perhydroacenaphthene

perhydroacenaphthene 구조식 이미지
카스 번호:
2146-36-3
상품명:
perhydroacenaphthene
동의어(영문):
Decahydroacenaphthene;Dodecahydroacenaphthylene;Einecs 218-412-6;perhydroacephthene;Perhydroacenaphthyle;perhydroacenaphthene;Acenaphthylene, dodecahydro-;Tricyclo[7.2.1.05,12]dodecane;Tricyclo(6,3,1,04,12)dodecane;Perhydroacenaphthene 2146-36-3 Decahydroacenaphthene
CBNumber:
CB1933376
분자식:
C12H20
포뮬러 무게:
164.29
MOL 파일:
2146-36-3.mol

perhydroacenaphthene 속성

녹는점
36℃
끓는 점
235℃
밀도
1.029 g/cm3
굴절률
1.577 (589.3 nm 20℃)
저장 조건
2-8°C
물리적 상태
액체
색상
갈색을 띤 노란색
EPA
Acenaphthylene, dodecahydro- (2146-36-3)
안전
  • 위험 및 안전 성명
  • 위험 및 사전주의 사항 (GHS)
그림문자(GHS): GHS hazard pictograms
신호 어: Danger
유해·위험 문구:
암호 유해·위험 문구 위험 등급 범주 신호 어 그림 문자 P- 코드
H304 삼켜서 기도로 유입되면 치명적일 수 있음 흡인 유해성물질 구분 1 위험 GHS hazard pictograms
예방조치문구:

perhydroacenaphthene C화학적 특성, 용도, 생산

용도

Perhydroacenaphthene or dodecahydroacenaphthylene is used in the synthesis of Alkyladamantanes by the passage of the latter over the alumina catalyst in a flow-type plant with a metal reactor that has application in the field of nanotechnology.

제조 방법

Perhydro acenaphthene is the main raw material of preparation 1,3-dimethyladamantane, is the important intermediate of preparation Derivatives of Adamantane.Derivatives of Adamantane is a kind of excellent antidementia agent, clinical research confirmation its have good efficacy to vascular dementia.
The synthesis of Perhydroacenaphthene:
1) adding industrial acenaphthylene to 95% ethanol, heating, refluxing and dissolving, then cooling, crystallizing, centrifuging to obtain refined acenaphthene, and carrying out distillation recycling of the filtrate;
2) adding the refined acenaphthene and a catalyst Raney Ni into a high-pressure kettle, replacing gas in the kettle with hydrogen, filling hydrogen to make the pressure in the kettle rise to 0.8 MPa, heating up to about 180 DEG C, starting a reaction for 5 h, continuously supplementing hydrogen during the reaction, making the pressure in the kettle rise slowly, and allowing the pressure after the reaction to be 4.0 MPa;
3) cooling after the reaction is finished, filtering the catalyst, and thus obtaining the perhydroacenaphthene.
https://patents.google.com/patent/CN105461499A/en

perhydroacenaphthene 준비 용품 및 원자재

원자재

준비 용품


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