4-(Iodomethyl)tetrahydro-2H-pyran
- CAS No.
- 101691-94-5
- Chemical Name:
- 4-(Iodomethyl)tetrahydro-2H-pyran
- Synonyms
- 4-(iodomethyl)oxane;4-IODOMETHYLTETRAHYDROPYRAN;4-(Iodomethyl)tetrahydropyrane;4-(IODOMETHYL)TETRAHYDRO-2H-PYRAN;(4-TETRAHYDROPYRANYL)METHYL IODIDE;Tetrahydro-4-(iodomethyl)-2H-pyran;4-(Iodomethyl)tetrahydro-2H-pyrane;2H-Pyran, tetrahydro-4-(iodomethyl)-
- CBNumber:
- CB9120260
- Molecular Formula:
- C6H11IO
- Molecular Weight:
- 226.06
- MDL Number:
- MFCD06410724
- MOL File:
- 101691-94-5.mol
- MSDS File:
- SDS
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS05 |
|||||||||
|---|---|---|---|---|---|---|---|---|---|---|
| Signal word | Danger | |||||||||
| Hazard statements | H314 | |||||||||
| Precautionary statements | P260-P264-P280-P301+P310+P330+P331-P303+P361+P353+P310-P304+P340+P310-P305+P351+P338+P310-P363-P405-P501 | |||||||||
| Risk Statements | 34 | |||||||||
| Safety Statements | 23-26-36/37/39-45 | |||||||||
| NFPA 704 |
|
4-(Iodomethyl)tetrahydro-2H-pyran price More Price(26)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| SynQuest Laboratories | 2H10-H-03 | 4-(Iodomethyl)oxane | 101691-94-5 | 1g | $83 | 2021-12-16 | Buy |
| Matrix Scientific | 092540 | 4-(Iodomethyl)tetrahydro-2H-pyran 95+% | 101691-94-5 | 250mg | $189 | 2021-12-16 | Buy |
| SynQuest Laboratories | 2H10-H-03 | 4-(Iodomethyl)oxane | 101691-94-5 | 5G | $300 | 2021-12-16 | Buy |
| Matrix Scientific | 092540 | 4-(Iodomethyl)tetrahydro-2H-pyran 95+% | 101691-94-5 | 1g | $420 | 2021-12-16 | Buy |
| American Custom Chemicals Corporation | HCH0022345 | 4-(IODOMETHYL)TETRAHYDRO-2H-PYRAN 95.00% | 101691-94-5 | 1G | $750.68 | 2021-12-16 | Buy |
4-(Iodomethyl)tetrahydro-2H-pyran Chemical Properties,Uses,Production
Synthesis
4-(Iodomethyl)tetrahydro-2H-pyran is prepared from 4-(methanesulfonyloxymethyl)tetrahydropyran by heating and refluxing under conditions of reaction with sodium iodide in acetone. The specific method of operation is described below:
.
Preparation: A mixture of Preparation (328g, 1.69mol) and sodium iodide (507g, 3.4mol) in acetone (3.3L) was refluxed for 4h. TLC (diethyl ether) showed significant mesylate remaining so further sodium iodide (127g, 0.65mol) was added and reflux continued for 16h. The mixture was cooled and filtered. The resulting cake was washed with acetone, dried, and11then partitioned between diethyl ether (800mL) and water (800mL). The aqueous phase was re-extracted with diethyl ether (200mL), the ether extracts combined and washed with 10% sodium thiosulphate solution (300mL) which decolourised the extract. Final washing with water (300mL), drying (MgS04) and then removal of the solvent provided the 4-(IODOMETHYL)TETRAHYDRO-2H-PYRAN (365g, 92% yield).
4-(Iodomethyl)tetrahydro-2H-pyran Preparation Products And Raw materials
Raw materials
Preparation Products
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| career henan chemical co | +86-0371-86658258 | sales@coreychem.com | China | 29914 | 58 |
| Accela ChemBio Inc. | (+1)-858-699-3322 | info@accelachem.com | United States | 19965 | 58 |
| Chongqing Chemdad Co., Ltd | +86-023-61398051 +8613650506873 | sales@chemdad.com | China | 39916 | 58 |
| Alchem Pharmtech,Inc. | 8485655694 | sales@alchempharmtech.com | United States | 63711 | 58 |
| CONIER CHEM AND PHARMA LIMITED | +8618523575427 | sales@conier.com | China | 49390 | 58 |
| Shanghai Boc Chemical Co., Ltd. | 021-34975602; +8618721111801 | shangli@bocchem.com | China | 138 | 58 |
| Guangzhou Yuheng Pharmaceutical Technology Co., Ltd | +8613580539051 | joe@yuhengpharm.com | CHINA | 21149 | 58 |
| Alfa Chemistry | info@alfa-chemistry.com | United States | 2344 | 58 | |
| Aston Chemical | 13000000000 | sales@astonchem.com | United States | 1634 | 58 |
| Hefei Hirisun Pharmatech Co., Ltd | +8615056975894 | shawn@hirisunpharm.com | CHINA | 9923 | 58 |
View Lastest Price from 4-(Iodomethyl)tetrahydro-2H-pyran manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
 |
2019-07-06 | 4-(Iodomethyl)tetrahydro-2H-pyran
101691-94-5
|
US $1.00 / KG | 1KG | 98% | 500kg | Career Henan Chemical Co |
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- 4-(Iodomethyl)tetrahydro-2H-pyran
101691-94-5
- US $1.00 / KG
- 98%
- Career Henan Chemical Co