1-Dibenzofuranylboronic Acid
|
|
1-Dibenzofuranylboronic Acid 속성
- 끓는 점
- 438.5±37.0 °C(Predicted)
- 밀도
- 1.34±0.1 g/cm3(Predicted)
- 저장 조건
- under inert gas (nitrogen or Argon) at 2-8°C
- 물리적 상태
- powder to crystal
- 산도 계수 (pKa)
- 8.20±0.30(Predicted)
- 색상
- 흰색에서 거의 흰색
안전
- 위험 및 안전 성명
- 위험 및 사전주의 사항 (GHS)
HS 번호 | 2932.99.7000 |
---|
1-Dibenzofuranylboronic Acid C화학적 특성, 용도, 생산
용도
Dibenzo[b,d]furan-1-ylboronic acid can be used as an intermediate in organic synthesis, mainly used in laboratory research and development and chemical production processes.Synthesis
180 g (728 mmol) of 1-bromodibenzofuran aredissolved in 1500 ml of dry THF and cooled to -78?? C. 305 ml (764 mmol/2.5 M in hexane) of n-butyllithium are added at this temperature over the course of about 5 min., and the mixture is subsequently stirred at -78?? C. for a further 2.5 h. 151 g (1456 mmol) of trimethyl borate are added as rapidly as possible at this temperature, and the reaction mixture is allowed to come slowly to room temperature (about 18 h). The reaction solution is washed with water, and the precipitated solid and the organic phase are dried azeo- tropically with toluene. The crude product is washed by stirring with toluene/methylene chloride at about 40?? C. and filtered off with suction. Yield: 146 g (690 mmol), 95% of theory.
1-Dibenzofuranylboronic Acid 준비 용품 및 원자재
원자재
준비 용품
1-Dibenzofuranylboronic Acid 공급 업체
글로벌( 147)공급 업체
공급자 | 전화 | 이메일 | 국가 | 제품 수 | 이점 |
---|---|---|---|---|---|
Zhengzhou HQ Material CO.,LTD. | +86-371-55919009 +8615225108189 |
sale1@hqmat.com | China | 633 | 58 |
Xinxiang Hongqi District Houyuan Trading Co.,Ltd | +86-0373-3695376 +86-13937349994 |
HYJM@houyuanjm.com | China | 300 | 58 |
Hebei Xinsheng New Material Technology Co., LTD. | +86-16632316109 |
xinshengkeji@xsmaterial.com | China | 1100 | 58 |
Henan Fengda Chemical Co., Ltd | +86-371-86557731 +86-13613820652 |
info@fdachem.com | China | 7377 | 58 |
Shaanxi Franta Biotechnology Co., Ltd | +86-13082019107 +86-13082019107 |
admin@flanderff.com | China | 229 | 58 |
Springchem New Material Technology Co.,Limited | +86-021-62885108 +8613917661608 |
info@spring-chem.com | China | 2068 | 57 |
Shanghai Daken Advanced Materials Co.,Ltd | +86-371-66670886 |
info@dakenam.com | China | 15371 | 58 |
ATK CHEMICAL COMPANY LIMITED | +undefined-21-51877795 |
ivan@atkchemical.com | China | 32480 | 60 |
Beijing Green Guardee Technology Co., Ltd | 86-010-69706062 |
sales2@greenguardee.com | CHINA | 650 | 58 |
Shenzhen Nexconn Pharmatechs Ltd | +86-755-89396905 +86-15013857715 |
admin@nexconn.com | China | 7838 | 58 |
1-Dibenzofuranylboronic Acid 관련 검색:
dibenzo[b,d]thiophene-4-carbaldehyde
Dibenzofuran -4,6 -diborate
DIBENZOFURAN-4-CARBOXALDEHYDE 97
Dibenzothiophene-2-carboxaldehyde
Dibenzothiophene-2-boronic acid
DIBENZOFURAN-2-CARBOXALDEHYDE
2-(Dibenzo[b,d]furan-1-yl)-4,4,5,5,-tetramethyl-1,3,2-dioxaborolane
Dibenzo[b,d]furan-2-ylboronic acid
dibenzo[b,d]furan-3-ylboronic acid
Dibenzothiophene-3-boronic acid