111928-07-5

四乙基六氟磷酸盐(111928-07-5)核磁图(¹HNMR)

产品名称:四乙基六氟磷酸盐

CAS:111928-07-5

分子式:C8H20F6P2

分子量: 292.18

Mass

MS-KW-0597          
tetraethylphosphonium hexafluorophosphate 
C8H20F6P2           (Mass of molecular ion:    292)

   Source Temperature: 210 °C
   Sample Temperature: 250 °C
   Direct, 75 eV

      17.0       1.7
      18.0       8.3
      20.0      18.3
      25.0       1.6
      26.0       9.1
      27.0      25.5
      28.0      15.7
      29.0      22.7
      31.0       1.4
      34.0       3.7
      39.0       7.5
      40.0       2.4
      41.0      25.3
      42.0       2.1
      43.0       8.4
      44.0       9.2
      45.0      15.1
      46.0       2.5
      47.0      10.0
      48.0       6.9
      49.0       3.1
      50.0       2.7
      53.0       2.6
      54.0       1.2
      55.0      27.9
      56.0       3.7
      57.0      34.1
      58.0      15.4
      59.0      43.7
      60.0      12.8
      61.0      91.4
      62.0     100.0
      63.0       6.2
      67.0       1.3
      69.0      14.0
      70.0       1.0
      71.0       5.0
      72.0       2.1
      73.0      10.8
      74.0       4.3
      75.0      66.4
      76.0      11.7
      77.0       2.8
      78.0       1.9
      79.0       1.1
      83.0       2.5
      85.0      22.6
      87.0       5.0
      88.0      21.0
      89.0      17.0
      90.0      88.7
      91.0       5.1
     101.0       2.4
     102.0       4.6
     103.0      19.8
     104.0      31.6
     105.0       2.3
     106.0       2.0
     107.0      50.2
     115.0       1.1
     116.0       4.1
     117.0      37.2
     118.0      50.4
     119.0       4.0
     130.0       2.4
     131.0       1.2
     132.0       3.2
     137.0       1.2
     145.0      13.2
     146.0      31.4
     147.0      11.7
     158.0       1.5

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₈H₂₀P PF₆	0.038 g : 0.5 ml DMSO-d₆
tetraethylphosphonium hexafluorophosphate

    Assign.     Shift(ppm)

     A           2.203
     B           1.132

     Hz     ppm     Int.

    898.93   2.249    143
    891.24   2.230    460
    885.63   2.216    175
    883.55   2.211    487
    877.93   2.197    461
    875.86   2.191    191
    870.24   2.177    458
    862.68   2.158    152
    468.76   1.173    506
    461.19   1.154   1000
    453.37   1.135    486
    450.81   1.128    513
    443.12   1.109    992
    435.43   1.090    459

in DMSO-d6