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3,4-Dimethoxyacetophenone

3,4-Dimethoxyacetophenone structure

CAS No.: 1131-62-0

Chemical Name:: 3,4-Dimethoxyacetophenone

Synonyms: 1-(3,4-DIMETHOXYPHENYL)ETHAN-1-ONE;3',4'-DIMETHOXYACETOPHENONE;ACETOVERATRONE;3,4-Dimethoxyacetophenon;3,4-Dimethoxyacetoph;Dimethoxyacetophenone;1-(3,4-DIMETHOXYPHENYL)-ETHANONE;KML-86;KML-118;AKOS 220-35

CBNumber:: CB6350428

Molecular Formula:: C10H12O3

Molecular Weight:: 180.2

MDL Number:: MFCD00008737

MOL File:: 1131-62-0.mol

MSDS File:: SDS

Last updated:2024-04-25 17:59:01

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3,4-Dimethoxyacetophenone Properties

Melting point	47-54 °C(lit.)
Boiling point	286-288 °C(lit.)
Density	1.1272 (rough estimate)
refractive index	1.5224 (estimate)
Flash point	>230 °F
storage temp.	Sealed in dry,Room Temperature
solubility	hot water: soluble
form	Crystalline Powder
color	Yellow to beige
Odor	at 10.00 % in dipropylene glycol. sweet woody floral
Odor Type	woody
Water Solubility	SOLUBLE IN HOT WATER
BRN	781213
LogP	1.822 (est)
CAS DataBase Reference	1131-62-0(CAS DataBase Reference)
FDA UNII	5RV6436S8A
NIST Chemistry Reference	Ethanone, 1-(3,4-dimethoxyphenyl)-(1131-62-0)
EPA Substance Registry System	Ethanone, 1-(3,4-dimethoxyphenyl)- (1131-62-0)

SAFETY

Risk and Safety Statements

Symbol(GHS)

GHS07

Signal word

Warning

Hazard statements

H315-H319-H335

Precautionary statements

P261-P280-P271

Hazard Codes

Safety Statements

24/25

WGK Germany

TSCA

Yes

HS Code

29145000

NFPA 704

	1
2		0

3,4-Dimethoxyacetophenone price More Price(32)

Manufacturer	Product number	Product description	CAS number	Packaging	Price	Updated	Buy
Sigma-Aldrich	156639	3′,4′-Dimethoxyacetophenone 98%	1131-62-0	25g	$62.2	2024-03-01	Buy
Sigma-Aldrich	156639	3′,4′-Dimethoxyacetophenone 98%	1131-62-0	100g	$199	2024-03-01	Buy
TCI Chemical	D1878	3',4'-Dimethoxyacetophenone >98.0%(GC)	1131-62-0	25g	$48	2024-03-01	Buy
TCI Chemical	D1878	3',4'-Dimethoxyacetophenone >98.0%(GC)	1131-62-0	100g	$122	2024-03-01	Buy
Alfa Aesar	L02737	3',4'-Dimethoxyacetophenone, 98+%	1131-62-0	50g	$40.65	2024-03-01	Buy

Product number	Packaging	Price	Buy
156639	25g	$62.2	Buy
156639	100g	$199	Buy
D1878	25g	$48	Buy
D1878	100g	$122	Buy
L02737	50g	$40.65	Buy

3,4-Dimethoxyacetophenone Chemical Properties,Uses,Production

Synthesis

To a stirred mixture of 3´,4´-dihydroxyacetophenone (100 mg, 0.66 mmol) and anhydrous K2CO3 (5 g, 36 mmol) in dry acetone (10 mL) was added MeI (1 mL, 16 mmol). The mixture was heated at reflflux for 45 min, cooled to room temperature, fifiltered, and evaporated under reduced pressure. The residue was dissolved in CH2Cl2, washed with 2 portions of water, dried over anhydrous Na2SO4, and evaporated under reduced pressure. The product was purifified by flflash chromatography (silica, hexane/EtOAc 4:1, v/v). Removal of the solvent gave a 93% yield of the product, 3´,4´-dimethoxyacetophenone (110 mg, 0.61 mmol). Reference: Khatib, S.; Nerya, O.; Musa, R.; Shmuel, M.; Tamir, S.; Vaya, J. Bioorg. Med. Chem. 2005, 13, 433−441.

Chemical Properties

yellow to beige crystalline powder

Uses

3',4'-Dimethoxyacetophenone is used as Catalytic agent; Petrochemical additive. It is also used in agrochemical, pharmaceutical and dyestuff field.

Preparation

Obtained by reaction of dimethyl sulfate with acetoguaiacone in the presence of sodium hydroxide in ethanol, first at 50°, then at reflux for 1 h (78%).

Definition

ChEBI: A member of the class of acetophenones that is acetophenone substituted by methoxy groups at positions 3' and 4' respectively.

Synthesis Reference(s)

Tetrahedron Letters, 36, p. 409, 1995 DOI: 10.1016/0040-4039(94)02221-V

3,4-Dimethoxyacetophenone Preparation Products And Raw materials

Raw materials

Preparation Products

4-Aminoveratrole 1,2-DIMETHOXY-4-ETHYLBENZENE 4-chloro-6,7-dimethoxyquinoline 2'-HYDROXY-3',4'-DIMETHOXYACETOPHENONE veratrylglycerol-beta-guaiacyl ether

2'-AMINO-4',5'-DIMETHOXYACETOPHENONE 1-(4,5-DIMETHOXY-2-NITRO-PHENYL)-ETHANONE 4-METHOXY-3-HYDROXYACETOPHENONE 2,6-Dimethoxyphenol 1,2-Dimethoxybenzene

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3,4-Dimethoxyacetophenone Suppliers

Global( 381)Suppliers

Supplier	Tel	Email	Country	ProdList	Advantage
Hebei Mojin Biotechnology Co., Ltd	+8613288715578	sales@hbmojin.com	China	12456	58
Hebei Guanlang Biotechnology Co,.LTD	+8619930503252	daisy@crovellbio.com	China	5964	58
Firsky International Trade (Wuhan) Co., Ltd	+8615387054039	admin@firsky-cn.com	China	436	58
Capot Chemical Co.,Ltd.	571-85586718 +8613336195806	sales@capotchem.com	China	29797	60
Shanghai Daken Advanced Materials Co.,Ltd	+86-371-66670886	info@dakenam.com	China	15928	58
Henan Tianfu Chemical Co.,Ltd.	+86-0371-55170693 +86-19937530512	info@tianfuchem.com	China	21691	55
ATK CHEMICAL COMPANY LIMITED	+undefined-21-51877795	ivan@atkchemical.com	China	32480	60
career henan chemical co	+86-0371-86658258	sales@coreychem.com	China	29914	58
SHANDONG ZHI SHANG CHEMICAL CO.LTD	+86 18953170293	sales@sdzschem.com	China	2931	58
Jinan Finer Chemical Co., Ltd	+86-531-88989536 +86-15508631887	sales@finerchem.com	China	2967	58

Supplier	Advantage
Hebei Mojin Biotechnology Co., Ltd	58
Hebei Guanlang Biotechnology Co,.LTD	58
Firsky International Trade (Wuhan) Co., Ltd	58
Capot Chemical Co.,Ltd.	60
Shanghai Daken Advanced Materials Co.,Ltd	58
Henan Tianfu Chemical Co.,Ltd.	55
ATK CHEMICAL COMPANY LIMITED	60
career henan chemical co	58
SHANDONG ZHI SHANG CHEMICAL CO.LTD	58
Jinan Finer Chemical Co., Ltd	58

View Lastest Price from 3,4-Dimethoxyacetophenone manufacturers

Update time	Product	Price	Min. Order	Purity	Supply Ability	Manufacturer
2024-04-25	3,4-Dimethoxyacetophenone 1131-62-0	US $10.00 / kg	1kg	99.8%	10000ton	Ouhuang Engineering Materials (Hubei) Co., Ltd
2023-10-08	3,4-Dimethoxyacetophenone 1131-62-0	US $30.00 / KG	1KG	99%	20T	Firsky International Trade (Wuhan) Co., Ltd
2023-08-25	3,4-Dimethoxyacetophenone 1131-62-0	US $30.00-10.00 / kg	10kg	99%	100000kg	Hebei Guanlang Biotechnology Co,.LTD

3,4-Dimethoxyacetophenone
1131-62-0
US $10.00 / kg
99.8%
Ouhuang Engineering Materials (Hubei) Co., Ltd

3,4-Dimethoxyacetophenone
1131-62-0
US $30.00 / KG
99%
Firsky International Trade (Wuhan) Co., Ltd

3,4-Dimethoxyacetophenone
1131-62-0
US $30.00-10.00 / kg
99%
Hebei Guanlang Biotechnology Co,.LTD

3,4-Dimethoxyacetophenone Spectrum

3,4-Dimethoxyacetophenone(1131-62-0)MS 3,4-Dimethoxyacetophenone(1131-62-0)¹HNMR 3,4-Dimethoxyacetophenone(1131-62-0)¹³CNMR 3,4-Dimethoxyacetophenone(1131-62-0)IR1 3,4-Dimethoxyacetophenone(1131-62-0)IR2 3,4-Dimethoxyacetophenone(1131-62-0)Raman

1131-62-0(3,4-Dimethoxyacetophenone)Related Search:

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3',5'-DIMETHOXYACETOPHENONE,3,5-DIMETHOXYACETOPHENONE,3',5'-Dimethoxyacetophenone 3,5-Dimethoxyacetophenone 2',3',4'-TRIMETHOXYACETOPHENONE 6-Acetyl-1,4-benzodioxane

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3,4-DIMETHOXYACETOPHENONE FOR SYNTHESIS 3,4-Dimethoxyacetophenone≥ 99% (GC) 3,4-DIMETHOXYACETOPHENONE 3,4-dimethoxyacetophenone (acetoveratrone) 3',4'-Dimethoxyacetophenone 1-(3,4-Dimethoxyphenyl)ethan-1-one 3,4-Dimethoxyacetophenone 3,4-dimethoxyacetophene 1-(3,4-Dimethoxyphenyle)ethane-1-one Acetyl veratrole 3' 4'-DIMETHOXYACETOPHENONE 98+% ACETYL VERATROL ACETOVERATRONE(RG) 1-(3,4-dimethoxyphenyl)-ethanon LABOTEST-BB LT00000195 3,4-Dimethoxyphenyl methyl ketone 3,4-Dimethoxyphenylmethylketone Acetophenone, 3',4'-dimethoxy- Acetophenone,3’,4’-dimethoxy- Ethanone,1-(3,4-dimethoxyphenyl)- Methyl3,4-dimethoxyphenylketone 1-(3,4-DIMETHOXYPHENYL)-ETHANO ACETOVERATRON AKOS 220-35 AKOS BBS-00003221 4-ACETYLPYROCATECHOL DIMETHYL ETHER 4-ACETYLVERATROLE 3',4'-Dimethoxyacetophenone> KML-86 Dimethoxyacetophenone 3,4-Dimethoxyacetoph 3',4'-DIMETHOXYACETOPHENONE 3,4-Dimethoxyacetophenon 1-(3,4-DIMETHOXYPHENYL)-ETHANONE 1-(3,4-DIMETHOXYPHENYL)ETHAN-1-ONE ACETOVERATRONE 3',4'-Dimethoxyacetophenone1131-62-0 KML-118 Compound PDK0029 3,4-DChemicalbookIMETHOXYACETOPHENONE 3',4'-Dimethoxyacetophenone 1131-62-0 1131-62-7 KETONE Ketones Organic Building Blocks Building Blocks C10 Carbonyl Compounds Alphabetical Listings C-D Flavors and Fragrances C10 Carbonyl Compounds Ketones Benzene derivatives Aromatic Acetophenones & Derivatives (substituted) 1131-62-0