13368-42-8

N-(三甲基硅基)吗啉(13368-42-8)核磁图(¹³CNMR)

产品名称:N-(三甲基硅基)吗啉

CAS:13368-42-8

分子式:C7H17NOSi

分子量: 159.3

InChI:InChI=1S/C7H17NOSi/c1-10(2,3)8-4-6-9-7-5-8/h4-7H2,1-3H3

InChIKey: JJOWIQMPCCUIGA-UHFFFAOYSA-N

Smiles:N1([Si](C)(C)C)CCOCC1

Mass

MS-NW-9945          
4-(trimethylsilyl)morpholine
C7H17NOSi           (Mass of molecular ion:    159)

   Source Temperature: 210 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      15.0       1.5
      27.0       3.4
      28.0      15.7
      29.0      19.4
      30.0       8.4
      31.0       4.1
      41.0       2.6
      42.0       7.4
      43.0      11.3
      44.0       4.8
      45.0      22.3
      46.0       1.5
      47.0       2.2
      52.0       1.2
      54.0       1.8
      55.0       6.6
      56.0      13.4
      57.0      28.9
      57.5       2.1
      58.0       6.3
      59.0      52.4
      60.0       4.1
      61.0       3.3
      66.0       2.9
      70.0       3.7
      71.0       2.1
      72.0       4.1
      73.0      81.0
      74.0       7.3
      75.0      22.8
      76.0       1.7
      77.0       2.4
      85.0       1.7
      86.0     100.0
      87.0      32.3
      88.0       5.3
      89.0       2.4
      93.0       1.2
     100.0      16.8
     101.0      83.4
     102.0      10.2
     103.0       9.8
     114.0      13.5
     115.0       2.3
     116.0       1.6
     128.0       1.6
     129.0      11.0
     130.0       2.0
     131.0       2.2
     144.0      74.5
     145.0       9.2
     146.0       3.5
     147.0      34.7
     148.0       5.5
     149.0       3.3
     158.0      20.2
     159.0      71.6
     160.0      11.2
     161.0       3.3
     229.0       1.5

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₇ H₁₇ N O Si	0.05 ml : 0.5 ml CDCl₃
4-(trimethylsilyl)morpholine

    Assign.     Shift(ppm)

      A             3.550
      B             2.827
      C             0.044

     Hz     ppm     Int.

   1423.71   3.563    139
   1419.19   3.552    154
   1414.43   3.540    163
   1134.64   2.840    150
   1129.88   2.828    158
   1125.24   2.816    159
     22.22   0.056     47
     21.24   0.054     76
     17.82   0.045   1000
     14.77   0.037    144

in CDCl3