吡啶硫酮(1121-30-8)核磁图(1HNMR)
InChI:InChI=1S/C5H5NOS/c7-6-4-2-1-3-5(6)8/h1-4,7H
InChIKey: YBBJKCMMCRQZMA-UHFFFAOYSA-N
Smiles:C1(=S)N(O)C=CC=C1
400 MHz in CDCl3
90 MHz in CDCl3
-
| 1H NMR |
399.65 MHz |
| C5H5NOS
|
0.038 g : 0.5 ml CDCl3
|
| 1-hydroxy-2(1H)-pyridinethione
|
 |
Assign. Shift(ppm)
A 12.1
B 8.100
C 7.673
D 7.293
E 6.804
|
Hz ppm Int.
4864.32 12.168 651
3242.63 8.111 654
3242.08 8.110 698
3241.17 8.108 690
3240.62 8.106 621
3235.86 8.095 662
3235.31 8.093 709
3234.39 8.091 691
3233.84 8.089 621
3072.83 7.687 581
3072.28 7.685 599
3071.18 7.683 596
3070.63 7.681 552
3064.22 7.665 639
3063.67 7.664 655
3062.57 7.661 656
3062.02 7.660 612
2923.90 7.314 531
2922.44 7.311 553
2919.32 7.303 184
2916.76 7.296 620
2915.29 7.293 1000
2913.83 7.289 520
2908.15 7.275 511
2906.68 7.271 521
2727.54 6.823 460
2725.89 6.819 468
2720.58 6.806 686
2718.93 6.802 673
2713.61 6.788 424
2711.97 6.784 405
-
| 1H NMR |
89.56 MHz |
| C5 H5 N O S
|
0.034 g : 0.5 ml CDCl3
|
| 1-hydroxy-2(1H)-pyridinethione
|
|
Assign. Shift(ppm)
A 11.
B 8.090
C 7.663
D 7.282
E 6.793
|
Hz ppm Int.
740.33 8.267 30
739.65 8.259 32
739.31 8.255 33
738.96 8.252 34
738.11 8.242 35
737.77 8.238 36
737.34 8.233 40
736.66 8.226 40
735.97 8.218 44
735.38 8.212 43
733.75 8.193 47
728.71 8.137 619
727.51 8.124 628
721.96 8.062 690
720.76 8.048 686
716.32 7.999 30
692.40 7.732 480
690.86 7.714 515
683.85 7.636 784
682.23 7.618 824
676.93 7.559 65
675.82 7.547 52
665.73 7.434 30
660.52 7.376 529
658.98 7.358 568
656.08 7.326 67
653.34 7.295 997
651.81 7.278 1000
650.44 7.263 404
644.80 7.200 475
643.26 7.183 490
636.68 7.109 38
635.57 7.097 32
615.49 6.873 418
613.70 6.853 421
608.48 6.795 627
606.77 6.776 620
603.61 6.740 82
601.65 6.718 284
599.85 6.698 274