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(S)-ALPHA-METHYL-4-NITROBENZYLAMINE HYDROCHLORIDE

(S)-ALPHA-METHYL-4-NITROBENZYLAMINE HYDROCHLORIDE 구조식 이미지
카스 번호:
132873-57-5
상품명:
(S)-ALPHA-METHYL-4-NITROBENZYLAMINE HYDROCHLORIDE
동의어(영문):
(S)-NITRESOLVE;(S)-(+)-1-(4-NITROPHENYL)-ETHYLAMINE HCL;(S)-alpha-methyl-4-nitrobenzenemethanamine;(S)-(+)-ALPHA-METHYL-4-NITROBENZYLAMINE HCL;(S)-α-Methyl-4-nitrobenzylamineHydrochloride;(S)-4-NITROPHENYL-1-ETHYLAMINE HYDROCHLORIDE;1-(S)-4-Nitrophenyl ethylamine hydrochloride;(S)-4-Nitro-α-methylbenzylamine hydrochloride;(S)-1-(4-Nitrophenyl)ethanaMine hydrochloride;(S)-α-Methyl-4-nitrobenzylamine Hydrochloride
CBNumber:
CB1467176
분자식:
C8H11ClN2O2
포뮬러 무게:
202.64
MOL 파일:
132873-57-5.mol
MSDS 파일:
SDS

(S)-ALPHA-METHYL-4-NITROBENZYLAMINE HYDROCHLORIDE 속성

녹는점
248-250 °C(lit.)
굴절률
-7.2 ° (C=1, 0.05mol/L NaOH)
저장 조건
Inert atmosphere,Room Temperature
물리적 상태
powder to crystal
색상
흰색에서 밝은 노란색
optical activity
[α]25/D 6.5°, c = 1 in 0.05 M NaOH
수용성
희미한 탁도
CAS 데이터베이스
132873-57-5(CAS DataBase Reference)
안전
  • 위험 및 안전 성명
  • 위험 및 사전주의 사항 (GHS)
위험품 표기 Xi
위험 카페고리 넘버 36/37/38
안전지침서 26-37/39
WGK 독일 3
F 고인화성물질 3-10
HS 번호 29214990
그림문자(GHS): GHS hazard pictograms
신호 어: Warning
유해·위험 문구:
암호 유해·위험 문구 위험 등급 범주 신호 어 그림 문자 P- 코드
H315 피부에 자극을 일으킴 피부부식성 또는 자극성물질 구분 2 경고 GHS hazard pictograms P264, P280, P302+P352, P321,P332+P313, P362
H319 눈에 심한 자극을 일으킴 심한 눈 손상 또는 자극성 물질 구분 2A 경고 GHS hazard pictograms P264, P280, P305+P351+P338,P337+P313P
예방조치문구:
P264 취급 후에는 손을 철저히 씻으시오.
P264 취급 후에는 손을 철저히 씻으시오.
P280 보호장갑/보호의/보안경/안면보호구를 착용하시오.
NFPA 704
0
2 0

(S)-ALPHA-METHYL-4-NITROBENZYLAMINE HYDROCHLORIDE C화학적 특성, 용도, 생산

용도

(S)-α-Methyl-4-nitrobenzylamine hydrochloride can be used as:

Purification Methods

To ensure dryness, the hydrochloride (ca 175 g) is extracted with EtOH (3x100mL) and evaporated to dryness (any residual H2O increases the solubility in EtOH and lowers the yield). The hydrochloride residue is triturated with absolute EtOH and dried in vacuo. The product is further purified by refluxing with absolute EtOH (200 mL for 83g) for 1hour, and cool to 10o to give 76.6g of hydrochloride m 243-245o(dec). The free base is prepared by dissolving in N NaOH, extracting with CH2Cl2 (3 x 500mL), drying (Na2CO3), filtering, evaporating and distilling it. It has m 27o, b 119-120o/0.5mm (105-107o/0.5mm, 157-159o/9mm, d 1.1764, n 1.5688, [] ±17.7o (neat) [Perry et al. Synthesis 492 1977,ORD: Nerdel & Liebig Justus Liebigs Ann Chem 621 142 1959]. [Beilstein 12 IV 2451.]

(S)-ALPHA-METHYL-4-NITROBENZYLAMINE HYDROCHLORIDE 준비 용품 및 원자재

원자재

준비 용품

(S)-ALPHA-METHYL-4-NITROBENZYLAMINE HYDROCHLORIDE 공급 업체

글로벌( 122)공급 업체
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Mainchem Co., Ltd. +86-0592-6210733
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(S)-ALPHA-METHYL-4-NITROBENZYLAMINE HYDROCHLORIDE 관련 검색:

에틸아민 하이드로클로라이드 Ammonium sulfate (R)-ALPHA-METHYL-4-NITROBENZYLAMINE HYDROCHLORIDE S-(-)-a-Methyl-p-aminobenzylamine (S)-1-(4-NITROPHENYL)-ETHYLAMINE 4-Nitrobenzylamine hydrochloride ALFA-ALFA-DIMETHYL-P-NITRO-BENZYLAMINE HYDROCHLORIDE 4-(1-AMINO-ETHYL)-PHENYLAMINE (S)-ALPHA-METHYL-4-NITROBENZYLAMINE HYDROCHLORIDE (1R,2R)-(+)-1,2-Bis(4-nitrophenyl)ethylenediaminedihydrochloride,min.98%
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