フェナシルアミン·塩酸塩
フェナシルアミン·塩酸塩 価格
もっと(2)
| メーカー |
製品番号 |
製品説明 |
CAS番号 |
包装 |
価格 |
更新時間 |
購入 |
|
Sigma-Aldrich Japan
|
A38207 |
2-アミノアセトフェノン 塩酸塩 99%
2-Aminoacetophenone hydrochloride 99% |
5468-37-1 |
1g |
￥11400 |
2024-03-01 |
購入 |
|
Sigma-Aldrich Japan
|
A38207 |
2-アミノアセトフェノン 塩酸塩 99%
2-Aminoacetophenone hydrochloride 99% |
5468-37-1 |
5g |
￥37800 |
2024-03-01 |
購入 |
フェナシルアミン·塩酸塩 化学特性,用途語,生産方法
化学的特性
Off-white crystalline
合成
To a stirred solution of phenacyl bromide (1 mmol, 1 equiv) in diethyl ether (13 mL) was added hexamethylenetetramine (1 mmol, 1 equiv) all at once and the mixture was stirred for 12 h at room temperature. The resulting solid was filtered, washed with diethyl ether (15 mL), and dried under reduced pressure to afford the quaternary salt, which was next placed in a two-necked round-bottomed flask fitted with a reflux condenser, and EtOH (22 mL) was added to it. Concentrated HCl (0.6 mL) was added, and the mixture was refluxed for 3 h (solid formed). After cooling to room temperature, the solid was filtered, washed with EtOH (20 mL), and dried under vacuum to afford pure 2-Aminoacetophenone hydrochloride.
純化方法
Crystallise the salt from Me2CO /EtOH, EtOH/ Et2O, 2-propanol or 2-propanol and a little HCl (slowly after a fe
フェナシルアミン·塩酸塩 上流と下流の製品情報
原材料
準備製品
フェナシルアミン·塩酸塩 生産企業
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フェナシルアミン·塩酸塩 スペクトルデータ(1HNMR、IR1、IR2、MS、Raman)
5468-37-1(フェナシルアミン·塩酸塩)キーワード:
- 5468-37-1
- ω-aminoacetophenone hydrochloride
- w-Aminoacetophenone hydrochloride
- aminomethylphenylketone hydrochloride
- 2-AMinoacetophenone hydrochloride, 96% 1GR
- OMEGA-AMINOACETOPHENONE HYDROCHLORIDE (CA. 4% NACL)
- 2-AMINOACETOPHENONE HYDROCHLORIDE 99%
- O-aminoacetophenone HCl ,1-(o-aminophenyl)ethanone
- ω-Aminoacetophenone hydrochloride, Phenacylamine hydrochloride
- 1-Phenyl-2-aminoethanone·hydrochloride
- Phenacylamine hydrochloride with 4% NaCl
- 2-amino-1-phenyl-ethanonhydrochloride
- 2-Aminoacetophenone hydrochloride,96%
- Acetophenone, 2-aMino-, hydrochloride
- Ethanone,2-aMino-1-phenyl-, hydrochloride (1:1)
- 2-Aminoacetophenone*HCl (with ca. 4% NaCl)
- 2-amino-acetophenonhydrochloride
- OMEGA-AMINOACETOPHENONE HYDROCHLORIDE
- O-AMINOACETOPHENONE HYDROCHLORIDE
- 2-AMINOACETOPHENONE HYDROCHLORIDE
- 2-AMINO-1-PHENYL-ETHANONE HYDROCHLORIDE
- ALPHA-AMINOACETOPHENONE HYDROCHLORIDE
- 2-OXO-2-PHENYL-ETHYL-AMMONIUM, CHLORIDE
- ETHANONE, 2-AMINO-1-PHENYL-, HYDROCHLORIDE
- 2-Aminoacetophenone hydrochloride with 4% NaCl
- w-Amino-acetophinone hydrochloride
- α-Aminoacetophenone (Mixed Salt, >85%)
- α-Aminoacetophenone
- α-Aminoacetophenone Hydrochloride
- 2-amino-acetophenonhydrochlo
- PHENACYLAMINE HYDROCHLORIDE
- 1-フェニル-2-アミノエタノン·塩酸塩
- ω-アミノアセトフェノン·塩酸塩
- ω-アミノアセトフェノン塩酸塩
- フェナシルアミン·塩酸塩
- α-アミノアセトフェノン·塩酸塩
- 2-アミノアセトフェノン 塩酸塩