydrazono]ethanoate pictures 2019-12-20 Ethyl(2Z)-chloro[(4-methoxyphenyl)hydrazono]ethanoate
473927-63-8
 US $1.00 / g 1g 99% g/kg/T Career Henan Chemical Co

473927-63-8(Ethyl (2Z)-chloro[(4-methoxyphenyl)hydrazono]ethanoate)Related Search:

Apixaban IMpurity 2 3-Morpholino-1-(4-(2-oxopiperidin-1-yl)phenyl)-5,6-dihydropyridin-2(1H)-one 3-Morpholino-1-(4-nitrophenyl)-5,6-dihydropyridin-2(1H)-one ethyl 6-(4-aMinophenyl)-1-(4-Methoxyphenyl)-7-oxo-4,5,6,7-tetrahydro-1H-pyrazolo[3,4-c]pyridine-3-carboxylate ETHYL (2E)-CHLORO[(4-CHLOROPHENYL)HYDRAZONO]ACETATE
1-(4-AMinophenyl)-5,6-dihydro-3-(4-Morpholinyl)-2(1h)-pyridinone 1-(4-Methoxyphenyl)-6-(4-(2-Methyl-6-oxopiperidin-1-yl)phenyl)-7-oxo-4,5,6,7-tetrahydro-1H-pyrazolo[3,4-c]pyridine-3-carboxaMide 1-(4-(2-methyl-6-oxopiperidin-1-yl)phenyl)-3-morpholino-5,6-dihydropyridin-2(1H)-one 1-(4-Hydroxyphenyl)-7-oxo-6-[4-(2-oxopiperidin-1-yl)phenyl]-4,5,6,7-tetrahydro-1H-pyrazolo[3,4-c]pyridine-3-carboxamide 1-(4-IODO-PHENYL)-PIPERIDIN-2-ONE
ethyl 1-(4-methoxyphenyl)-6-(4-nitrophenyl)-7-oxo-4,5,6,7-tetrahydro-1H-pyrazolo[3,4-c]pyridine-3-carboxylate Apixaban IMpurity(BMS-591329-01) 3,3-Dichloro-1-(4-nitrophenyl)piperidin-2-one Apixaban Impurity 16 Apixaban Impurity 13
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Acetic acid, chloro[(4-Methoxyphenyl)hydrazono]-, ethyl ester, (2Z)- Ethyl (2Z)-chloro[(4-methoxyphenyl)hydrazono]ethanoate (2Z)-2-Chloro-2-[2-(4-methoxyphenyl)hydrazinylidene]acetic acid ethyl ester Ethyl (2Z)-chloro[(4-methoxyphenyl)hydrazono]acetate Apixaban I ethyl (2Z)-2-chloro-2-[2-(4-methoxyphenyl)hydrazin-1-ylidene]acetate Apixaban Impurity O Apixaban int Acetic acid, 2-chloro-2-[2-(4-methoxyphenyl)hydrazinylidene]-, ethyl ester, (2Z)- Acetic acid, chloro[(4-methoxyphenyl)hydrazono]-, ethyl este... Ethyl 2-chloro-2-(2-(4-methoxyphenyl)hydrazono)acetateQ: What is Ethyl 2-chloro-2-(2-(4-methoxyphenyl)hydrazono)acetate Q: What is the CAS Number of Ethyl 2-chloro-2-(2-(4-methoxyphenyl)hydrazono)acetate Ethyl (2Z)-2-chloro-2-[2-(4-methoxyphenyl)hydrazinylidene]acetate 473927-63-8 473927-63-8