2-요오드벤조 산
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2-요오드벤조 산 속성
- 녹는점
- 160-162 °C(lit.)
- 끓는 점
- 313.9±25.0 °C(Predicted)
- 밀도
- 2.25
- 저장 조건
- Keep in dark place,Inert atmosphere,Room temperature
- 용해도
- 디메틸 설폭사이드 및 메탄올에 용해됨
- 산도 계수 (pKa)
- 2.85(at 25℃)
- 물리적 상태
- 분말, 결정 또는 플레이크
- 색상
- 연한 노란색에서 주황색 갈색까지
- 수용성
- 난용성
- 감도
- Light Sensitive
- Merck
- 14,5030
- BRN
- 1861406
- 안정성
- 안정적인. 강한 산화제, 강한 염기와 호환되지 않습니다.
- InChIKey
- CJNZAXGUTKBIHP-UHFFFAOYSA-N
- CAS 데이터베이스
- 88-67-5(CAS DataBase Reference)
안전
- 위험 및 안전 성명
- 위험 및 사전주의 사항 (GHS)
| 위험품 표기 | Xn,Xi | ||
|---|---|---|---|
| 위험 카페고리 넘버 | 22-37/38-41-36/37/38-20/21/22 | ||
| 안전지침서 | 26-39-24/25-22-36 | ||
| WGK 독일 | 3 | ||
| RTECS 번호 | DH2975000 | ||
| 위험 참고 사항 | Irritant | ||
| TSCA | T | ||
| 위험 등급 | IRRITANT, LIGHT SENSITIVE | ||
| HS 번호 | 29163900 | ||
| 기존화학 물질 | KE-21035 |
2-요오드벤조 산 C화학적 특성, 용도, 생산
개요
2-iodobenzoic acid and its derivatives are important pharmaceutical and chemical raw materials, which are necessary for the synthesis of various high-iodine reagents. It is commonly used as a precursor for the synthesis of 2-Iodoxybenzoic acid (IBX) and Dess-Martin peridinane, which are used as mild oxidants. It is also used in Suziki reaction.화학적 성질
white crystal powder. Soluble in alcohol and ether, insoluble in water.용도
Reagent for detection of sulfhydryl groups in proteins. 2-Iodobenzoic acid acts as a precursor in the preparation of 2-Iodoxybenzoic acid (IBX) and Dess-Martin periodinane, which finds application as an oxidizing agent in synthetic chemistry. It is also used in Suzuki reaction.제조 방법
2-Iodobenzoic acid is obtained from Anthranilic acid by diazotization and substitution. Diazotization of Anthranilic acid with sodium nitrite in the presence of sulfuric acid, control the temperature below 10℃, filter the diazotization solution, add the mixture of potassium iodide and sulfuric acid, stir for 10min after addition, and boil. Filter, wash with sodium thiosulfate solution, 2-Iodobenzoic acid can be recrystallized from water.정의
ChEBI: An iodobenzoic acid with a single iodo substituent placed at the 2-position.Purification Methods
Crystallise the acid repeatedly from water and EtOH. Sublime it under vacuum at 100o. [Beilstein 9 IV 1030.]2-요오드벤조 산 준비 용품 및 원자재
원자재
안트라닐산
2-Iodobenzoic acid phenacyl ester
Benzenediazonium, 2-iodo-, tetrafluoroborate(1-)
2-Iodobenzyl alcohol
2-IODOBENZALDEHYDE
2-IODOSTYRENE
t-Butyl2-iodobenzoate
Methyl 2-iodobenzoate
준비 용품
2-IODOBENZOYL CHLORIDE
Dess-Martin periodinane
2-Iodoxybenzoic acid
2'-IODOHIPPURIC ACID
플루페나믹 산
2-Ethoxycarbonylphenylboronic acid pinacol ester
1-Hydroxy-2-oxa-1-ioda(III)indan-3-one
1,3-Dihydro-3,3-dimethyl-1-(trifluoromethyl)-1,2-benziodoxole, Tognis Reagent
Methyl 2-(2-iodophenyl)acetate
N-(2-AMINO-4-CHLOROPHENYL)ANTHRANILIC ACID
5-Bromo-2-iodobenzoic acid
2-요오드벤조 산 공급 업체
글로벌( 635)공급 업체
| 공급자 | 전화 | 이메일 | 국가 | 제품 수 | 이점 |
|---|---|---|---|---|---|
| Dalian Richfortune Chemicals Co., Ltd | 0411-84820922 8613904096939 |
sales@richfortunechem.com | China | 303 | 57 |
| Mascot I.E.Co .,Ltd. | |
China | 303 | 58 | |
| Hebei Mojin Biotechnology Co., Ltd | +8613288715578 |
sales@hbmojin.com | China | 12456 | 58 |
| Hebei Yanxi Chemical Co., Ltd. | +8617531190177 |
peter@yan-xi.com | China | 5993 | 58 |
| Zibo Hangyu Biotechnology Development Co., Ltd | +86-0533-2185556 +8617865335152 |
Mandy@hangyubiotech.com | China | 11013 | 58 |
| Shaanxi Haibo Biotechnology Co., Ltd | +undefined18602966907 |
qinhe02@xaltbio.com | China | 1000 | 58 |
| Henan Fengda Chemical Co., Ltd | +86-371-86557731 +86-13613820652 |
info@fdachem.com | China | 7845 | 58 |
| Hebei Zhuanglai Chemical Trading Co.,Ltd | +8613343047651 |
admin@zlchemi.com | China | 476 | 58 |
| Capot Chemical Co.,Ltd. | 571-85586718 +8613336195806 |
sales@capotchem.com | China | 29797 | 60 |
| Shanghai Daken Advanced Materials Co.,Ltd | +86-371-66670886 |
info@dakenam.com | China | 15928 | 58 |