1119-49-9

N-丁基乙酰胺(1119-49-9)核磁图(¹HNMR)

产品名称:N-丁基乙酰胺

CAS:1119-49-9

分子式:C6H13NO

分子量: 115.17

InChI:InChI=1S/C6H13NO/c1-3-4-5-7-6(2)8/h3-5H2,1-2H3,(H,7,8)

InChIKey: GYLDXXLJMRTVSS-UHFFFAOYSA-N

Smiles:C(NCCCC)(=O)C

¹HNMR

¹³CNMR

IR1

Mass

MS-IW-3841          
n-butylacetamide
C6H13NO             (Mass of molecular ion:    115)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       6.4
      18.0       3.1
      26.0       1.4
      27.0      12.9
      28.0      26.4
      29.0      13.9
      30.0     100.0
      31.0       7.5
      32.0       4.0
      38.0       1.1
      39.0      10.4
      40.0       2.3
      41.0      22.0
      42.0      13.5
      43.0      94.2
      44.0      60.9
      45.0       6.2
      53.0       1.4
      54.0       1.5
      55.0       5.3
      56.0       9.8
      57.0       8.9
      58.0      12.7
      59.0       2.4
      60.0      31.8
      61.0       1.0
      70.0       1.0
      72.0      98.8
      73.0      79.2
      74.0       3.5
      86.0      33.5
      87.0       4.2
     100.0      23.4
     101.0       1.4
     115.0      50.8
     116.0       4.5

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₆ H₁₃ N O	0.05 ml : 0.5 ml CDCl₃
N-butylacetamide

    Assign.     Shift(ppm)

      A             7.05
      B             3.214
      C             1.983
      D             1.489
      E             1.352
      F             0.919

     Hz     ppm     Int.

   2815.67   7.046     36
   1294.68   3.240    113
   1288.82   3.225    157
   1287.48   3.222    195
   1281.74   3.208    197
   1280.27   3.204    158
   1274.54   3.190    128
    792.60   1.984   1000
    612.06   1.532     39
    611.33   1.530     37
    604.98   1.514    107
    602.05   1.507     57
    597.05   1.494    165
    594.48   1.488     97
    590.45   1.478    125
    589.72   1.476    127
    587.52   1.471     69
    582.52   1.458     71
    582.03   1.457     70
    558.35   1.398     45
    551.15   1.380    115
    546.02   1.367     56
    543.95   1.362    140
    543.33   1.360    144
    542.60   1.358    130
    538.57   1.348     61
    535.28   1.340    151
    531.37   1.330     33
    528.32   1.322     92
    521.36   1.305     34
    374.51   0.938    414
    367.19   0.919    726
    362.55   0.908     43
    359.86   0.901    353

in CDCl3