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TERT-BUTYL 4-BROMOBENZYLCARBAMATE

TERT-BUTYL 4-BROMOBENZYLCARBAMATE 구조식 이미지

카스 번호:: 68819-84-1

상품명:: TERT-BUTYL 4-BROMOBENZYLCARBAMATE

동의어(영문):: N-BOC-4-broMobenzylaMine;4-Bromo-N-BOC-benzylamine;TERT-BUTYL 4-BROMOBENZYLCARBAMATE;tert-Butyl N-(4-bromobenzyl)carbamate;tert-Butyl 4-bromobenzylcarbamate 98%;tert-butyl N-[(4-bromophenyl)methyl]carbamate;N-(4-Bromobenzyl)carbamic acid tert-butyl ester;(4-BROMO-BENZYL)-CARBAMIC ACID TERT-BUTYL ESTER;Carbamic acid, (4-bromophenyl)methyl-, 1,1-dimethylethyl ester;N-[(4-Bromophenyl)methyl]-carbamic acid 1,1-dimethylethyl ester

CBNumber:: CB6838195

분자식:: C12H16BrNO2

포뮬러 무게:: 286.16

MOL 파일:: 68819-84-1.mol

속성

안전

용도

공급 업체 114

TERT-BUTYL 4-BROMOBENZYLCARBAMATE 속성

녹는점: 86-88℃

끓는 점: 374.3±25.0 °C(Predicted)

밀도: 1.319±0.06 g/cm3(Predicted)

저장 조건: Sealed in dry,Room Temperature

물리적 상태: 고체

물리적 상태: 단단한 모양

산도 계수 (pKa): 12.05±0.46(Predicted)

색상: 회백색

안전

위험 및 안전 성명
위험 및 사전주의 사항 (GHS)

위험품 표기	Xn
위험 카페고리 넘버	22
HS 번호	2924297099

그림문자(GHS):

신호 어:

Warning

유해·위험 문구:

암호	유해·위험 문구	위험 등급	범주	신호 어	P- 코드
H315	피부에 자극을 일으킴	피부부식성 또는 자극성물질	구분 2	경고	P264, P280, P302+P352, P321,P332+P313, P362
H319	눈에 심한 자극을 일으킴	심한 눈 손상 또는 자극성 물질	구분 2A	경고	P264, P280, P305+P351+P338,P337+P313P
H335	호흡 자극성을 일으킬 수 있음	특정 표적장기 독성 - 1회 노출;호흡기계 자극	구분 3	경고

예방조치문구:

P280	보호장갑/보호의/보안경/안면보호구를 착용하시오.
P301+P312	삼켜서 불편함을 느끼면 의료기관(의사)의 진찰을 받으시오.

TERT-BUTYL 4-BROMOBENZYLCARBAMATE C화학적 특성, 용도, 생산

Synthesis

Tert-Butyl 4-bromobenzylcarbamate is prepared by the reaction of di-tert-butyl dicarbonate and 4-bromobenzylamine hydrochloride. The specific synthesis steps are as follows:
To a stirred suspension of 4-bromo-benzylamine hydrochloride (968mg, 4.35mmol) and triethylamine (0.666ml, 4.79mmol) in chloroform (15ml) was added di-tert-butyldicarbonate (949mg, 4.35mmol). The resulting solution was stirred at ambient temperature for 2h and then diluted with DCM (40ml). The organic solution was washed sequentially with 10% aqueous citric acid (40ml) and brine (40ml). The organic phase was dried over anhydrous magnesium sulfate and the filtrate evaporated at reduced pressure to afford Tert-Butyl 4-bromobenzylcarbamate (1.23g, 99%). 1H NMR 7.48-7.43 (2H, m), 7.18 (2H, d, 8.4), 4.84 (1H, br s), 4.27 (2H, d, 5.7), 1.46 (9H, s).

TERT-BUTYL 4-BROMOBENZYLCARBAMATE 준비 용품 및 원자재

원자재

준비 용품

tert-Butyl 4-ethynylbenzylcarbamate (4-IODO-BENZYL)-CARBAMIC ACID TERT-BUTYL ESTER [1-(4-BROMO-PHENYL)-ETHYL]-CARBAMIC ACID TERT-BUTYL ESTER 4-AMINOMETHYLPHENYLBORONIC ACID, PINACOL ESTER, HCL (4-BROMO-BENZYL)-METHYL-CARBAMIC ACID TERT-BUTYL ESTER Methyl 3-(4-((tert-butoxycarbonylaMino)Methyl)phenylsulfonyl)propanoate

TERT-BUTYL 4-BROMOBENZYLCARBAMATE 공급 업체

글로벌( 114)공급 업체

공급자	전화	이메일	국가	제품 수	이점
Accela ChemBio Inc.	(+1)-858-699-3322	info@accelachem.com	United States	19965	58
Alchem Pharmtech,Inc.	8485655694	sales@alchempharmtech.com	United States	63711	58
career henan chemical co	+86-0371-86658258 15093356674;	factory@coreychem.com	China	29826	58
Hubei Ipure Biology Co., Ltd	+8613367258412	ada@ipurechemical.com	China	10326	58
HONG KONG IPURE BIOLOGY CO.,LIMITED	86 18062405514 18062405514	ada@ipurechemical.com	CHINA	3465	58
Shanxi Xuanran Import and Export Trade Co., Ltd.	+8617735180244	mike_yan@xuanranglobal.com	CHINA	4022	58
Blocksynth Pharmaceutical Technology Co.,Ltd	0086-19817745290; +8619817745290	bd@blocksynth.com	China	5657	58
Labnetwork lnc.	+86-27-50766799 +8618062016861	contact@labnetwork.com	China	19994	58
Hefei TNJ Chemical Industry Co.,Ltd.	0551-65418684 +8618949823763	sales@tnjchem.com	China	25363	58
LEAP CHEM CO., LTD.	+86-852-30606658	market18@leapchem.com	China	24738	58

TERT-BUTYL 4-BROMOBENZYLCARBAMATE 관련 검색:

N-Boc-4-(Cyclopropylmethyl)piperazine 1-BOC-4-(1-PYRROLIDINYL)-3,6-DIHYDRO-2H-PYRIDINE 2(1H)-ISOQUINOLINECARBOXYLIC ACID, 3,4-DIHYDRO-7-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-, 1,1-DIMETHYLETHYL ESTER tert-butyl 4-(2-bromo-5-fluoropyridin-4-yl)-4-hydroxypiperidine-1-carboxylate 1-N-Boc-4-(Phenylamino)piperidine tert-butyl 4-(2-aminoethyl)-3,3-difluoropiperidine-1-carboxylate 4-(3-AMINO-PHENYL)-PIPERIDINE-1-CARBOXYLIC ACID TERT-BUTYL ESTER 1-Boc-4-(2-hydroxyethyl)piperidine tert-butyl 4-(3-cyano-4-(methoxycarbonyl)phenyl)piperazine-1-carboxylate tert-butyl 5-tert-butylisoxazol-3-ylcarbamate 1-Piperazinecarboxylic acid, 4-[3-bromo-4-(methoxycarbonyl)phenyl]-, 1,1-dimethylethyl ester 5H-Pyrrolo[3,2-c]pyridine-5-carboxylic acid, 1,4,6,7-tetrahydro-4-oxo-2-(4-pyridinyl)-, 1,1-dimethylethyl ester INDEX NAME NOT YET ASSIGNED Pentanoic acid, 4,5-diamino-5-oxo-, 1,1-dimethylethyl ester Boc-4-Bromo-L-beta-phenylalanine Boc-4-Bromo-D-beta-phenylalanine (4-Bromophenyl)-tert-butoxycarbonylaminoacetic acid methyl ester (R,S)-Boc-3-amino-3-(4-bromophenyl)-propionic acid