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2,3-DICHLOROANISOLE

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Company Name: Capot Chemical Co.,Ltd.
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Products Intro: Product Name:2,3-Dichloroanisole
CAS:1984-59-4
Purity:98%(Min GC HPLC)g point Package:1G;1KG;100KG
Company Name: Nanjing ChemLin Chemical Industry Co., Ltd.
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Products Intro: CAS:1984-59-4
Purity:98% Package:g-Kg Remarks:Colorless transparent liquid
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Products Intro: CAS:1984-59-4
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Products Intro: Product Name: 2,3-DICHLOROANISOLE
CAS:1984-59-4
Purity:99% Package:1kg;8USD
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Products Intro: Product Name:2,3-Dichloro Anisole
CAS:1984-59-4

2,3-DICHLOROANISOLE manufacturers

  • 2,3-Dichloroanisole
  • 2,3-Dichloroanisole pictures
  • $138.00 / 500mg
  • 2026-05-11
  • CAS:1984-59-4
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  • Purity: 99.90%
  • Supply Ability: 10g
  • 2,3-Dichloroanisole
  • 2,3-Dichloroanisole pictures
  • $138.00 / 500mg
  • 2026-04-22
  • CAS:1984-59-4
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  • Purity: 99.90%
  • Supply Ability: 10g
  • 2,3-DICHLOROANISOLE
  •  	2,3-DICHLOROANISOLE pictures
  • $8.00 / 1kg
  • 2019-07-06
  • CAS:1984-59-4
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  • Purity: 99%
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2,3-DICHLOROANISOLE Basic information
Product Name:2,3-DICHLOROANISOLE
Synonyms:1,2-DICHLORO-3-METHOXYBENZENE;DICHLOROANISOLE(2,3-);1,2-dichloro-3-methoxy-benzen;2,3-DICHLOROMETHOXYBENZENE;2,3-DICHLOROANISOLE;2,3-DICHLORANISOL;ATRAZIN-2-HYDROXY PESTANAL, 250 MG;2,3-DICHLOROANISOLE, 97+%
CAS:1984-59-4
MF:C7H6Cl2O
MW:177.03
EINECS:217-853-1
Product Categories:Aromatics, Metabolites and Impurities, Pharmaceuticals, Intermediates & Fine Chemicals;Halogenated benzene series;Aromatic Ethers;Anisole;Anisoles, Alkyloxy Compounds & Phenylacetates;Chlorine Compounds
Mol File:1984-59-4.mol
2,3-DICHLOROANISOLE Structure
2,3-DICHLOROANISOLE Chemical Properties
Melting point 31-33 °C(lit.)
Boiling point 115-116°C 12mm
density 1.2970 (rough estimate)
refractive index 1.5430 (estimate)
Fp >230 °F
storage temp. Inert atmosphere,Room Temperature
solubility Chloroform, Methanol
form Solid
color Off-White
Water Solubility Soluble in water (86.9 mg/L).
BRN 1909166
Henry's Law Constant2.2×10-2 mol/(m3Pa) at 25℃, Pfeifer et al. (2001)
InChIInChI=1S/C7H6Cl2O/c1-10-6-4-2-3-5(8)7(6)9/h2-4H,1H3
InChIKeyHFEASCCDHUVYKU-UHFFFAOYSA-N
SMILESC1(Cl)=CC=CC(OC)=C1Cl
CAS DataBase Reference1984-59-4(CAS DataBase Reference)
EPA Substance Registry System2,3-Dichloroanisole (1984-59-4)
Safety Information
Hazard Codes Xn
Risk Statements 36/37/38-20/22
Safety Statements 22-24/25-37/39-26
WGK Germany 3
TSCA TSCA listed
HS Code 29093090
Storage Class11 - Combustible Solids
MSDS Information
ProviderLanguage
ACROS English
SigmaAldrich English
ALFA English
2,3-DICHLOROANISOLE Usage And Synthesis
Chemical Propertieswhite to brownish crystalline low melting solid
UsesThe product has been used to develop an analytical method for the determination of biogenic halogenated anisoles in the picogram/m3 range in air.
Agricultural Uses2,3-Dichloroanisole is a volatile organic compound that has been shown to be an attractant for termites. It is used as a pesticide and agrochemical. 2,3-Dichloroanisole is used as an insecticide against termites and other pests in agriculture. This chemical has been shown to inhibit the sodium channel of the nerve cell membrane, which leads to paralysis of insects. The mechanism of action for this compound is not well understood but it has been suggested that it may act by blocking the reorientation of the sodium ion channels. 2,3-Dichloroanisole can also be used as a metal salt in some thermodynamic reactions.
Synthesis
2,3-Dichlorophenol

576-24-9

Dimethyl sulfate

77-78-1

2,3-DICHLOROANISOLE

1984-59-4

General procedure for the synthesis of 2,3-dichloroanisole from 2,3-dichlorophenol and dimethyl sulfate: 2,3-dichlorophenol (20.0 g, 122.7 mmol) was placed in a reaction flask, 120 mL of acetone was added to dissolve it, followed by the addition of potassium carbonate (18.7 g, 135.0 mmol), and magnetically stirred for 0.5 hours. Then dimethyl sulfate (17.0 g, 135.0 mmol) was slowly added dropwise through a dropping funnel and heated to 60°C and refluxed for 3 hours. The progress of the reaction was monitored by thin layer chromatography (TLC) (unfolding agent: petroleum ether/ethyl acetate=5:1, Rf=0.8). After completion of the reaction, it was cooled to room temperature, potassium carbonate was removed by filtration with a pump and the filter cake was washed with acetone. After evaporation to remove acetone, ethyl acetate and saturated sodium bicarbonate solution were added sequentially, and the organic phase was washed twice each time with saturated aqueous sodium chloride solution, and then the organic phase was dried with anhydrous sodium sulfate. After filtration, the solvent was evaporated under reduced pressure to give 2,3-dichloroanisole. The product was a colorless oil with a yield of 21.5 g and 99.1%.

References[1] Patent: CN106916116, 2017, A. Location in patent: Paragraph 0063; 0064; 0065
[2] Recueil des Travaux Chimiques des Pays-Bas, 1918, vol. 37, p. 105
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