2-Methyl-5-nitropyridine
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2-Methyl-5-nitropyridine 속성
- 녹는점
- 112 C
- 끓는 점
- 237.1±20.0 °C(Predicted)
- 밀도
- 1.246±0.06 g/cm3(Predicted)
- 저장 조건
- Inert atmosphere,Room Temperature
- 산도 계수 (pKa)
- 1.92±0.10(Predicted)
- 물리적 상태
- 고체
- 물리적 상태
- 단단한 모양
- 색상
- 밝은 노란색에서 갈색까지
- 수용성
- 물에 약간 용해됩니다.
- InChI
- InChI=1S/C6H6N2O2/c1-5-2-3-6(4-7-5)8(9)10/h2-4H,1H3
- InChIKey
- USZINSZJSVMICC-UHFFFAOYSA-N
- SMILES
- C1(C)=NC=C([N+]([O-])=O)C=C1
- CAS 데이터베이스
- 21203-68-9(CAS DataBase Reference)
안전
- 위험 및 안전 성명
- 위험 및 사전주의 사항 (GHS)
2-Methyl-5-nitropyridine C화학적 특성, 용도, 생산
용도
2-Methyl-5-nitropyridine is used as pharmaceutical intermediate.Synthesis
2-(5-nitro-pyridin-2-yl)-malonic acid diethyl ester could be used as a starting material to synthesize 2-methyl-5-nitropyridine. The specific operations are as follows: To 2-(5-nitro-pyridin-2-yl)-malonic acid diethyl ester (12.0 g, 42.5 mmol) was added cold aq. 20% sulfuric acid (120 mL) and the mixture was heated to 100 ℃ for 2h. The cooled reaction was added to a cold dilute sodium hydroxide solution and the pH adjusted to 10. The organics were extracted with dichloromethane (x 4), and then the combined organic phases were dried over sodium sulfate. The filtrate was concentrated to afford 2-methyl-5-nitropyridine (5.0 g, 83 %) as a brown solid.
2-Methyl-5-nitropyridine 준비 용품 및 원자재
원자재
5-nitro-2-phenylpyrimidine
2'-Hydroxy-4'-methyl-5'-acetylacetophenone
1-METHYL-5-NITRO-2(1H)-PYRIMIDINONE
2-Methyl-3-nitropyridine
2-Chloro-3-nitro-6-methylpyridine
DIETHYL (5-NITROPYRIDIN-2-YL)MALONATE
6-Hydroxy-5-nitro-2-picoline
N-ETHYL-4-NITROANILINE
2'-히드록시-5'-니트로아세토페논
Pyrimidine, 5-nitro- (8CI,9CI)
1-METHYL-3,5-DINITRO-1H-PYRIDIN-2-ONE
말론산 디에틸
2-Chloro-5-nitropyridine
준비 용품
2-Methyl-5-nitropyridine 공급 업체
글로벌( 292)공급 업체
| 공급자 | 전화 | 이메일 | 국가 | 제품 수 | 이점 |
|---|---|---|---|---|---|
| PNP Biotech Co. Ltd | +8618516098983 |
sales@pnpbiotech.com | China | 1001 | 58 |
| Henan Fengda Chemical Co., Ltd | +86-371-86557731 +86-13613820652 |
info@fdachem.com | China | 8095 | 58 |
| Hi-Tech Chemistry Corp | 0519-86626038 |
yuhh@hitechem.com | CHINA | 811 | 58 |
| Hangzhou FandaChem Co.,Ltd. | 008657128800458; +8615858145714 |
fandachem@gmail.com | China | 9348 | 55 |
| ATK CHEMICAL COMPANY LIMITED | +undefined-21-51877795 |
ivan@atkchemical.com | China | 32480 | 60 |
| career henan chemical co | +86-0371-86658258 |
sales@coreychem.com | China | 29914 | 58 |
| Biochempartner | 0086-13720134139 |
candy@biochempartner.com | CHINA | 967 | 58 |
| Changzhou Ansciep Chemical Co., Ltd. | +86 519 86305871 |
sales@ansciepchem.com | CHINA | 4242 | 58 |
| Shenzhen Nexconn Pharmatechs Ltd | +86-755-89396905 +86-15013857715 |
admin@nexconn.com | China | 10248 | 58 |
| Hubei Jusheng Technology Co.,Ltd. | 18871490254 |
linda@hubeijusheng.com | CHINA | 28180 | 58 |