135984-01-9

1,5-二苯基-3-(2-噻吩基)甲(135984-01-9)核磁图(¹HNMR)

产品名称:1,5-二苯基-3-(2-噻吩基)甲

CAS:135984-01-9

分子式:C17H14N4S

分子量: 306.38

InChI:InChI=1S/C17H14N4S/c1-3-8-14(9-4-1)18-20-17(16-12-7-13-22-16)21-19-15-10-5-2-6-11-15/h1-13,18H

InChIKey: YYNVZGCGVPELJN-UHFFFAOYSA-N

Smiles:C(=NNC1=CC=CC=C1)(N=NC1=CC=CC=C1)C1SC=CC=1

¹HNMR

¹³CNMR

IR1

400 MHz in CDCl3

90 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₇ H₁₄ N₄ S	0.040 g : 0.5 ml CDCl₃
1,5-diphenyl-3-(2-thienyl)formazan

    Assign.     Shift(ppm)

      A            14.23
      B             7.63
      C             7.62
      D             7.42
      E             7.25
      F             7.25
      G             7.068
     
     J(B,F)=1.2HZ. J(B,G)=3.8HZ. J(F,G)=5.1HZ.
     90MHZ. : HSP-03-424

     Hz     ppm     Int.

   5685.30  14.226    276
   3066.89   7.674     36
   3065.92   7.672     42
   3063.23   7.665     46
   3062.01   7.662     53
   3060.79   7.659     50
   3054.69   7.644    376
   3053.47   7.641    413
   3050.78   7.634    861
   3049.56   7.631   1000
   3047.61   7.626    278
   3041.99   7.612    877
   3041.02   7.610    804
   3039.06   7.605    138
   2984.62   7.469     31
   2983.15   7.465     34
   2977.78   7.451     78
   2975.83   7.447    165
   2974.12   7.442    577
   2972.17   7.437    233
   2966.80   7.424    850
   2960.21   7.408    247
   2958.50   7.403    568
   2956.54   7.398    100
   2908.69   7.279     55
   2907.96   7.277     57
   2905.27   7.270    227
   2904.05   7.267    352
   2903.08   7.265    231
   2898.19   7.252    515
   2896.97   7.249    767
   2893.07   7.240    369
   2891.85   7.236    351
   2890.63   7.233    179
   2889.40   7.230    243
   2888.43   7.228    140
   2828.61   7.078    328
   2824.95   7.069    331
   2823.49   7.065    308
   2819.82   7.056    281

¹H NMR	89.56 MHz
C₁₇ H₁₄ N₄ S	0.040 g : 0.5 ml CDCl₃
1,5-diphenyl-3-(2-thienyl)formazan

    Assign.     Shift(ppm)

      A            14.19
      B             7.64
      C             7.61
      D             7.42
      E             7.25
      F             7.24
      G             7.069
     
     400MHZ. : HSP-41-319

     Hz     ppm     Int.

   1271.29  14.195    293
    688.38   7.687    413
    686.52   7.666    737
    681.54   7.610    807
    679.69   7.590   1000
    678.61   7.578    994
    676.17   7.550    254
    673.24   7.518    404
    671.58   7.499    471
    669.34   7.474    285
    665.04   7.426    952
    657.03   7.337    628
    654.00   7.303    562
    652.25   7.283    505
    650.88   7.268    385
    647.07   7.225    759
    646.09   7.215    690
    643.75   7.188    150
    641.80   7.167    128
    641.31   7.161    125
    640.82   7.156    139
    640.43   7.151    139
    636.62   7.109    355
    633.01   7.069    314
    631.45   7.051    213
    627.83   7.011    171

in CDCl3