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3,5-Bis(trifluoromethyl)benzyl bromide

3,5-Bis(trifluoromethyl)benzyl bromide structure

CAS No.: 32247-96-4

Chemical Name:: 3,5-Bis(trifluoromethyl)benzyl bromide

Synonyms: 1-(BROMOMETHYL)-3,5-BIS(TRIFLUOROMETHYL)BENZENE;5-Bis(trifluoroMethyl)benzyl broMide;3,5-Bis(trifluoremethyl)benzylbromide;3,5-BIS(TRIFLUOROMETHYL)BENZYL BROMIDE;3,5-DI(TRIFLUORO METHYL)BENZYL BROMIDE;3,5-Bis(trifluoromethyl)benzylbromiode;3,5-Bis(trifluoromethyl)benzylbromide98%;3,5-Bis(trifluoromethyl)benzyl bromide 98%;3,5-Bis(trifluoromethyl)benzyl Bromide >3,5-Bis(trifluoromethyl)benzyl bromide, 97+%

CBNumber:: CB8709789

Molecular Formula:: C9H5BrF6

Molecular Weight:: 307.03

MDL Number:: MFCD00009905

MOL File:: 32247-96-4.mol

MSDS File:: SDS

Last updated:2023-12-25 17:47:29

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3,5-Bis(trifluoromethyl)benzyl bromide Properties

Melting point	18°C
Boiling point	136-140°C 14mm
Density	1.675 g/mL at 25 °C(lit.)
refractive index	n20/D 1.445(lit.)
Flash point	79 °F
storage temp.	Inert atmosphere,2-8°C
solubility	Difficult to mix.
form	Liquid
color	Clear colorless to yellow-brown
Specific Gravity	1.675
Sensitive	Lachrymatory
BRN	656506
CAS DataBase Reference	32247-96-4(CAS DataBase Reference)
NIST Chemistry Reference	3,5-Bis(trifluoromethyl)benzyl bromide(32247-96-4)

SAFETY

Risk and Safety Statements

Symbol(GHS)

GHS02,GHS05

Signal word

Danger

Hazard statements

H226-H314

Precautionary statements

P210-P233-P240-P280-P303+P361+P353-P305+P351+P338

Hazard Codes

C,F

Risk Statements

10-34

Safety Statements

26-36/37/39-45-25-16

RIDADR

UN 2920 8/PG 2

WGK Germany

Hazard Note

Corrosive/Lachrymatory

HazardClass

PackingGroup

III

HS Code

29039990

NFPA 704

	3
3		0

3,5-Bis(trifluoromethyl)benzyl bromide price More Price(33)

Manufacturer	Product number	Product description	CAS number	Packaging	Price	Updated	Buy
Sigma-Aldrich	263397	3,5-Bis(trifluoromethyl)benzyl bromide 97%	32247-96-4	1g	$26.5	2024-03-01	Buy
Sigma-Aldrich	263397	3,5-Bis(trifluoromethyl)benzyl bromide 97%	32247-96-4	5g	$63	2024-03-01	Buy
TCI Chemical	B1867	3,5-Bis(trifluoromethyl)benzyl Bromide >96.0%(GC)	32247-96-4	5g	$37	2024-03-01	Buy
TCI Chemical	B1867	3,5-Bis(trifluoromethyl)benzyl Bromide >96.0%(GC)	32247-96-4	25g	$146	2024-03-01	Buy
Alfa Aesar	A19590	3,5-Bis(trifluoromethyl)benzyl bromide, 98%	32247-96-4	1g	$37.6	2021-12-16	Buy

Product number	Packaging	Price	Buy
263397	1g	$26.5	Buy
263397	5g	$63	Buy
B1867	5g	$37	Buy
B1867	25g	$146	Buy
A19590	1g	$37.6	Buy

3,5-Bis(trifluoromethyl)benzyl bromide Chemical Properties,Uses,Production

Chemical Properties

White or Colorles to Yellow to Orange powder to lump to clear liquid

Uses

3,5-Bis(trifluoromethyl)benzyl bromide is used as derivatization reagent in detection of uracil in DNA by GC and negative chemical ionization mass spectrometry in enantioselective synthesis of non-peptidic neurokinin NK1 receptor antagonist.

Synthesis

Synthesis of 3, 5-bis (trifluoromethyl)-benzyl bromide:
In a 4-neck flask with capacity 1000 ml equipped with mechanical agitator, thermometer, bubble condenser and 100 ml loading funnel, 262.2 g of the product of Example 1 (ii) at 92. 8% (0. 988 moles), 550,2 g HBr 48% (3.2645 moles) are loaded; this is heated at 50°C so as to melt the alcohol, then one starts to dose 113 g of concentrated His04 (1.153 moles). Pouring is accomplished in 30 minutes, noting an increase of the internal temperature. This is heated to 100-105°C and left to react for 8 hours. The reaction is completed by reflux heating for per 1.5 hours. the mixture is left to settle and the phases are separated; the solvents are removed from the organic phase and the product in the title is obtained with a yield of 99.1 %.
Synthesis of 3, 5-bis (trifluoromethyl)-benzyl bromide.png

3,5-Bis(trifluoromethyl)benzyl bromide Preparation Products And Raw materials

Raw materials

Preparation Products

3,5-Bis(trifluoromethyl)benzyl bromide Suppliers

Global( 290)Suppliers

Supplier	Tel	Email	Country	ProdList	Advantage
Henan Fengda Chemical Co., Ltd	+86-371-86557731 +86-13613820652	info@fdachem.com	China	7845	58
Capot Chemical Co.,Ltd.	571-85586718 +8613336195806	sales@capotchem.com	China	29797	60
Henan Tianfu Chemical Co.,Ltd.	+86-0371-55170693 +86-19937530512	info@tianfuchem.com	China	21691	55
career henan chemical co	+86-0371-86658258	sales@coreychem.com	China	29914	58
Changzhou Ansciep Chemical Co., Ltd.	+86 519 86305871	sales@ansciepchem.com	CHINA	4242	58
Hubei xin bonus chemical co. LTD	86-13657291602	linda@hubeijusheng.com	CHINA	22968	58
Alchem Pharmtech,Inc.	8485655694	sales@alchempharmtech.com	United States	63711	58
Wuhan Chemwish Technology Co., Ltd	027-67849912	sales@chemwish.com	CHINA	10828	58
CONIER CHEM AND PHARMA LIMITED	+8618523575427	sales@conier.com	China	49390	58
Shaanxi Dideu Medichem Co. Ltd	+86-029-81148696 +8615536356810	1047@dideu.com	China	3408	58

Supplier	Advantage
Henan Fengda Chemical Co., Ltd	58
Capot Chemical Co.,Ltd.	60
Henan Tianfu Chemical Co.,Ltd.	55
career henan chemical co	58
Changzhou Ansciep Chemical Co., Ltd.	58
Hubei xin bonus chemical co. LTD	58
Alchem Pharmtech,Inc.	58
Wuhan Chemwish Technology Co., Ltd	58
CONIER CHEM AND PHARMA LIMITED	58
Shaanxi Dideu Medichem Co. Ltd	58

View Lastest Price from 3,5-Bis(trifluoromethyl)benzyl bromide manufacturers

Update time	Product	Price	Min. Order	Purity	Supply Ability	Manufacturer
2023-12-26	3,5-Bis(trifluoromethyl)benzyl bromide 32247-96-4	US $100.00-1.00 / KG	1KG	99%	g-kg-tons, free sample is available	Henan Fengda Chemical Co., Ltd
2022-09-16	3,5-Bis(trifluoromethyl)benzyl bromide 32247-96-4	US $0.00-0.00 / kg	1kg	98%	1Ton	Henan Aochuang Chemical Co.,Ltd.
2020-01-08	3,5-Bis(trifluoromethyl)benzyl bromide 32247-96-4	US $0.10 / KG	1KG	99.0%	1000 tons	Shaanxi Dideu Medichem Co. Ltd

3,5-Bis(trifluoromethyl)benzyl bromide
32247-96-4
US $100.00-1.00 / KG
99%
Henan Fengda Chemical Co., Ltd

3,5-Bis(trifluoromethyl)benzyl bromide
32247-96-4
US $0.00-0.00 / kg
98%
Henan Aochuang Chemical Co.,Ltd.

3,5-Bis(trifluoromethyl)benzyl bromide
32247-96-4
US $0.10 / KG
99.0%
Shaanxi Dideu Medichem Co. Ltd

3,5-Bis(trifluoromethyl)benzyl bromide Spectrum

3,5-Bis(trifluoromethyl)benzyl bromide(32247-96-4)MS 3,5-Bis(trifluoromethyl)benzyl bromide(32247-96-4)¹HNMR 3,5-Bis(trifluoromethyl)benzyl bromide(32247-96-4)¹³CNMR 3,5-Bis(trifluoromethyl)benzyl bromide(32247-96-4)IR1 3,5-Bis(trifluoromethyl)benzyl bromide(32247-96-4)Raman

32247-96-4(3,5-Bis(trifluoromethyl)benzyl bromide)Related Search:

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3,5-Bis(trifluoromethyl)benzyl bromide, 97+% 5-Bis(trifluoroMethyl)benzyl broMide 3,5-Bis(trifluoremethyl)benzylbromide 1,3-Bis(trifluoromethyl)-5-(bromomethyl)benzene 3,5-Bis(trifluoromethyl)benzylbromiode {[3,5-bis(trifluoroMethyl)phenyl]Methyl}broManuide 3,5-Bis(trifluoroMethyl)benzyl broMide, 97% 1GR Benzene,1-(broMoMethyl)-3,5-bis(trifluoroMethyl)- 3, 5 - double three fluorinated Methyl benzyl broMide 3,5-DI(TRIFLUORO METHYL)BENZYL BROMIDE 3,5-BIS(TRIFLUOROMETHYL)BENZYL BROMIDE 1-(BROMOMETHYL)-3,5-DI(TRIFLUOROMETHYL)BENZENE 3,5-Di(Trifluoro Methyl)Benzyl Bromide 3,5-bis(Trifluoromethyl)benzyl Bromide 3,5-Bis(trifluoromethyl)benzyl bromide 98% 3,5-Bis(trifluoromethyl)benzylbromide98% 1-(Bromomethyl)-3,5-bis(trifluoromethyl)benzene1,3-Ditrifluoromethyl-5-bromobenzene 3,5-Bis(trifluoromethyl)benzyl Bromide > 3,5-Bis(trifluoromethyl)benzyl bromide ISO 9001：2015 REACH 1-(BROMOMETHYL)-3,5-BIS(TRIFLUOROMETHYL)BENZENE 32247-96-4 CF32C6H3CH2Br C9H5BrF6 Organic Building Blocks Halogenated Hydrocarbons Building Blocks C9 to C12 Aryl Aromatic Halides (substituted) Fluorides