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Bromoacetaldehyde diethyl acetal

Bromoacetaldehyde diethyl acetal
Bromoacetaldehyde diethyl acetal structure
CAS No.
2032-35-1
Chemical Name:
Bromoacetaldehyde diethyl acetal
Synonyms
BADEA;NSC 8036;2032-35-1;Bromacetal;BROMOACETAL;-Bromodiethylacetal;Diethyl bromoacetal;BROMO ACETYL DIACETAL;2,2-DIETHOXYETHYL BROMIDE;1,1-DIETHOXY-2-BROMOETHANE
CBNumber:
CB4437547
Molecular Formula:
C6H13BrO2
Formula Weight:
197.07
MOL File:
2032-35-1.mol

Bromoacetaldehyde diethyl acetal Properties

Boiling point:
66-67 °C18 mm Hg(lit.)
Density 
1.31 g/mL at 25 °C(lit.)
refractive index 
n20/D 1.439(lit.)
Flash point:
125 °F
storage temp. 
0-6°C
Specific Gravity
1.310
Water Solubility 
immiscible
Sensitive 
Moisture Sensitive
BRN 
635754
InChIKey
LILXDMFJXYAKMK-UHFFFAOYSA-N
CAS DataBase Reference
2032-35-1(CAS DataBase Reference)
NIST Chemistry Reference
Ethane, 2-bromo-1,1-diethoxy-(2032-35-1)
EPA Substance Registry System
Ethane, 2-bromo-1,1-diethoxy- (2032-35-1)
SAFETY
  • Risk and Safety Statements
Symbol(GHS) 
GHS06,GHS02,GHS07
Signal word  Danger
Hazard statements  H226-H301+H331-H227-H335-H301-H315-H319-H330
Precautionary statements  P260-P304+P340+P310-P305+P351+P338-P403+P233-P210-P233-P240-P241+P242+P243-P261-P264-P270-P271-P280-P301+P310+P330-P302+P352+P332+P313+P362+P364-P304+P340+P311-P305+P351+P338+P337+P313-P405-P501-P301+P310a-P304+P340-P320-P330-P501a
Hazard Codes  Xi,T
Risk Statements  10-36-36/38-23-22
Safety Statements  16-26-45-38-37/39-28A-36/37
RIDADR  UN 1993 3/PG 3
WGK Germany  3
8-9-21
Hazard Note  Toxic/Irritant
TSCA  Yes
HazardClass  6.1
PackingGroup  III
HS Code  29110000
NFPA 704
2
1 0

Bromoacetaldehyde diethyl acetal price More Price(9)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Sigma-Aldrich 123986 Bromoacetaldehyde diethyl acetal 97% 2032-35-1 100g $31.9 2020-08-18 Buy
Sigma-Aldrich 123986 Bromoacetaldehyde diethyl acetal 97% 2032-35-1 1kg $228 2020-08-18 Buy
TCI Chemical B0957 Bromoacetaldehyde Diethyl Acetal >95.0%(GC) 2032-35-1 25mL $19 2020-06-24 Buy
TCI Chemical B0957 Bromoacetaldehyde Diethyl Acetal >95.0%(GC) 2032-35-1 100mL $41 2020-06-24 Buy
Alfa Aesar A13276 Bromoacetaldehyde diethyl acetal, 97% 2032-35-1 500g $95.4 2020-06-24 Buy

Bromoacetaldehyde diethyl acetal Chemical Properties,Uses,Production

Chemical Properties

Colorless to light yellow liqui

Uses

Synthetic building block1,2

Preparation

To a flask containing 118.0 gm (1.0 mole) of diethyl acetal and 55 gm (0.55 mole) of calcium carbonate is dropwise added 55 ml (1.0 mole) of bromine over a 30-45 min period while keeping the reaction temperature at 5°-10°C. The reaction mixture is allowed to stand 24 hr, steam is introduced to dissolve the salts, the oil separated, dried over potassium carbonate, and distilled to afford 61-83 gm (31-42%), b.p. 167°-170°C. The product is further purified by shaking with potassium carbonate and distilling it under reduced pressure, b.p. 48°-49°C (3 mm Hg). The pure acetal is unstable and becomes colored in a few hours and black after several days. However, the crude acetal boiling at 167°-170°C is stable for several months.
Preparation of Bromoacetaldehyde Diethyl Acetal

Bromoacetaldehyde diethyl acetal Preparation Products And Raw materials

Raw materials

Preparation Products


Bromoacetaldehyde diethyl acetal Suppliers

Global( 364)Suppliers
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Capot Chemical Co.,Ltd.
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View Lastest Price from Bromoacetaldehyde diethyl acetal manufacturers

Image Release date Product Price Min. Order Purity Supply Ability Manufacturer
2018-08-06 Bromoacetaldehyde diethyl acetal
2032-35-1
US $1.00 / KG 1KG 98% 200KG career henan chemical co

Bromoacetaldehyde diethyl acetal Spectrum


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