N-ACETYL-2-(4-NITROPHENYL)ETHYLAMINE

N-ACETYL-2-(4-NITROPHENYL)ETHYLAMINE 구조식 이미지
카스 번호:
6270-07-1
상품명:
N-ACETYL-2-(4-NITROPHENYL)ETHYLAMINE
동의어(영문):
Nsc 59178;Nsc 33833;Acetylnitrophenylethylamine;N-(4-NITROPHENETHYL)ACETAMIDE;N-(4-NITROPHENYLETHYL)ACETAMID;N-ACETYL-4-NITROPHENETHYLAMINE;N-(4-nitrophenylethyl)acetamide;n-[2-(4-nitrophenyl)ethyl]-acetamid;n-(2-(p-nitrophenyl)ethyl)acetamide;N-[2-(4-NITROPHENYL)ETHYL]ACETAMIDE
CBNumber:
CB2705648
분자식:
C10H12N2O3
포뮬러 무게:
208.21
MOL 파일:
6270-07-1.mol

N-ACETYL-2-(4-NITROPHENYL)ETHYLAMINE 속성

녹는점
140°C
저장 조건
2-8°C
CAS 데이터베이스
6270-07-1(CAS DataBase Reference)
EPA
Acetamide, N-[2-(4-nitrophenyl)ethyl]- (6270-07-1)

안전

HS 번호 2924.21.4500

N-ACETYL-2-(4-NITROPHENYL)ETHYLAMINE C화학적 특성, 용도, 생산

화학적 성질

Pale yellow powder

용도

N-ACETYL-2-(4-NITROPHENYL)ETHYLAMINE can be used as organic synthesis intermediate and pharmaceutical intermediate, mainly used in laboratory research and development process and chemical production process.

Synthesis

3.png
450Kg of concentrated sulfuric acid was added to the reactor, the temperature of the reaction solution was room temperature, the reaction solution containing the intermediate 1 was slowly added dropwise, and after sufficient stirring, 75 kg of 70% nitric acid was slowly added. After stirring until completion of the reaction, 800kg of crushed ice was added to the reaction solution and stirred constantly , Finally, pH was adjusted to 7~8 with ammonia solution to give crude product after filtration, crude product was recrystallized from methyl ethyl ketone to give 140 Kg of Intermediate 2, with a yield of 81.5%.

N-ACETYL-2-(4-NITROPHENYL)ETHYLAMINE 준비 용품 및 원자재

원자재

준비 용품


N-ACETYL-2-(4-NITROPHENYL)ETHYLAMINE 공급 업체

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