TERT-BUTYLUREA

TERT-BUTYLUREA 구조식 이미지
카스 번호:
1118-12-3
상품명:
TERT-BUTYLUREA
동의어(영문):
T-butylurea;tert-butyl-ure;TERT-BUTYLUREA;N-TERT-BUTYLUREA;1-tert-Butylurea;Urea, tert-butyl-;tert-Butylurea,98%;mono-tert-butylurea;TIMTEC-BB SBB008606;1-tert-Butylisourea
CBNumber:
CB5469921
분자식:
C5H12N2O
포뮬러 무게:
116.16
MOL 파일:
1118-12-3.mol

TERT-BUTYLUREA 속성

녹는점
~185 °C (dec.)
끓는 점
217.23°C (rough estimate)
밀도
1.0551 (rough estimate)
굴절률
1.4432 (estimate)
산도 계수 (pKa)
14.37±0.46(Predicted)
물리적 상태
결정 또는 결정성 분말
색상
하얀색
BRN
1744501
CAS 데이터베이스
1118-12-3(CAS DataBase Reference)
EPA
tert-Butylurea (1118-12-3)

안전

위험품 표기 Xn
위험 카페고리 넘버 37-20/21/22
안전지침서 22-24/25
WGK 독일 2
RTECS 번호 YS3680000
HS 번호 29241900

TERT-BUTYLUREA C화학적 특성, 용도, 생산

화학적 성질

white crystals or crystalline powder

생산 방법

tert-Butylurea is produced by treating 1 mol urea with 2 mol of tert-butanol in the presence of 2 mol of concentrated sulfuric acid at 20–25 ℃ with ice cooling.

Purification Methods

Possible impurity is N,N'-di-tert-butyl urea which is quite insoluble in H2O. Recrystallise it from hot H2O, filter off insoluble material, and cool to 0o to -5o with stirring. Dry in vacuum at room temperature over KOH or H2SO4. If dried at higher temperatures, it sublimes slowly. It can be recrystallised from EtOH as long white needles or from 95% aqueous EtOH as plates. During melting point determination the bath temperature has to be raised rapidly as the urea sublimes slowly above 100o at 760mm. [Smith & Emerson Org Synth Coll Vol III 151 1955, Beilstein 4 IV 665.]

TERT-BUTYLUREA 준비 용품 및 원자재

원자재

준비 용품


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