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9-phenylanthracene

9-phenylanthracene structure

CAS No.: 602-55-1

Chemical Name:: 9-phenylanthracene

Synonyms: NSC 90796;9-phenylantracene;9-PHENYLANTHRACENE;Phenylanthracene,98%;anthracene,9-phenyl-;9-Phenylanthracene97%;9-Phenylanthracene>9-Phenylanthracene,98%;9-Phenylanthracene 97%;9-PHENYLANTHRACENE OEKANAL

CBNumber:: CB8778824

Molecular Formula:: C20H14

Molecular Weight:: 254.33

MDL Number:: MFCD00001252

MOL File:: 602-55-1.mol

MSDS File:: SDS

Last updated:2023-11-08 17:00:29

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9-phenylanthracene Properties

Melting point	153-155 °C (lit.)
Boiling point	417 °C (lit.)
Density	1.1180 (estimate)
refractive index	1.7040 (estimate)
storage temp.	Sealed in dry,Room Temperature
solubility	Chloroform (Slightly), Ethyl Acetate (Slightly)
form	Solid
color	Off-white to pale brown
Sensitive	Light Sensitive
BRN	1910570
CAS DataBase Reference	602-55-1(CAS DataBase Reference)
FDA UNII	DC63Z5S1UP
EPA Substance Registry System	Anthracene, 9-phenyl- (602-55-1)

SAFETY

Risk and Safety Statements

Symbol(GHS)

GHS09

Signal word

Warning

Hazard statements

H410

Precautionary statements

P273-P501

Hazard Codes

Risk Statements

50/53

Safety Statements

60-61

RIDADR

UN 3077 9/PG 3

WGK Germany

HazardClass

HS Code

29029090

NFPA 704

	1
0		0

9-phenylanthracene price More Price(19)

Manufacturer	Product number	Product description	CAS number	Packaging	Price	Updated	Buy
Sigma-Aldrich	P18004	9-Phenylanthracene 98%	602-55-1	5g	$183.6	2024-03-01	Buy
Sigma-Aldrich	P18004	9-Phenylanthracene 98%	602-55-1	1g	$86.3	2023-06-20	Buy
TCI Chemical	P0138	9-Phenylanthracene >98.0%(GC)	602-55-1	1g	$113	2024-03-01	Buy
TCI Chemical	P0138	9-Phenylanthracene >98.0%(GC)	602-55-1	5g	$394	2024-03-01	Buy
Alfa Aesar	H64419	9-Phenylanthracene, 98%	602-55-1	1g	$23.8	2021-12-16	Buy

Product number	Packaging	Price	Buy
P18004	5g	$183.6	Buy
P18004	1g	$86.3	Buy
P0138	1g	$113	Buy
P0138	5g	$394	Buy
H64419	1g	$23.8	Buy

9-phenylanthracene Chemical Properties,Uses,Production

Chemical Properties

Pale Yellow Plates

Uses

9-Phenylanthracene is used to synthesize organic light-emitting material intermediates.

Preparation

The synthesis of 9-phenylanthracene involved mixing phenylboronic acid (2.13 g, 17.49 mmol), 9-bromoanthracene (3 g, 11.66 mmol), Pd(PPh3)4 (140 mg, 0.12 mmol), K2CO3 (16 mL, 2 M), and ethanol (8 mL) in a 100 mL flask with anhydrous toluene (32 mL). The mixture was refluxed for 48 h under nitrogen. After cooled to room temperature, the reaction mixture was quenched with dilute hydrochloric acid solution and extracted with CH2Cl2. The organic extracts were dried over anhydrous MgSO4 and concentrated by rotary evaporation. The crude product was further purified by silica gel column chromatography (CH2Cl2/petroleum ether (1:4,v/v)) to get a white powder (2.43 g, 81.9 %). 1H NMR (500 MHz, CDCl3) δ 8.53 (s, 1H), 8.08 (d, J = 8.5 Hz, 2H), 7.70 – 7.67 (m, 2H), 7.63 – 7.54 (m, 3H), 7.50 – 7.45 (m, 4H), 7.37 (ddd, J = 8.7, 6.5, 1.2 Hz, 2H). EI-MS (m/z): Calculated for C20H14: 254.33. Found [M+]: 253.02.
preparation of 9-phenylanthracene
Synthesis of 9-phenylanthracene

Synthesis Reference(s)

Journal of the American Chemical Society, 79, p. 393, 1957 DOI: 10.1021/ja01559a042

Purification Methods

Chromatograph it on alumina in *C6H6 and recrystallise it from AcOH or toluene. [Beilstein 5 H 725, 5 II 639, 5 III 2462.]

9-phenylanthracene Preparation Products And Raw materials

Raw materials

Anthrone Bromobenzene Magnesium Phenylboronic acid 9-Bromoanthracene

Tetrakis(triphenylphosphine)palladium Potassium carbonate Ethanol

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Preparation Products

9-phenylanthracene Suppliers

Global( 176)Suppliers

Supplier	Tel	Email	Country	ProdList	Advantage
Hebei Xinsheng New Material Technology Co., LTD.	+86-16632316109	xinshengkeji@xsmaterial.com	China	1100	58
Springchem New Material Technology Co.,Limited	+86-021-62885108 +8613917661608	info@spring-chem.com	China	2068	57
Shanghai Daken Advanced Materials Co.,Ltd	+86-371-66670886	info@dakenam.com	China	15928	58
ATK CHEMICAL COMPANY LIMITED	+undefined-21-51877795	ivan@atkchemical.com	China	32480	60
AB PharmaTech,LLC	323-480-4688		United States	989	55
Beijing Green Guardee Technology Co., Ltd	86-010-69706062	sales2@greenguardee.com	CHINA	650	58
career henan chemical co	+86-0371-86658258	sales@coreychem.com	China	29914	58
Xiamen AmoyChem Co., Ltd	+86-592-6051114 +8618959220845	sales@amoychem.com	China	6387	58
BAYNOE CHEM CO.,LTD	+86-21-34783353 +8615000719740	baynoe@baynoe.com	CHINA	934	58
Chongqing Chemdad Co., Ltd	+86-023-61398051 +8613650506873	sales@chemdad.com	China	39916	58

Supplier	Advantage
Hebei Xinsheng New Material Technology Co., LTD.	58
Springchem New Material Technology Co.,Limited	57
Shanghai Daken Advanced Materials Co.,Ltd	58
ATK CHEMICAL COMPANY LIMITED	60
AB PharmaTech,LLC	55
Beijing Green Guardee Technology Co., Ltd	58
career henan chemical co	58
Xiamen AmoyChem Co., Ltd	58
BAYNOE CHEM CO.,LTD	58
Chongqing Chemdad Co., Ltd	58

View Lastest Price from 9-phenylanthracene manufacturers

Update time	Product	Price	Min. Order	Purity	Supply Ability	Manufacturer
2024-01-23	9-PHENYLANTHRACENE 602-55-1	US $0.00 / KG	1KG	98.00%	150KG /month	Shanghai Daken Advanced Materials Co.,Ltd
2023-11-08	9-Phenylanthracene 602-55-1	US $0.00-0.00 / kg	1kg	99.9%	30000 KG	Hebei Xinsheng New Material Technology Co., LTD.
2023-09-23	9-phenylanthracene 602-55-1	US $35.00-25.00 / kg	1kg	99%	20 Ton	Hebei Xinsheng New Material Technology Co., LTD.

9-PHENYLANTHRACENE
602-55-1
US $0.00 / KG
98.00%
Shanghai Daken Advanced Materials Co.,Ltd

9-Phenylanthracene
602-55-1
US $0.00-0.00 / kg
99.9%
Hebei Xinsheng New Material Technology Co., LTD.

9-phenylanthracene
602-55-1
US $35.00-25.00 / kg
99%
Hebei Xinsheng New Material Technology Co., LTD.

9-phenylanthracene Spectrum

9-phenylanthracene(602-55-1)MS 9-phenylanthracene(602-55-1)¹HNMR 9-phenylanthracene(602-55-1)¹³CNMR 9-phenylanthracene(602-55-1)IR1 9-phenylanthracene(602-55-1)IR2 9-phenylanthracene(602-55-1)Raman

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