1-ブロモカルバゾール
1-ブロモカルバゾール 物理性質
- 融点 :
- 123-124℃ (acetic acid )
- 沸点 :
- 409.2±18.0 °C(Predicted)
- 比重(密度) :
- 1.617±0.06 g/cm3(Predicted)
- 貯蔵温度 :
- Sealed in dry,Room Temperature
- 外見 :
- powder to crystal
- 酸解離定数(Pka):
- 16.14±0.30(Predicted)
- 色:
- White to Light yellow
1-ブロモカルバゾール 価格
もっと(13)
| メーカー |
製品番号 |
製品説明 |
CAS番号 |
包装 |
価格 |
更新時間 |
購入 |
|
富士フイルム和光純薬株式会社(wako)
|
W01COBQJ-7085 |
1-ブロモ-9H-カルバゾール
1-Bromo-9h-carbazole |
16807-11-7 |
1g |
￥10000 |
2024-03-01 |
購入 |
|
富士フイルム和光純薬株式会社(wako)
|
W01COBQJ-7085 |
1-Bromo-9h-carbazole |
16807-11-7 |
5g |
￥35000 |
2024-03-01 |
購入 |
|
富士フイルム和光純薬株式会社(wako)
|
W01COBQJ-7085 |
1-Bromo-9h-carbazole |
16807-11-7 |
10g |
￥65000 |
2024-03-01 |
購入 |
|
富士フイルム和光純薬株式会社(wako)
|
W01COBQJ-7085 |
1-Bromo-9h-carbazole |
16807-11-7 |
25g |
￥127500 |
2024-03-01 |
購入 |
|
富士フイルム和光純薬株式会社(wako)
|
W01COBQJ-7085 |
1-Bromo-9h-carbazole |
16807-11-7 |
100g |
￥360000 |
2024-03-01 |
購入 |
1-ブロモカルバゾール 化学特性,用途語,生産方法
外観
白色～うすい黄色粉末～結晶
化学的特性
White to yellow powder or crystals.
使用
1-Bromo-9H-carbazole is a useful research chemical, mainly used as a pharmaceutical intermediate and an intermediate in organic synthesis.
製造方法
A 1-Bromo-9H-carbazole is synthesized as follows：Under noble gas protection, by 3,6- bis- Tert-butyl carbazole is dissolved in 1,2- dichloroethanes, adds hydrobromic acid, controlling reaction temperature to be slowly added dropwise hydrogen peroxide, dropping is completely Overnight, reactant liquor is washed, and separates organic layer for natural temperature reaction, is dried, and adds methyl alcohol dispersion, obtains the tertiary fourth of bromo- 3, the 6- of 1- bis- Base carbazole；Then 1- bromo- 3,6- di-t-butyl carbazole and isopropanol solvent are added in reaction bulb, controlling reaction temperature slowly adds Enter alchlor reaction, add water after terminating terminating reaction, through extraction, organic layer sodium hydrate aqueous solution is washed, and is dried overnight, concentrate Obtain crude product, methylene chloride-methanol mixed solvent is recrystallized to give product 1-Bromo-9H-carbazole.
Production method of 1-bromocarbazole
定義
1-Bromo-9H-carbazole is a bromide-substitution of carbazole. The carbazole ring system is essentially planar (r.m.s. deviation of 0.024? for the non-H atoms). It is a photoelectric material intermediate and be used to synthesize OLED materials.
1-ブロモカルバゾール 上流と下流の製品情報
原材料
準備製品
1-ブロモカルバゾール 生産企業
Global( 210)Suppliers
1-ブロモカルバゾール スペクトルデータ(FT-IR)
16807-11-7(1-ブロモカルバゾール)キーワード:
- 16807-11-7
- -broMo-9H-carbazole
- 1-broMo-9H-carbazole
- 9H-Carbazole, 1-broMo-
- 1-bromo-9H-carbozle
- 1-Bromocarbazole >
- -broMo-9H-carbazole
- 1-broMocarbazole
- 1-ブロモカルバゾール
- 1-ブロモ-9H-カルバゾール