t-Butyl (E)-4-Iodo-2-methyl-2-butenoate

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Products Intro:	Product Name:t-Butyl (E)-4-Iodo-2-methyl-2-butenoate CAS:53689-87-5

t-Butyl (E)-4-Iodo-2-methyl-2-butenoate Basic information

Product Name:	t-Butyl (E)-4-Iodo-2-methyl-2-butenoate
Synonyms:	t-Butyl (E)-4-Iodo-2-methyl-2-butenoate;2-Butenoic acid, 4-iodo-2-methyl-, 1,1-dimethylethyl ester;t-butyl γ-iodotiglate
CAS:	53689-87-5
MF:	C9H15IO2
MW:	282.12
EINECS:
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Mol File:	53689-87-5.mol

t-Butyl (E)-4-Iodo-2-methyl-2-butenoate Chemical Properties

Boiling point

80 °C/0.005 mmHg

Safety Information

MSDS Information

t-Butyl (E)-4-Iodo-2-methyl-2-butenoate Usage And Synthesis

Reactivity Profile	t-Butyl (E)-4-Iodo-2-methyl-2-butenoate could be used in egioselective annulations; methyl vinyl ketone equivalent.
Synthesis	Treatment of Chloroacetaldehyde with the phosphorane shown in eq 1 followed by halogen exchange with Sodium Iodide/acetone affords t-Butyl (E)-4-Iodo-2-methyl-2-butenoate in 76% overall yield.
References	1. (a) Gawley, R. E. S 1976, 777; (b) Hill, K. H. Ph.D. Thesis, University of Texas, Austin, TX, 1972. 2. (a) Stotter, P. L.; Hill, K. A. TL 1975, 16, 1679. (b) Stotter, P. L.; Hill, K. A. JACS 1974, 96, 6524. 3. Weinstock, J. JOC 1961, 26, 3511.

t-Butyl (E)-4-Iodo-2-methyl-2-butenoate Preparation Products And Raw materials

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