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4-NITROBENZO-15-CROWN-5

4-NITROBENZO-15-CROWN-5 structure

CAS No.: 60835-69-0

Chemical Name:: 4-NITROBENZO-15-CROWN-5

Synonyms: NITROBENZO-15-CROWN-5;4-NITROBENZO-15-CROWN-5;4'-NITROBENZO-15-CROWN-5;Nitrobenzo-15-crown-5,99%;4-nitryl-benzo-15-crown-5;4-Nitrobenzo-15-crown-5,99%;4'-NITROBENZO-15-CROWN 5-ETHER;4'-Nitrobenzo-15-crown 5-Ether;4'-Nitrobenzo-15-crown5-Ether>4- Nitrobenzene -15- crown ether -5

CBNumber:: CB9439728

Molecular Formula:: C14H19NO7

Molecular Weight:: 313.3

MDL Number:: MFCD00060713

MOL File:: 60835-69-0.mol

MSDS File:: SDS

Last updated:2023-04-23 13:52:06

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4-NITROBENZO-15-CROWN-5 Properties

Melting point	93-97 °C(lit.)
Boiling point	453.11°C (rough estimate)
Density	1.191
refractive index	1.5230 (estimate)
storage temp.	Store below +30°C.
solubility	It is soluble in non-polar solvents.
form	powder to crystal
color	Light orange to Yellow to Green
BRN	1598970
CAS DataBase Reference	60835-69-0(CAS DataBase Reference)

SAFETY

Risk and Safety Statements

Symbol(GHS)

GHS07

Signal word

Warning

Hazard statements

H315-H319-H335

Precautionary statements

P261-P280a-P304+P340-P305+P351+P338-P405-P501a

Hazard Codes

Risk Statements

36/37/38

Safety Statements

26-36

WGK Germany

HazardClass

IRRITANT

HS Code

29329985

NFPA 704

	0
2		0

4-NITROBENZO-15-CROWN-5 price More Price(14)

Manufacturer	Product number	Product description	CAS number	Packaging	Price	Updated	Buy
Sigma-Aldrich	341878	4′-Nitrobenzo-15-crown-5 99%	60835-69-0	1g	$50.9	2023-01-07	Buy
TCI Chemical	N0561	4'-Nitrobenzo-15-crown 5-Ether >99.0%(GC)	60835-69-0	1g	$67	2024-03-01	Buy
TCI Chemical	N0561	4'-Nitrobenzo-15-crown 5-Ether >99.0%(GC)	60835-69-0	5g	$202	2024-03-01	Buy
Alfa Aesar	A16225	4-Nitrobenzo-15-crown-5, 99%	60835-69-0	5g	$170	2024-03-01	Buy
Alfa Aesar	A16225	4-Nitrobenzo-15-crown-5, 99%	60835-69-0	1g	$35.3	2021-12-16	Buy

Product number	Packaging	Price	Buy
341878	1g	$50.9	Buy
N0561	1g	$67	Buy
N0561	5g	$202	Buy
A16225	5g	$170	Buy
A16225	1g	$35.3	Buy

4-NITROBENZO-15-CROWN-5 Chemical Properties,Uses,Production

Chemical Properties

LIGHT YELLOW GRANULAR POWDER

Uses

4-Nitrobenzo-15-crown-5 is a raw material used in synthesis as well as an intemediate in chemical syntheis and pharmaceutica intemediate. It is also used to separate cations, dissolve inorganic salts into organic solvents to perform naked anion chemistry, serve as phase transfer catalysts, and chiral crown ethers have been used to resolve racemic mixtures or separate isomers by chiral chromatography.

Purification Methods

Recrystallise the crown ether from EtOH, MeOH or *C6H6/hexane as for the 18-crown-6 compound below. It complexes with Na+, K+, NH4+, Ca2+, Mg2+ and Cd2+. The 1HNMR spectrum (CDCl3) has (ppm): 3.6-4.4 (m 16CH2), 6.8 (d 1H arom), 7.65 (d 1H arom), 7.80 (dd 1H arom Jab 9Hz and Jbc 3Hz) [Schmid et al. J Am Chem Soc 98 5198 1976, Kikukawa et al. Bull Chem Soc Jpn 50 2207 1977, Toke et al. Justus Liebigs Ann Chem 349 349, 761 1988, Lindner et al. Z Anal Chem 322 157 1985].

4-NITROBENZO-15-CROWN-5 synthesis

Synthesis of 4-NITROBENZO-15-CROWN-5 from Benzo-15-crown-5

4-NITROBENZO-15-CROWN-5 Preparation Products And Raw materials

Raw materials

DIETHYLENE GLYCOL BIS(2-CHLOROETHYL) ETHER Benzo-15-crown-5

Preparation Products

4'-AMINO-5'-NITROBENZO-15-CROWN-5

4-NITROBENZO-15-CROWN-5 Suppliers

Global( 109)Suppliers

Supplier	Tel	Email	Country	ProdList	Advantage
Ningxia LabsChem Co., Ltd.	0952-9294929 +8613895679378	48472788@qq.com	China	352	58
Capot Chemical Co.,Ltd.	571-85586718 +8613336195806	sales@capotchem.com	China	29797	60
CONIER CHEM AND PHARMA LIMITED	+8618523575427	sales@conier.com	China	47465	58
Zhengzhou Alfa Chemical Co.,Ltd	+8618530059196	sale04@alfachem.cn	China	12478	58
Eastar Chemical Corp	+1-8008982436 +86-13998381317	manannan@chinaeastar.com	United States	376	58
Aladdin Scientific	+1-833-552-7181	sales@aladdinsci.com	United States	57511	58
Qingdao Dexin Chemical Co., Ltd	+8615553333686	15553333686@qq.com	China	2983	58
Amadis Chemical Company Limited	571-89925085	sales@amadischem.com	China	131981	58
Mainchem Co., Ltd.	+86-0592-6210733	sale@mainchem.com	China	32360	55
Bide Pharmatech Ltd.	400-6005915	sales@picasso-e.com	China	39661	58

Supplier	Advantage
Ningxia LabsChem Co., Ltd.	58
Capot Chemical Co.,Ltd.	60
CONIER CHEM AND PHARMA LIMITED	58
Zhengzhou Alfa Chemical Co.,Ltd	58
Eastar Chemical Corp	58
Aladdin Scientific	58
Qingdao Dexin Chemical Co., Ltd	58
Amadis Chemical Company Limited	58
Mainchem Co., Ltd.	55
Bide Pharmatech Ltd.	58

4-NITROBENZO-15-CROWN-5 Spectrum

4-NITROBENZO-15-CROWN-5(60835-69-0)¹HNMR 4-NITROBENZO-15-CROWN-5(60835-69-0)¹³CNMR 4-NITROBENZO-15-CROWN-5(60835-69-0)IR1 4-NITROBENZO-15-CROWN-5(60835-69-0)Raman

60835-69-0(4-NITROBENZO-15-CROWN-5)Related Search:

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2,3,5,6,8,9,11,12-Octahydro-15-nitro-1,4,7,10,13-benzopentaoxacyclopentadecin CROWN ETHER/4'-NITROBENZO-15-CROWN-5 FOR Crown ether/4'-Nitrobenzo-15-crown-5 for synthesis 15-Nitro-2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecine 17-Nitro-2,3-benzo-1,4,7,10,13-pentaoxacyclopentadecen-2 NITROBENZO-15-CROWN-5 CROWN ETHER/4'-NITROBENZO-15-CROWN-5 4'-NITROBENZO-15-CROWN-5 4-NITROBENZO-15-CROWN-5 4'-NITROBENZO-15-CROWN 5-ETHER 2,3-(4-NITROBENZO)-1,4,7,10,13-PENTAOXACYCLOPENTADEC-2-ENE CARBON DISULFIDE, REAGENTPLUS, >=99.9%, LOW BENZENE 4-Nitrobenzo-15-crown-5,99% 1,4,7,10,13-Benzopentaoxacyclopentadecin, 2,3,5,6,8,9,11,12-octahydro-15-nitro- 1,13-(4-Nitro-1,2-phenylene)-1,4,7,10,13-pentaoxatridecane 1,2-(1,4,7,10,13-Pentaoxatridecane-1,13-diyl)-4-nitrobenzene 15-Nitro-2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecin 16-Nitro-2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecin Nitrobenzo-15-crown-5,99% 4-nitryl-benzo-15-crown-5 17-nitro-2,5,8,11,14-pentaoxabicyclo[13.4.0]nonadeca-1(15),16,18-triene 4'-Nitrobenzo-15-crown5-Ether> 4- Nitrobenzene -15- crown ether -5 4'-Nitrobenzo-15-crown 5-Ether 60835-69-0 33408-96-1 C14H19NO7 Macrocycles for Host-Guest Chemistry Crown Ethers Synthetic Reagents Chelation/Complexation Compounds Synthetic Reagents Crown Ethers Chelation/Complexation Compounds Macrocycles for Host-Guest Chemistry Functional Materials Crown Ethers