6-O-BETA-D-GLUCOPYRANOSYL-D-GLUCOPYRANOSE
- CAS No.
- 5996-00-9
- Chemical Name:
- 6-O-BETA-D-GLUCOPYRANOSYL-D-GLUCOPYRANOSE
- Synonyms
- GENTIOBIOSE;B-GENTIOBIOSE;β-Gentiobiose;GENTIOBIOSE, B-;BETA-GENTIOBIOSE;BETA-D-GENTIOBIOSE;GENTIOBIOSE, B-(RG);6-O-b-D-Glucopyranosyl-b-D-glucopyranose;6-O-BETA-D-GLUCOPYRANOSYL-D-GLUCOPYRANOSE;β-D-Glucopyranose, 6-O-β-D-glucopyranosyl-
- CBNumber:
- CB7135840
- Molecular Formula:
- C12H22O11
- Molecular Weight:
- 342.3
- MDL Number:
- MFCD00198061
- MOL File:
- 5996-00-9.mol
- MSDS File:
- SDS
| Melting point | 190 °C |
|---|---|
| Boiling point | 662.8±55.0 °C(Predicted) |
| Density | 1.57 g/cm3 |
| pka | 12.10±0.70(Predicted) |
| LogP | -3.200 (est) |
| FDA UNII | N2VA1H3TIQ |
SAFETY
Risk and Safety Statements
| Safety Statements | 24/25 |
|---|
6-O-BETA-D-GLUCOPYRANOSYL-D-GLUCOPYRANOSE price More Price(3)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| American Custom Chemicals Corporation | CRB0001210 | BETA-GENTIOBIOSE 95.00% | 5996-00-9 | 1G | $715.75 | 2021-12-16 | Buy |
| American Custom Chemicals Corporation | CRB0001210 | BETA-GENTIOBIOSE 95.00% | 5996-00-9 | 5G | $1034.53 | 2021-12-16 | Buy |
| American Custom Chemicals Corporation | CRB0001210 | BETA-GENTIOBIOSE 95.00% | 5996-00-9 | 10G | $1534.3 | 2021-12-16 | Buy |
6-O-BETA-D-GLUCOPYRANOSYL-D-GLUCOPYRANOSE Chemical Properties,Uses,Production
Definition
ChEBI: Beta-D-Glcp-(1->6)-beta-D-Glcp is a glycosylglucose in which two beta-D-glucose residues are linked (1->6). It has a role as an epitope.
Purification Methods
-Gentiobiose is best purified via the octaacetate which is recrystallised from MeOH, EtOH or better from methyl cellosolve by heating at 80o. The octaacetate (15g) is hydrolysed by suspending it in dry 0.05N NaOMe in MeOH (180mL) for 1hour with occasional shaking at room temperature. Dilute this with H2O to dissolve suspended matter, pass through Amberlite IR-120 and Duolite A-4 columns and the eluate is evaporated under reduced pressure to a syrup. Residual H2O is removed by repeated distillation with absolute EtOH under reduced pressure. The syrup is dissolved in methyl cellosolve (~40mL), filtered, nucleated and placed in an oven at 80o. The crystals are filtered off, washed with absolute EtOH (yield 6.7g, 89%), dried and have m 187-189o. Further recrystallisation from methyl cellosolve gives m 190o, and mutarotates from [] D 28 -1.5o (initial) to +10.6o (final, c 4, H2O). The -octaacetate has m 193o (crystallised from 95% EtOH) and has [] D 20 -5o (c 1.8, CHCl3). [Goldstein & Whelan Methods in Carbohydrate Chemistry I 313 1962, Academic Press, Beilstein 17/7 V 203.]
6-O-BETA-D-GLUCOPYRANOSYL-D-GLUCOPYRANOSE Preparation Products And Raw materials
Raw materials
Preparation Products
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Xi'an Kono chem co., Ltd., | 029-86107037 13289246953 | info@konochemical.com | China | 2995 | 58 |
| Shanghai Jizhi Biochemical Technology Co. Ltd. | 400-400-400-9004166 18616739031 | 3007523370@qq.com | China | 52712 | 58 |
| Beijing OKA biological technology co., LTD | 010-62971590 18548936886 | 3462612863@qq.com | China | 6912 | 58 |
| Shenzhen Polymeri Biochemical Technology Co., Ltd. | +86-400-002-6226 13028896684 | sales@rrkchem.com | China | 55717 | 58 |
| Jiangsu aikang biomedical research and development co., LTD | 025-66110311 13155353615 | qzhang@aikonchem.com | China | 15527 | 58 |
| cjbscvictory | 13348960310 13348960310 | 3003867561@qq.com | China | 9946 | 58 |
| Foshan Treasure Biotechnology Co., Ltd | 0757-85921206 18520245316 | 2329783215@qq.com | China | 12664 | 58 |
| Shanghai Haohong Scientific Co., Ltd. | 400-400-8210725 | malulu@leyan.com | China | 40041 | 58 |
| Nanjing Shizhou Biology Technology Co.,Ltd | 025-85560043 15850508050 | rose.shi@synzest.com | China | 5889 | 58 |