3-クロロ-5-(トリフルオロメチル)安息香酸
3-クロロ-5-(トリフルオロメチル)安息香酸 物理性質
- 融点 :
- 98-101℃
- 沸点 :
- 263℃
- 比重(密度) :
- 1.523
- 闪点 :
- 113℃
- 貯蔵温度 :
- Sealed in dry,Room Temperature
- 水溶解度 :
- 水に溶ける。
- CAS データベース:
- 53985-49-2
3-クロロ-5-(トリフルオロメチル)安息香酸 価格
もっと(14)
| メーカー |
製品番号 |
製品説明 |
CAS番号 |
包装 |
価格 |
更新時間 |
購入 |
|
富士フイルム和光純薬株式会社(wako)
|
W01MAS009469 |
3-クロロ-5-(トリフルオロメチル)安息香酸
3-Chloro-5-(trifluoromethyl)benzoic acid |
53985-49-2 |
25g |
￥105800 |
2024-03-01 |
購入 |
|
富士フイルム和光純薬株式会社(wako)
|
W01APOPC6011 |
3-クロロ-5-(トリフルオロメチル)安息香酸
3-Chloro-5-(trifluoromethyl)benzoic acid |
53985-49-2 |
1g |
￥5800 |
2024-03-01 |
購入 |
|
富士フイルム和光純薬株式会社(wako)
|
W01APOPC6011 |
3-クロロ-5-(トリフルオロメチル)安息香酸
3-Chloro-5-(trifluoromethyl)benzoic acid |
53985-49-2 |
5g |
￥16300 |
2024-03-01 |
購入 |
|
富士フイルム和光純薬株式会社(wako)
|
W01MAS009469 |
3-クロロ-5-(トリフルオロメチル)安息香酸
3-Chloro-5-(trifluoromethyl)benzoic acid |
53985-49-2 |
1g |
￥8700 |
2024-03-01 |
購入 |
|
富士フイルム和光純薬株式会社(wako)
|
W01COBQA-6429 |
3-クロロ-5-(トリフルオロメチル)安息香酸
3-Chloro-5-(trifluoromethyl)benzoic acid |
53985-49-2 |
1g |
￥10000 |
2024-03-01 |
購入 |
3-クロロ-5-(トリフルオロメチル)安息香酸 化学特性,用途語,生産方法
使用
2-Chloro-5-(trifluoromethyl)benzoic acid may be used as surrogate standard to investigate the exposure and home contamination in urine and hand wipe samples collected from farmers.
合成
A solution of tBuONO (35.2 g) and CuCl (38.6 g) in CH3CN (375 mL) was warmed to 45-50° C. The compound (50.0 g) obtained in step 2 was added slowly while cooling the reaction mixture to maintain 45-50° C. After stirring at 50° C. for 30 min, the mixture was cooled to 10° C. 6N Hydrochloric acid (250 mL) was added and the mixture was stirred for 10 min. The resultant product was extracted twice with ethyl acetate. The organic layer was-washed with 10% aqueous citric acid solution and water and dried, and the solvent was evaporated under reduced pressure. The obtained residue was purified by silica gel column chromatography (solvent gradient; 10→25% ethyl acetate/hexane) to give 3-chloro-5-(trifluoromethyl)benzoic acid (33.1 g, 60%) as a white powder.
3-クロロ-5-(トリフルオロメチル)安息香酸 上流と下流の製品情報
原材料
準備製品
3-クロロ-5-(トリフルオロメチル)安息香酸 生産企業
Global( 94)Suppliers
53985-49-2(3-クロロ-5-(トリフルオロメチル)安息香酸)キーワード:
- 53985-49-2
- 3-CHLORO-5-(TRIFLUOROMETHYL)BENZOIC ACID
- 3-Chloro-5-carboxybenzotrifluoride
- 3-Carboxy-5-chlorobenzotrifluoride, 5-Chloro-alpha,alpha,alpha-trifluoro-m-toluic acid
- Benzoic acid, 3-chloro-5-(trifluoromethyl)-
- 3-クロロ-5-(トリフルオロメチル)安息香酸