6-Bromoindanone

6-Bromoindanone 구조식 이미지
카스 번호:
14548-39-1
상품명:
6-Bromoindanone
동의어(영문):
6-bromo-2,3-dihydro-1H-inden-1-one;6-BROMO-1-INDANONE;6-BROMO-2,3-DIHYDROINDEN-1-ONE;6-broindone;6-BroMoindaonoe;6-BROMO INDANONE;6-bromofluorenone;6-BROMO-INDAN-1-ONE;6-Bromo-1-indanone>6-Bromo-1-indanone,98%
CBNumber:
CB0426226
분자식:
C9H7BrO
포뮬러 무게:
211.06
MOL 파일:
14548-39-1.mol

6-Bromoindanone 속성

녹는점
111-115 °C(lit.)
끓는 점
291.6±29.0 °C(Predicted)
밀도
1.608±0.06 g/cm3(Predicted)
저장 조건
Inert atmosphere,Room Temperature
물리적 상태
결정질 분말 또는 바늘
색상
흰색에서 노란색으로
최대 파장(λmax)
302nm(EtOH)(lit.)
InChIKey
SEQHEDQNODAFIU-UHFFFAOYSA-N
CAS 데이터베이스
14548-39-1(CAS DataBase Reference)
NIST
1-Indanone, 6-bromo-,(14548-39-1)
안전
  • 위험 및 안전 성명
  • 위험 및 사전주의 사항 (GHS)
안전지침서 24/25
WGK 독일 3
HS 번호 29147000
그림문자(GHS): GHS hazard pictograms
신호 어: Warning
유해·위험 문구:
암호 유해·위험 문구 위험 등급 범주 신호 어 그림 문자 P- 코드
H315 피부에 자극을 일으킴 피부부식성 또는 자극성물질 구분 2 경고 GHS hazard pictograms P264, P280, P302+P352, P321,P332+P313, P362
H319 눈에 심한 자극을 일으킴 심한 눈 손상 또는 자극성 물질 구분 2A 경고 GHS hazard pictograms P264, P280, P305+P351+P338,P337+P313P
예방조치문구:
P264 취급 후에는 손을 철저히 씻으시오.
P264 취급 후에는 손을 철저히 씻으시오.
P280 보호장갑/보호의/보안경/안면보호구를 착용하시오.
NFPA 704
1
2 0

6-Bromoindanone C화학적 특성, 용도, 생산

화학적 성질

White to yellow crystalline powder or needles. Density 1.608g/cm3, melting point 111-115°C(lit.), boiling point 291.6°C at 760mmHg, flash point 111.6°C, refractive index 1.6231, vapor pressure 0.002mmHg at 25°C. 6-Bromoindanone can be used as intermediate in pharmaceutical and chemical synthesis.

용도

6-Bromo-1-indanone is used as an organic chemical synthesis intermediate.

제조 방법

6-Bromoindanone synthesis: Trifluoromethanesulfonic acid (0.35 mL, 4 mmol) was added to anhydrous CHCl3 or CH2Cl2 (2 mL) solution of amide substrate 6 (1 mmol). The mixture was stirred for 4 h and then poured into ice. The product was extracted into CHCl3, and the organic solution was washed with H2O, brine and dried with anhydrous sodium sulfate. The crude product was isolated and purified by column chromatography (hexane:ethyl acetate). Recovery of nitro-substituted aniline: The aqueous extract was made basic by the addition of 10MNaOH and the solution was extracted with CHCl3. The organic solution was washed with H2O, brine (2x) and dried over anhydrous sodium sulfate to yield 6-bromoindanone in 88% yield.

6-Bromoindanone 준비 용품 및 원자재

원자재

준비 용품


6-Bromoindanone 공급 업체

글로벌( 358)공급 업체
공급자 전화 이메일 국가 제품 수 이점
PharmOrgSyn Laboratories Co., Ltd.
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Hebei Mojin Biotechnology Co., Ltd
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Henan Fengda Chemical Co., Ltd
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Capot Chemical Co.,Ltd.
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Shanghai Daken Advanced Materials Co.,Ltd
+86-371-66670886
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Hi-Tech Chemistry Corp
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Henan Tianfu Chemical Co.,Ltd.
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info@tianfuchem.com China 21695 55
Hangzhou FandaChem Co.,Ltd.
008657128800458; +8615858145714
fandachem@gmail.com China 9352 55
ATK CHEMICAL COMPANY LIMITED
+undefined-21-51877795
ivan@atkchemical.com China 32480 60
career henan chemical co
+86-0371-86658258
sales@coreychem.com China 29914 58

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