4-bromo-3-bromomethyl-benzoic acid methyl ester
4-bromo-3-bromomethyl-benzoic acid methyl ester 物理性質
- 沸点 :
- 356.9±32.0 °C(Predicted)
- 比重(密度) :
- 1.780±0.06 g/cm3(Predicted)
- 貯蔵温度 :
- under inert gas (nitrogen or Argon) at 2-8°C
- 外見 :
- White flakes
- InChI:
- InChI=1S/C9H8Br2O2/c1-13-9(12)6-2-3-8(11)7(4-6)5-10/h2-4H,5H2,1H3
- InChIKey:
- GRJDNFSKEWOMIM-UHFFFAOYSA-N
- SMILES:
- C(OC)(=O)C1=CC=C(Br)C(CBr)=C1
4-bromo-3-bromomethyl-benzoic acid methyl ester 価格
もっと(10)
| メーカー |
製品番号 |
製品説明 |
CAS番号 |
包装 |
価格 |
更新時間 |
購入 |
|
富士フイルム和光純薬株式会社(wako)
|
W01COBSH-5660 |
Methyl 4-bromo-3-(bromomethyl)benzoate |
142031-67-2 |
10g |
￥180000 |
2024-03-01 |
購入 |
|
富士フイルム和光純薬株式会社(wako)
|
W01APOOR400600 |
Methyl 4-Bromo-3-(bromomethyl)benzoate |
142031-67-2 |
250mg |
￥17300 |
2024-03-01 |
購入 |
|
富士フイルム和光純薬株式会社(wako)
|
W01APOOR400600 |
Methyl 4-Bromo-3-(bromomethyl)benzoate |
142031-67-2 |
1g |
￥43200 |
2024-03-01 |
購入 |
|
富士フイルム和光純薬株式会社(wako)
|
W01COBSH-5660 |
Methyl 4-bromo-3-(bromomethyl)benzoate |
142031-67-2 |
1g |
￥30000 |
2024-03-01 |
購入 |
|
富士フイルム和光純薬株式会社(wako)
|
W01COBSH-5660 |
Methyl 4-bromo-3-(bromomethyl)benzoate |
142031-67-2 |
5g |
￥105000 |
2024-03-01 |
購入 |
4-bromo-3-bromomethyl-benzoic acid methyl ester 化学特性,用途語,生産方法
合成
In a 6-liter reactor equipped with a condenser, a central mechanical stirrer, and a thermometer, introduce 575 g (2.5 mol) of methyl 4-bromo-3-methylbenzoate, 3 liters of methylene chloride, 494 g (2.75 mol) of N-bromosuccinimide and 17 g of benzoyl peroxide (0.05 mol; 70percent in water). Heat the mixture at reflux under irradiation with a 1000-watt lamp for 10 h. Wash the mixture twice with 1 liter of water, then with 1 liter of saturated sodium chloride solution. Evaporate the methylene chloride. Recrystallize the crude product obtained from heptane. This gives 596 g of 4-bromo-3-bromomethyl-benzoic acid methyl ester as off-white crystals.
4-bromo-3-bromomethyl-benzoic acid methyl ester 上流と下流の製品情報
原材料
準備製品
4-bromo-3-bromomethyl-benzoic acid methyl ester 生産企業
Global( 69)Suppliers
142031-67-2()キーワード:
- 142031-67-2
- Methyl 4-broMo-3-(broMoMethyl)benzoate
- 4-BROMO-3-BROMOMETHYL-BENZOIC ACID METHYL ESTER
- Benzoic acid, 4-bromo-3-(bromomethyl)-, methyl ester
- Methyl 3-(bromomethyl)-3-bromophenylacetate
- 3-Bromomethyl-4-bromobenzoic acid methyl ester