화재 시 불을 끄기 위해 (Section 5. 폭발, 화재시 대처방법의 적절한 소화제)을(를) 사용하시오.
P403+P235
환기가 잘 되는 곳에 보관하고 저온으로 유지하시오.
P501
...에 내용물 / 용기를 폐기 하시오.
NFPA 704
2
1
0
다이메톡시메틸페닐실란 C화학적 특성, 용도, 생산
화학적 성질
Colorless or yellowish transparent liquid
용도
The reaction of dimethoxymethylphenylsilane with Li metal in excess Me3SiCl in THF to produce the products the diastereomeric isomers of 2-[2,2-bis(trimethylsilyl)ethylidene]-1-methoxy-1-methyl-3,4,5-tris(trimethylsilyl)silolane, contracted from six- to five-membered rings, as well as the expected products dimethoxymethyl(Ttc)silane synthesized via a Birch-type reductive silylation[1].
Synthesis
Sodium metal particles suspension was added to a mixture of 62.5 g of chlorobenzene and 227 g of methyltrimethoxysilane, and then 0.32 g of 15-crown-5 was added. The reaction was carried out at 38 ° C for 2 h , The reaction was stopped, and the reaction mixture was filtered and vacuum-distilled to give Dimethoxymethylphenylsilane in a yield of 87%.
