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BIS(2,2,2-TRIFLUOROETHYL) PHOSPHITE

BIS(2,2,2-TRIFLUOROETHYL) PHOSPHITE 구조식 이미지

카스 번호:: 92466-70-1

상품명:: BIS(2,2,2-TRIFLUOROETHYL) PHOSPHITE

동의어(영문):: BIS(2,2,2-TRIFLUOROETHYL) PHOSPHITE;BIS(2,2,2-TRIFLUOROETHYL) PHOSPHONATE;Bis(2,2,2-trifluoroethyl) Phosphite >PHOSPHONIC ACID BIS(2,2,2-TRIFLUOROETHYL) ESTER;BIS(2,2,2-TRIFLUOROETHYL) PHOSPHITE, TEC H., 90%;PHOSPHOROUS ACID BIS(2,2,2-TRIFLUOROETHYL) ESTER;Bis(2,2,2-trifluoroethyl) phosphite technical grade, 90%;Bis(2,2,2-trifluoroethyl) phosphite,Phosphonic acid bis(2,2,2-trifluoroethyl) ester;Bis(2,2,2-trifluoroethyl) Phosphonate Phosphonic Acid Bis(2,2,2-trifluoroethyl) Ester Phosphorous Acid Bis(2,2,2-trifluoroethyl) Ester

CBNumber:: CB8384111

분자식:: C4H5F6O3P

포뮬러 무게:: 246.04

MOL 파일:: 92466-70-1.mol

속성

안전

용도

공급 업체 50

BIS(2,2,2-TRIFLUOROETHYL) PHOSPHITE 속성

끓는 점: 43-44 °C/2 mmHg (lit.)

밀도: 1.545 g/mL at 25 °C (lit.)

굴절률: n20/D 1.332(lit.)

인화점: 169 °F

물리적 상태: 액체

색상: 무색 내지 거의 무색

안전

위험 및 안전 성명
위험 및 사전주의 사항 (GHS)

위험품 표기	Xi
위험 카페고리 넘버	36/37/38
안전지침서	23-26-28-36
WGK 독일	3
HS 번호	2920.90.5100

그림문자(GHS):

신호 어:

Warning

유해·위험 문구:

암호	유해·위험 문구	위험 등급	범주	신호 어	P- 코드
H315	피부에 자극을 일으킴	피부부식성 또는 자극성물질	구분 2	경고	P264, P280, P302+P352, P321,P332+P313, P362
H319	눈에 심한 자극을 일으킴	심한 눈 손상 또는 자극성 물질	구분 2A	경고	P264, P280, P305+P351+P338,P337+P313P
H335	호흡 자극성을 일으킬 수 있음	특정 표적장기 독성 - 1회 노출;호흡기계 자극	구분 3	경고

예방조치문구:

P302+P352	피부에 묻으면 다량의 물로 씻으시오.
P305+P351+P338	눈에 묻으면 몇 분간 물로 조심해서 씻으시오. 가능하면 콘택트렌즈를 제거하시오. 계속 씻으시오.

NFPA 704

	2
2		0

BIS(2,2,2-TRIFLUOROETHYL) PHOSPHITE C화학적 특성, 용도, 생산

Synthesis Reference(s)

Synthesis, p. 410, 1984 DOI: 10.1055/s-1984-30856

Synthesis

The synthesis method of Bis(2,2,2-trifluoroethyl) Phosphite is as follows: A solution of phosphorus trichloride (43.5 mL, 0.50 mol) in dichloromethane (100 mL) was placed in an oven dried 1L round bottom flask. A reflux condenser and pressure equalizing addition funnel were attached to the round bottom flask. The addition funnel was charged with a solution of 2-methyl-2-propanol (48.0 mL, 0.50 mol) in dichloromethane (100 mL), and then the contents of the addition funnel were added in a dropwise manner to the round bottom flask under argon gas at 0 ℃over the course of 30 min. The reaction mixture was allowed to stir for an additional 30 min, then the addition funnel is recharged with a solution of 2,2,2-trifluoroethanol (70.0 mL, 0.96 mol) and dichloromethane (100 mL) and then the contents of the addition funnel were added in a dropwise manner to the round bottom flask under argon gas at 0 ℃ over the course of 30 min. The reaction mixture was then allowed to stir at RT overnight. The gaseous vapors were then degassed into NaOH (30.2 g, 0.98 mol) in 200 mL of water over the course of 8 hrs. The solvents were removed by rotary evaporation and the crude material was fractionally distilled under reduced pressure yielding Bis(2,2,2-trifluoroethyl) Phosphite (100.89 g, 0.41 mol, 82.2%) as colorless liquid.

BIS(2,2,2-TRIFLUOROETHYL) PHOSPHITE 준비 용품 및 원자재

원자재

준비 용품

ETHYL [BIS(2,2,2-TRIFLUOROETHOXY)PHOSPHINYL]ACETATE

BIS(2,2,2-TRIFLUOROETHYL) PHOSPHITE 공급 업체

글로벌( 50)공급 업체

공급자	전화	이메일	국가	제품 수	이점
Hubei xin bonus chemical co. LTD	86-13657291602	linda@hubeijusheng.com	CHINA	22968	58
career henan chemical co	+86-0371-86658258 15093356674;	factory@coreychem.com	China	29826	58
Shaanxi Dideu Medichem Co. Ltd	18192627656	1012@dideu.com	China	3453	58
Career Henan Chemica Co	+86-0371-86658258 15093356674;	laboratory@coreychem.com	China	30255	58
Dayang Chem (Hangzhou) Co.,Ltd.	571-88938639 +8617705817739	info@dycnchem.com	CHINA	52867	58
LEAP CHEM CO., LTD.	+86-852-30606658	market18@leapchem.com	China	24738	58
Aladdin Scientific	+1-833-552-7181	sales@aladdinsci.com	United States	57511	58
Amadis Chemical Company Limited	571-89925085	sales@amadischem.com	China	131981	58
J & K SCIENTIFIC LTD.	010-82848833 400-666-7788	jkinfo@jkchemical.com	China	94838	76
Meryer (Shanghai) Chemical Technology Co., Ltd.	4006608290; 18621169109	market03@meryer.com	China	40241	62

BIS(2,2,2-TRIFLUOROETHYL) PHOSPHITE 관련 검색:

BIS(2,2,2-TRIFLUOROETHYL) (METHOXYCARBONYLMETHYL)PHOSPHONATE Phosphite BIS(2,2,2-TRIFLUOROETHYL) PHOSPHITE alamifovir [BIS-(2,2,2-TRIFLUORO-ETHOXY)-PHOSPHORYL]-BROMO-ACETIC ACID METHYL ESTER ETHYL [BIS(2,2,2-TRIFLUOROETHOXY)PHOSPHINYL]ACETATE BIS-(2,2,2-TRIFLUOROETHYL) METHOXYCARBONYLMETHYL PHOSPHONATE, [1,2-14C] ETHYL 2-[BIS(2,2,2-TRIFLUOROETHYL)PHOSPHONO] PROPIONATE [2-(2-AMINO-6-CHLORO-PURIN-9-YL)-ETHOXYMETHYL]-PHOSPHONIC ACID BIS-(2,2,2-TRIFLUORO-ETHYL) ESTER TRIS(2,2,2-TRIFLUOROETHYL)PHOSPHATE BIS(TRIFLUOROETHYL) METHYLPHOSPHONATE