2-フルオロ-3-ニトロ安息香酸メチル
2-フルオロ-3-ニトロ安息香酸メチル 物理性質
- 融点 :
- 77- 80° C
- 沸点 :
- 310.8±27.0 °C(Predicted)
- 比重(密度) :
- 1.388±0.06 g/cm3(Predicted)
- 貯蔵温度 :
- Sealed in dry,Room Temperature
- 溶解性:
- クロロホルム（微量）、メタノール（微量）
- 外見 :
- 個体
- 色:
- オフホワイトからペールイエロー
2-フルオロ-3-ニトロ安息香酸メチル 価格
もっと(5)
| メーカー |
製品番号 |
製品説明 |
CAS番号 |
包装 |
価格 |
更新時間 |
購入 |
|
富士フイルム和光純薬株式会社(wako)
|
W01COBAN-2888 |
2-フルオロ-3-ニトロ安息香酸メチル
Methyl 2-fluoro-3-nitrobenzoate |
946126-94-9 |
1g |
￥10000 |
2024-03-01 |
購入 |
|
富士フイルム和光純薬株式会社(wako)
|
W01COBAN-2888 |
2-フルオロ-3-ニトロ安息香酸メチル
Methyl 2-fluoro-3-nitrobenzoate |
946126-94-9 |
5g |
￥10000 |
2024-03-01 |
購入 |
|
富士フイルム和光純薬株式会社(wako)
|
W01COBAN-2888 |
Methyl 2-fluoro-3-nitrobenzoate |
946126-94-9 |
100g |
￥87500 |
2024-03-01 |
購入 |
|
富士フイルム和光純薬株式会社(wako)
|
W01COBAN-2888 |
2-フルオロ-3-ニトロ安息香酸メチル
Methyl 2-fluoro-3-nitrobenzoate |
946126-94-9 |
25g |
￥32500 |
2024-03-01 |
購入 |
|
富士フイルム和光純薬株式会社(wako)
|
W01COBAN-2888 |
2-フルオロ-3-ニトロ安息香酸メチル
Methyl 2-fluoro-3-nitrobenzoate |
946126-94-9 |
10g |
￥76500 |
2023-06-01 |
購入 |
2-フルオロ-3-ニトロ安息香酸メチル 化学特性,用途語,生産方法
使用
Methyl 2-fluoro-3-nitrobenzoate can be used as organic synthesis intermediates and pharmaceutical intermediates, mainly used in laboratory research and development processes and chemical production processes.
合成
A solution of 2-fluoro-3-nitrobenzoic acid (5 g, 27.0 mmol) in MeOH (50 mL) was treated with concentrated H2SO4 (1.4 mL, 27.0 mmol) and the resulting reaction was stirred at 50 °C for 16 h. The solvent was removed under reduced pressure and the residue was diluted with EtO Ac. The organic solution was washed with saturated aqueous NaHCO3 solution until the water phase reached neutral pH. The two phases were separated. Organics were washed with water, brine and dried (Na2SO4). The solution was filtered and concentrated to give crude methyl 2-fluoro-3-nitrobenzoate which was used as is in the next step. (5.1 g, 25.2 mmol, 93 %) as a pale yellow solid.
2-フルオロ-3-ニトロ安息香酸メチル 上流と下流の製品情報
原材料
準備製品
2-フルオロ-3-ニトロ安息香酸メチル 生産企業
Global( 166)Suppliers
2-フルオロ-3-ニトロ安息香酸メチル スペクトルデータ(FT-IR)
946126-94-9(2-フルオロ-3-ニトロ安息香酸メチル)キーワード:
- 946126-94-9
- methyl 2-fluoro-3-nitrobenzoate
- Benzoic acid, 2-fluoro-3-nitro-, Methyl ester
- 2-Fluoro-3-(methoxycarbonyl)nitrobenzene
- 2-fluoro-3-nitrobenzoate
- 2-フルオロ-3-ニトロ安息香酸メチル