1,4-苯二甲硫醇(105-09-9)核磁图(¹³CNMR)

Mass

MS-IW-4109          
p-phenylenebis(methanethiol)
C8H10S2             (Mass of molecular ion:    170)

   Source Temperature: 230 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      34.0       2.1
      39.0       3.2
      45.0      17.0
      47.0       2.0
      50.0       1.7
      51.0       5.1
      52.0       2.2
      59.0       2.3
      63.0       3.0
      65.0       3.5
      67.0       3.2
      68.0       6.1
      69.0       1.1
      76.0       1.3
      77.0       8.3
      78.0       8.2
      79.0       1.4
      89.0       3.3
      90.0       1.6
      91.0      25.7
      92.0       2.6
      93.0       3.9
      97.0       1.4
     102.0       2.2
     103.0      13.7
     104.0      62.4
     105.0       6.2
     121.0       2.3
     123.0       5.4
     134.0       2.2
     135.0       7.7
     136.0       2.9
     137.0     100.0
     138.0      10.0
     139.0       5.1
     170.0      39.4
     171.0       4.1
     172.0       3.8

Parameter ppm Hz D(A) 7.263 D(B) 3.710 D(C) 1.745 J(B,C) 7.57

     Hz     ppm     Int.

   2178.90   7.263   1000
   1116.81   3.723    495
   1109.27   3.698    508
    531.03   1.770    129
    523.48   1.745    246
    515.94   1.720    123