ChemicalBook >> CAS DataBase List >>3,3-diMethyl-6-nitrobenzo[c][1,2]oxaborol-1(3H)-ol

3,3-diMethyl-6-nitrobenzo[c][1,2]oxaborol-1(3H)-ol

CAS No.
1266084-47-2
Chemical Name:
3,3-diMethyl-6-nitrobenzo[c][1,2]oxaborol-1(3H)-ol
Synonyms
3,3-diMethyl-6-nitrobenzo[c][1,2]oxaborol-1(3H)-ol;3,3-Dimethyl-6-Nitrobenzo[C][1,2]Oxaborol-1(3H)-Ol(WXC00403);1,3-dihydro-1-hydroxy-3,3-dimethyl-6-nitro-2,1-Benzoxaborole;2,1-Benzoxaborole, 1,3-dihydro-1-hydroxy-3,3-dimethyl-6-nitro-
CBNumber:
CB32684496
Molecular Formula:
C9H10BNO4
Molecular Weight:
206.99
MDL Number:
MOL File:
1266084-47-2.mol
Last updated:2023-10-17 10:05:41

3,3-diMethyl-6-nitrobenzo[c][1,2]oxaborol-1(3H)-ol price More Price(4)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
TRC D480708 3,3-Dimethyl-6-Nitrobenzo[C][1,2]Oxaborol-1(3H)-Ol 1266084-47-2 2.5mg $45 2021-12-16 Buy
TRC D480708 3,3-Dimethyl-6-Nitrobenzo[C][1,2]Oxaborol-1(3H)-Ol 1266084-47-2 25mg $175 2021-12-16 Buy
Crysdot CD11303613 3,3-Dimethyl-6-nitrobenzo[c][1,2]oxaborol-1(3H)-ol 95+% 1266084-47-2 1g $892 2021-12-16 Buy
Crysdot CD11303613 3,3-Dimethyl-6-nitrobenzo[c][1,2]oxaborol-1(3H)-ol 95+% 1266084-47-2 5g $2679 2021-12-16 Buy
Product number Packaging Price Buy
D480708 2.5mg $45 Buy
D480708 25mg $175 Buy
CD11303613 1g $892 Buy
CD11303613 5g $2679 Buy

3,3-diMethyl-6-nitrobenzo[c][1,2]oxaborol-1(3H)-ol Chemical Properties,Uses,Production

Chemical Properties

Yellow solid

Synthesis

At -40°C, to 100% fuming nitric acid (10 mL) was added dropwise a solution of 3,3-dimethylbenzo[c][l,2]oxaborol-l(3H)-ol (XCVI) (1.37 g, 0.0085 mol) in carbon tetrachloride (40 mL), maintaining the temperature below -40°C. After 20 min, the yellow solution was poured into ice and was stirred for 10 min at RT. The mixture was extracted with EtOAc. 1M aqueous NaOH was added to the organic layer to adjust the pH=7. The organic layer was separated, and washed with water, dried over MgS04, and filtered, and the solvent was removed in vacuo to give an orange viscous oil. The oily residue was triturated with hexane to give pure 3,3-diMethyl-6-nitrobenzo[c][1,2]oxaborol-1(3H)-ol.3,3-diMethyl-6-nitrobenzo[c][1,2]oxaborol-1(3H)-ol

221352-10-9
1266084-47-2
Synthesis of 3,3-diMethyl-6-nitrobenzo[c][1,2]oxaborol-1(3H)-ol from 3,3-diMethylbenzo[c][1,2]oxaborol-1(3H)-ol

3,3-diMethyl-6-nitrobenzo[c][1,2]oxaborol-1(3H)-ol Preparation Products And Raw materials

3,3-diMethyl-6-nitrobenzo[c][1,2]oxaborol-1(3H)-ol Suppliers

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Shanghai Boc Chemical Co., Ltd.
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Shanghai Haohong Pharmaceutical Co., Ltd. 400-8210725 4008210725 malulu@leyan.com China 39997 58
3,3-diMethyl-6-nitrobenzo[c][1,2]oxaborol-1(3H)-ol 1,3-dihydro-1-hydroxy-3,3-dimethyl-6-nitro-2,1-Benzoxaborole 3,3-Dimethyl-6-Nitrobenzo[C][1,2]Oxaborol-1(3H)-Ol(WXC00403) 2,1-Benzoxaborole, 1,3-dihydro-1-hydroxy-3,3-dimethyl-6-nitro- 1266084-47-2